CA2474622A1 - Apparatus and method for closed-loop control of laser welder for welding polymeric catheter components - Google Patents
Apparatus and method for closed-loop control of laser welder for welding polymeric catheter components Download PDFInfo
- Publication number
- CA2474622A1 CA2474622A1 CA002474622A CA2474622A CA2474622A1 CA 2474622 A1 CA2474622 A1 CA 2474622A1 CA 002474622 A CA002474622 A CA 002474622A CA 2474622 A CA2474622 A CA 2474622A CA 2474622 A1 CA2474622 A1 CA 2474622A1
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- Prior art keywords
- bond site
- laser beam
- laser
- directing
- mirror
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/02—Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
- B23K26/03—Observing, e.g. monitoring, the workpiece
- B23K26/034—Observing the temperature of the workpiece
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/02—Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
- B23K26/03—Observing, e.g. monitoring, the workpiece
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/16—Laser beams
- B29C65/1629—Laser beams characterised by the way of heating the interface
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/05—Particular design of joint configurations
- B29C66/10—Particular design of joint configurations particular design of the joint cross-sections
- B29C66/11—Joint cross-sections comprising a single joint-segment, i.e. one of the parts to be joined comprising a single joint-segment in the joint cross-section
- B29C66/114—Single butt joints
- B29C66/1142—Single butt to butt joints
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
- B29C66/51—Joining tubular articles, profiled elements or bars; Joining single elements to tubular articles, hollow articles or bars; Joining several hollow-preforms to form hollow or tubular articles
- B29C66/52—Joining tubular articles, bars or profiled elements
- B29C66/522—Joining tubular articles
- B29C66/5221—Joining tubular articles for forming coaxial connections, i.e. the tubular articles to be joined forming a zero angle relative to each other
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
- B29C66/51—Joining tubular articles, profiled elements or bars; Joining single elements to tubular articles, hollow articles or bars; Joining several hollow-preforms to form hollow or tubular articles
- B29C66/53—Joining single elements to tubular articles, hollow articles or bars
- B29C66/532—Joining single elements to the wall of tubular articles, hollow articles or bars
- B29C66/5324—Joining single elements to the wall of tubular articles, hollow articles or bars said single elements being substantially annular, i.e. of finite length
- B29C66/53241—Joining single elements to the wall of tubular articles, hollow articles or bars said single elements being substantially annular, i.e. of finite length said articles being tubular and said substantially annular single elements being of finite length relative to the infinite length of said tubular articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/73—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset
- B29C66/739—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset
- B29C66/7392—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of at least one of the parts being a thermoplastic
- B29C66/73921—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of at least one of the parts being a thermoplastic characterised by the materials of both parts being thermoplastics
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/912—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux
- B29C66/9121—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux by measuring the temperature
- B29C66/91211—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux by measuring the temperature with special temperature measurement means or methods
- B29C66/91216—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux by measuring the temperature with special temperature measurement means or methods enabling contactless temperature measurements, e.g. using a pyrometer
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/912—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux
- B29C66/9121—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux by measuring the temperature
- B29C66/91221—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by measuring the temperature, the heat or the thermal flux by measuring the temperature of the parts to be joined
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/914—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux
- B29C66/9141—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature
- B29C66/91411—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature of the parts to be joined, e.g. the joining process taking the temperature of the parts to be joined into account
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/914—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux
- B29C66/9141—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature
- B29C66/91431—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature the temperature being kept constant over time
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/914—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux
- B29C66/9161—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the heat or the thermal flux, i.e. the heat flux
- B29C66/91641—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the heat or the thermal flux, i.e. the heat flux the heat or the thermal flux being non-constant over time
- B29C66/91643—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the heat or the thermal flux, i.e. the heat flux the heat or the thermal flux being non-constant over time following a heat-time profile
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/919—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux characterised by specific temperature, heat or thermal flux values or ranges
- B29C66/9192—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux characterised by specific temperature, heat or thermal flux values or ranges in explicit relation to another variable, e.g. temperature diagrams
- B29C66/91951—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux characterised by specific temperature, heat or thermal flux values or ranges in explicit relation to another variable, e.g. temperature diagrams in explicit relation to time, e.g. temperature-time diagrams
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/96—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process
- B29C66/961—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process involving a feedback loop mechanism, e.g. comparison with a desired value
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
- B29C35/08—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
- B29C35/0805—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation
- B29C2035/0822—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation using IR radiation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/16—Laser beams
