CA2398108A1 - Partially dehydrated reaction product, process for making same, and emulsion containing same - Google Patents
Partially dehydrated reaction product, process for making same, and emulsion containing same Download PDFInfo
- Publication number
- CA2398108A1 CA2398108A1 CA002398108A CA2398108A CA2398108A1 CA 2398108 A1 CA2398108 A1 CA 2398108A1 CA 002398108 A CA002398108 A CA 002398108A CA 2398108 A CA2398108 A CA 2398108A CA 2398108 A1 CA2398108 A1 CA 2398108A1
- Authority
- CA
- Canada
- Prior art keywords
- mixture
- water
- amide
- reaction
- hydroxyamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000839 emulsion Substances 0.000 title abstract 4
- 239000007795 chemical reaction product Substances 0.000 title 1
- 239000000203 mixture Substances 0.000 abstract 10
- 150000001408 amides Chemical class 0.000 abstract 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 6
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 5
- 150000002148 esters Chemical class 0.000 abstract 5
- 229920000768 polyamine Polymers 0.000 abstract 5
- 229920005862 polyol Polymers 0.000 abstract 5
- 150000003077 polyols Chemical class 0.000 abstract 5
- 150000003839 salts Chemical class 0.000 abstract 5
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical class OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 abstract 5
- 239000013067 intermediate product Substances 0.000 abstract 4
- FALRKNHUBBKYCC-UHFFFAOYSA-N 2-(chloromethyl)pyridine-3-carbonitrile Chemical class ClCC1=NC=CC=C1C#N FALRKNHUBBKYCC-UHFFFAOYSA-N 0.000 abstract 3
- 229940014800 succinic anhydride Drugs 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 239000003995 emulsifying agent Substances 0.000 abstract 2
- 150000003949 imides Chemical class 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- 239000001384 succinic acid Substances 0.000 abstract 2
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 239000002360 explosive Substances 0.000 abstract 1
- 239000003337 fertilizer Substances 0.000 abstract 1
- 239000000446 fuel Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 125000001183 hydrocarbyl group Chemical group 0.000 abstract 1
- 239000000314 lubricant Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/32—Liquid carbonaceous fuels consisting of coal-oil suspensions or aqueous emulsions or oil emulsions
- C10L1/328—Oil emulsions containing water or any other hydrophilic phase
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
- C06B47/14—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase comprising a solid component and an aqueous phase
- C06B47/145—Water in oil emulsion type explosives in which a carbonaceous fuel forms the continuous phase
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/16—Amines or polyamines
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/22—Amides or hydrazides
Abstract
An emulsifier composition comprising a partially deyhdrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, or a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of the acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating the first intermediate product to form a second intermediate product with water of reaction being formed, and separating a portion of the water of reaction from the second intermediate product, when (A) is the succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of the succinic anhydride, when (A) is one succinic acid the amount of water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of the succinic acid, the partially dehydrated product having a total acid number in the range of about 20 to about 100 mg of KOH/g. The emulsifier composition can be used for making emulsions, for example explosive emulsions, emulsion fertilizers, water-blended fuels and lubricants.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/490,759 US6780209B1 (en) | 2000-01-24 | 2000-01-24 | Partially dehydrated reaction product process for making same, and emulsion containing same |