- B29C65/1603—Laser beams characterised by the type of electromagnetic radiation
- B29C65/1612—Infrared [IR] radiation, e.g. by infrared lasers
- B29C65/1616—Near infrared radiation [NIR], e.g. by YAG lasers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/16—Laser beams
- B29C65/1603—Laser beams characterised by the type of electromagnetic radiation
- B29C65/1612—Infrared [IR] radiation, e.g. by infrared lasers
- B29C65/1619—Mid infrared radiation [MIR], e.g. by CO or CO2 lasers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/16—Laser beams
- B29C65/1629—Laser beams characterised by the way of heating the interface
- B29C65/1635—Laser beams characterised by the way of heating the interface at least passing through one of the parts to be joined, i.e. laser transmission welding
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/16—Laser beams
- B29C65/1629—Laser beams characterised by the way of heating the interface
- B29C65/1674—Laser beams characterised by the way of heating the interface making use of laser diodes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/16—Laser beams
- B29C65/1687—Laser beams making use of light guides
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/71—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the composition of the plastics material of the parts to be joined
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/74—Joining plastics material to non-plastics material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/74—Joining plastics material to non-plastics material
- B29C66/742—Joining plastics material to non-plastics material to metals or their alloys
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/74—Joining plastics material to non-plastics material
- B29C66/746—Joining plastics material to non-plastics material to inorganic materials not provided for in groups B29C66/742 - B29C66/744
- B29C66/7465—Glass
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/914—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux
- B29C66/9141—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature
- B29C66/91441—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature the temperature being non-constant over time
- B29C66/91443—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the temperature the temperature being non-constant over time following a temperature-time profile
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/91—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux
- B29C66/919—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux characterised by specific temperature, heat or thermal flux values or ranges
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/94—Measuring or controlling the joining process by measuring or controlling the time
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/959—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 characterised by specific values or ranges of said specific variables
- B29C66/9592—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 characterised by specific values or ranges of said specific variables in explicit relation to another variable, e.g. X-Y diagrams
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/96—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process
- B29C66/962—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process using proportional controllers, e.g. PID controllers [proportional–integral–derivative controllers]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/96—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process
- B29C66/965—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process using artificial neural networks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/96—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process
- B29C66/966—Measuring or controlling the joining process characterised by the method for implementing the controlling of the joining process using fuzzy logic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- B29L2031/00—Other particular articles
- B29L2031/753—Medical equipment; Accessories therefor
- B29L2031/7542—Catheters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- B29L2031/00—Other particular articles
- B29L2031/753—Medical equipment; Accessories therefor
- B29L2031/7542—Catheters
- B29L2031/7543—Balloon catheters
Abstract
A detector (30) detects thermal radiation (28) being emitted from a fusion bond site (26) while a laser beam (14) impinges on and heats at least a portion of the bond site. The detector (30) can provide an electrical signal to a signal processor for controllably adjusting the laser beam power. The electrical signal may be substantially correlated to the temperature of at least a region of the bond site. A workpiece support preferably positions a first (20) and second (22) polymeric body so that a fusion bond site is formed. The laser impinges on at least a portion of the fusion bond site such that it emits thermal radiation. The detector (30) senses the thermal radiation and preferably provides a signal to the signal processor. In an aspect of the present invention, the signal processor controllably adjusts the power of the laser beam based on the signal provide by the detector.
Claims (61)
1. A method for forming a fusion bond between polymeric materials comprising the steps of:
forming a bond site by positioning a portion of a first polymeric body with respect to a portion of a second body so that a fusion bond site is formed;
directing laser energy onto at least a portion of the first polymeric body within the bond site so that a fusion zone having an increased temperature is formed, the laser energy being directed to the bond site to provide a controllable emissive power spectrum of the fusion zone;
detecting the emissive power spectrum of infrared radiation being emitted from the fusion zone while directing the laser energy onto the bond site;
converting the detected emissive power spectrum of infrared radiation into an electrical signal; and controllably adjusting the laser energy that is directed onto the bond site based on the electrical signal to controllably obtain an emissive power spectrum of infrared radiation emitted from the fusion zone.
forming a bond site by positioning a portion of a first polymeric body with respect to a portion of a second body so that a fusion bond site is formed;
directing laser energy onto at least a portion of the first polymeric body within the bond site so that a fusion zone having an increased temperature is formed, the laser energy being directed to the bond site to provide a controllable emissive power spectrum of the fusion zone;
detecting the emissive power spectrum of infrared radiation being emitted from the fusion zone while directing the laser energy onto the bond site;
converting the detected emissive power spectrum of infrared radiation into an electrical signal; and controllably adjusting the laser energy that is directed onto the bond site based on the electrical signal to controllably obtain an emissive power spectrum of infrared radiation emitted from the fusion zone.
2. The method of claim 1, wherein the second body is a polymeric body.
3. The method of claim 1, wherein the second body is a stainless steel body.
4. The method of claim 1, wherein the first polymeric body of the forming step is a tubular catheter and the second body of the forming step is a polymeric dilatation balloon.
5. The method of claim 1, wherein the directing step comprises directing laser energy provided by a laser beam from CO2 laser, the laser energy having a wavelength of about 10.6 microns.
6. The method of claim 1, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at an angle between about 45 degrees and about 90 degrees.
7. The method of claim 1, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at a substantially normal angle of incidence.
8. The method of claim 1, wherein the detecting step comprises detecting the emissive power spectrum of infrared radiation being emitted from the fusion zone by a radiation detecting device.
9. The method of claim 8, wherein the radiation detecting device comprises a mercury-cadmium-telluride detector.
10. The method of claim 1, wherein the directing step further comprises directing the laser energy to the bond site with a mirror.
11. The method of claim 10, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at a substantially normal angle of incidence.
12. The method of claim 11, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at an angle between about 45 degrees and about 90 degrees.
13. The method of claim 12, wherein the detecting step comprises detecting the emissive power spectrum with a detector positioned on axis with at least a portion of the laser beam that is directed to the bond site.
14. The method of claim 13, wherein the mirror is a dichroic mirror.
15. The method of claim 1, wherein the controllably adjusting step comprises operatively connecting a control system to a detector by a signal based connection and operatively connecting the control system to a laser by a signal based connection.
16. The method of claim 15, further comprising providing an output signal from the control system for receipt of the laser by using a process control algorithm for controllably adjusting the power of the laser energy in response to the electrical signal of the converting step.
17. The method of claim 16, wherein the process control algorithm is a PID control algorithm.
18. The method of claim 1, further comprising directing the laser energy to an optical system with a first mirror, refocusing the laser beam to a predetermined shape with the optical system, and directing the laser energy to the bond site with a second mirror.
19. The method of claim 18, wherein the optical system comprises a first lens and a second lens for refocusing the laser energy as a hollow cylinder.
20. The method of claim 19, wherein the first mirror is a dichroic mirror and the second mirror is a parabolic mirror.
21. The method of claim 20, further comprising improving the signal to noise ratio of the detected infrared radiation by optically modulating and amplifying the infrared radiation and filtering out the radiation which is not modulated.
22. The method of claim 1, wherein the forming step comprises forming a bond site by positioning a portion of a first tubular catheter component with respect to a portion of a second tubular catheter component so that a substantially circular fusion bond site is formed.
23. The method of claim 1, wherein the forming step comprises forming a bond site by positioning a portion of a tubular catheter component with respect to portion of a dilatation balloon so that a substantially circular fusion bond site is formed.
24. An apparatus for forming a fusion bond between a component comprising a polymeric material and at least one additional component, the apparatus comprising:
a workpiece support for supporting and positioning a portion of a first workpiece body with respect to a portion of a second workpiece body so that a fusion bond site is formed;
a laser operatively positioned for directing a laser beam toward at least a portion of the bond site so as to form a fusion zone having an increased temperature, the laser comprising an adjustable power output laser;
a detector operatively positioned for detecting infrared radiation emitted from a fusion zone while a bond site comprising at least a portion of the polymeric material component is illuminated by the laser beam, wherein the infrared radiation has an emissive power spectrum that can be substantially correlated with the temperature of the fusion zone, and the detector includes a signal generator for creating a detector signal based on the emissive power spectrum; and a control system for receiving the detector signal and for sending a control signal to the laser for adjusting the power of the laser beam to obtain a predetermined emissive power spectrum for the infrared radiation being emitted from the fusion zone.
a workpiece support for supporting and positioning a portion of a first workpiece body with respect to a portion of a second workpiece body so that a fusion bond site is formed;
a laser operatively positioned for directing a laser beam toward at least a portion of the bond site so as to form a fusion zone having an increased temperature, the laser comprising an adjustable power output laser;
a detector operatively positioned for detecting infrared radiation emitted from a fusion zone while a bond site comprising at least a portion of the polymeric material component is illuminated by the laser beam, wherein the infrared radiation has an emissive power spectrum that can be substantially correlated with the temperature of the fusion zone, and the detector includes a signal generator for creating a detector signal based on the emissive power spectrum; and a control system for receiving the detector signal and for sending a control signal to the laser for adjusting the power of the laser beam to obtain a predetermined emissive power spectrum for the infrared radiation being emitted from the fusion zone.