US09/490,759 | 2000-01-24 | ||
PCT/US2001/001939 WO2001052976A2 (en) | 2000-01-24 | 2001-01-22 | Partially dehydrated reaction product, process for making same, and emulsion containing same |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2398108A1 true CA2398108A1 (en) | 2001-07-26 |
CA2398108C CA2398108C (en) | 2008-12-23 |
Family
ID=23949341
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002398108A Expired - Fee Related CA2398108C (en) | 2000-01-24 | 2001-01-22 | Partially dehydrated reaction product, process for making same, and emulsion containing same |
Country Status (7)
Country | Link |
---|---|
US (2) | US6780209B1 (en) |
EP (1) | EP1259311B1 (en) |
JP (1) | JP5322362B2 (en) |
AU (1) | AU782124B2 (en) |
CA (1) | CA2398108C (en) |
DE (1) | DE60110044T2 (en) |
WO (1) | WO2001052976A2 (en) |
Families Citing this family (32)
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US6444716B1 (en) | 2000-01-24 | 2002-09-03 | The Procter & Gamble Company | Foam materials and high internal phase emulsions made using oxidatively stable emulsifiers |
US6207724B1 (en) * | 2000-01-24 | 2001-03-27 | The Procter & Gamble Company | Foam materials and high internal phase emulsions made using oxidatively stable emulsifiers |
AUPR253901A0 (en) * | 2001-01-12 | 2001-02-08 | Nuplex Industries (Aust) Pty Ltd | Emulsifier |
US20030158079A1 (en) * | 2001-10-19 | 2003-08-21 | The Procter & Gamble Company | Controlled benefit agent delivery system |
US20110104501A1 (en) * | 2005-03-01 | 2011-05-05 | The Wood Coatings Research Group, | Emulsions Useful for Coatings and Coating Additives |
US7771550B2 (en) * | 2005-10-07 | 2010-08-10 | Dyno Nobel, Inc. | Method and system for manufacture and delivery of an emulsion explosive |
JP4163219B2 (en) * | 2006-04-27 | 2008-10-08 | 横浜ゴム株式会社 | Thermoplastic elastomer and thermoplastic elastomer composition |
TWI392518B (en) * | 2006-05-23 | 2013-04-11 | Fancl Corp | Cosmetics containing diethylene glycol diol diol |
WO2008013844A2 (en) * | 2006-07-25 | 2008-01-31 | General Vortex Energy, Inc. | System, apparatus and method for combustion of metal and other fuels |
AT506695B1 (en) * | 2008-11-14 | 2009-11-15 | Kemira Chemie Ges Mbh | COMPOSITION FOR PAPER LUBRICATION |
US8221566B1 (en) * | 2009-07-02 | 2012-07-17 | The United States Of America As Represented By The Secretary Of The Navy | Process for employing HNFX as a biocidal explosive |
US8613838B2 (en) * | 2009-07-31 | 2013-12-24 | Vertex Energy, Lp | System for making a usable hydrocarbon product from used oil |
US8398847B2 (en) * | 2009-07-31 | 2013-03-19 | Vertex Energy, Lp | Method for making a usable hydrocarbon product from used oil |
WO2011146827A1 (en) | 2010-05-21 | 2011-11-24 | James Kenneth Sanders | Methods for increasing oil production |
PL2865735T3 (en) | 2011-03-29 | 2018-08-31 | Fuelina Technologies, Llc | Method and apparatus for making a hybrid fuel |
SE1150359A1 (en) * | 2011-04-26 | 2012-10-27 | OrganoPetroleum PSP AB | Improved method |
KR101963693B1 (en) | 2011-09-13 | 2019-03-29 | 루브리졸 어드밴스드 머티어리얼스, 인코포레이티드 | Surfactant responsive emulsion polymerized micro-gels |
BR112014005903B1 (en) | 2011-09-13 | 2021-03-02 | Lubrizol Advanced Mat Inc | flow limit fluid composition, drilling fluid, hydraulic fracture fluid, and, use of a flow limit fluid composition |
CN102718613B (en) * | 2012-07-03 | 2014-09-03 | 保利民爆济南科技有限公司 | Half-esterification high polymer emulsifying agent for industrial explosives |
WO2014028715A1 (en) | 2012-08-16 | 2014-02-20 | Helena Holding Company | Solvent free n-alkyl thiosphoric triamide formulations |
US9096476B2 (en) | 2012-08-31 | 2015-08-04 | Helena Chemical Corp. | Stabilized n-alkyl thiosphoric triamide solvent systems for use in nitrogen fertilizer |
BR112015014494A2 (en) | 2012-12-20 | 2017-07-11 | Lubrizol Advanced Mat Inc | method for reducing skin irritation induced by a surfactant-containing composition, and, |
KR20150128792A (en) | 2013-03-08 | 2015-11-18 | 루브리졸 어드밴스드 머티어리얼스, 인코포레이티드 | Polymers and methods to mitigate the loss of silicone deposition from keratinous substrates |
KR20150126894A (en) | 2013-03-08 | 2015-11-13 | 루브리졸 어드밴스드 머티어리얼스, 인코포레이티드 | Improved foaming performance in cleansing compositions through the use of nonionic, amphiphilic polymers |
EP3227411B1 (en) | 2014-12-03 | 2019-09-04 | Drexel University | Direct incorporation of natural gas into hydrocarbon liquid fuels |
WO2016100160A1 (en) | 2014-12-15 | 2016-06-23 | Dyno Nobel Inc. | Explosive compositions and related methods |
CN104927896B (en) * | 2015-06-04 | 2017-03-15 | 天津亿利科能源科技发展股份有限公司 | A kind of viscous crude field high efficient oil dissolubility demulsifier |
MX2018002654A (en) | 2015-09-01 | 2019-05-27 | Univ Sydney | Blasting agent. |
SG11202006602WA (en) * | 2018-02-20 | 2020-08-28 | Dyno Nobel Inc | Inhibited emulsions for use in blasting in reactive ground or under high temperature conditions |
CN110846000A (en) * | 2018-08-20 | 2020-02-28 | 任丘市诚亿化工有限公司 | Emulsifier for oil-based drilling fluid and production process and application thereof |
USD927084S1 (en) | 2018-11-22 | 2021-08-03 | Riddell, Inc. | Pad member of an internal padding assembly of a protective sports helmet |
WO2023137323A1 (en) * | 2022-01-13 | 2023-07-20 | Ecolab Usa Inc. | Antistatic fuel additives |
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US2868781A (en) | 1956-04-23 | 1959-01-13 | Monsanto Chemicals | Carbohydrate esters of carboxylic acids and methods of preparing same |
US2973353A (en) | 1956-06-29 | 1961-02-28 | Monsanto Chemicals | Carbohydrate mono-esters |
US3256321A (en) | 1962-07-16 | 1966-06-14 | Continental Oil Co | 2, 2-dialkyl alkanoic acid diesters of 2, 2-dialkyl glycols |
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-
2000
- 2000-01-24 US US09/490,759 patent/US6780209B1/en not_active Expired - Fee Related
-
2001
- 2001-01-22 JP JP2001553020A patent/JP5322362B2/en not_active Expired - Fee Related
- 2001-01-22 DE DE60110044T patent/DE60110044T2/en not_active Expired - Lifetime
- 2001-01-22 EP EP01906608A patent/EP1259311B1/en not_active Expired - Lifetime
- 2001-01-22 CA CA002398108A patent/CA2398108C/en not_active Expired - Fee Related
- 2001-01-22 AU AU34497/01A patent/AU782124B2/en not_active Ceased
- 2001-01-22 WO PCT/US2001/001939 patent/WO2001052976A2/en active IP Right Grant
-
2003
- 2003-08-22 US US10/646,281 patent/US7044988B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1259311B1 (en) | 2005-04-13 |
US6780209B1 (en) | 2004-08-24 |
AU3449701A (en) | 2001-07-31 |
EP1259311A2 (en) | 2002-11-27 |
DE60110044T2 (en) | 2006-01-26 |
WO2001052976A9 (en) | 2002-10-24 |
JP2003520665A (en) | 2003-07-08 |
WO2001052976A2 (en) | 2001-07-26 |
AU782124B2 (en) | 2005-07-07 |
CA2398108C (en) | 2008-12-23 |
JP5322362B2 (en) | 2013-10-23 |
US20040055677A1 (en) | 2004-03-25 |
DE60110044D1 (en) | 2005-05-19 |
US7044988B2 (en) | 2006-05-16 |
WO2001052976A3 (en) | 2002-09-12 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKLA | Lapsed |
Effective date: 20170123 |