25. The apparatus of claim 24, wherein the first workpiece body is a polymeric body.
26. The apparatus of claim 24, wherein the first workpiece body is a polymeric body and the second workpiece body is a polymeric body.
27. The apparatus of claim 26, wherein the first polymeric body is a tubular catheter and the second polymeric body is a dilatation balloon.
28. The apparatus of claim 24, wherein the laser is a CO2 laser having a wavelength of about 10.6 microns.
29. The apparatus of claim 24, wherein the laser is positioned such that the laser beam impinges on the bond site at a substantially normal angle of incidence.
30. The apparatus of claim 24, wherein the laser is positioned such that the laser beam impinges on the bond site at an angle between about 45 degrees and about 90 degrees.
31. The apparatus of claim 24, wherein the detector is a mercury-cadmium-telluride detector
32. The apparatus of claim 24, further comprising a mirror for directing the laser beam wherein the mirror is positioned such that the laser beam impinges on the bond site.
33. The apparatus of claim 32, wherein the mirror is positioned such that the laser beam impinges on the bond site at a substantially normal angle of incidence.
34. The apparatus of claim 33, wherein the detector is positioned on axis with a portion of the laser beam that is directed to the bond site.
35. The apparatus of claim 34, wherein the mirror is a dichroic mirror.
36. The apparatus of claim 24, wherein the control system is operatively connected to the detector by a signal based connection and wherein the control system is operatively connected to the laser by a signal based connection.
37. The apparatus of claim 36, wherein the control system utilizes a process control algorithm for providing an output signal for controllably adjusting the power of the laser beam in response to an input signal from the detector.
38. The apparatus of claim 37, wherein the process control algorithm is a PID control algorithm.
39. The apparatus of claim 24, further comprising an optical system for refocusing the laser beam to a predetermined shape and further comprising a mirror for directing the laser beam to the optical system and a mirror for directing the laser beam to the bond site after the laser beam leaves the optical system.
40. The apparatus of claim 39, wherein the optical system comprises a first lens and a second lens for refocusing the laser beam as a hollow cylinder.
41. The apparatus of claim 40, wherein the mirror is a parabolic mirror.
42. The apparatus of claim 24, further comprising an optical chopper and a lock-in amplifier for improving the signal to noise ration of the detected thermal radiation.
43. A method for forming a fusion bond between a plurality of components of a balloon catheter system comprising the steps of forming a bond site by positioning a portion of a tubular catheter component with respect to a portion of a dilatation balloon so that a substantially circular fusion bond site is formed;
directing laser energy onto at least a portion of the bond site so that a fusion zone having an increased temperature is formed, the laser energy being directed to the bond site to provide an emissive power spectrum of the fusion zone;
detecting the emissive power spectrum of infrared radiation being emitted from the fusion zone while directing the laser energy onto the bond site;
converting the detected emissive power spectrum of infrared radiation into an electrical signal; and controllably adjusting the laser energy that is directed onto the bond site based on the electrical signal to controllably obtain an emissive power spectrum of infrared radiation emitted from the fusion zone.
directing laser energy onto at least a portion of the bond site so that a fusion zone having an increased temperature is formed, the laser energy being directed to the bond site to provide an emissive power spectrum of the fusion zone;
detecting the emissive power spectrum of infrared radiation being emitted from the fusion zone while directing the laser energy onto the bond site;
converting the detected emissive power spectrum of infrared radiation into an electrical signal; and controllably adjusting the laser energy that is directed onto the bond site based on the electrical signal to controllably obtain an emissive power spectrum of infrared radiation emitted from the fusion zone.
44. The method of claim 43, wherein the tubular catheter component is a polymeric catheter component.
45. The method of claim 43, wherein the directing step comprises directing laser energy provided by a laser beam from CO2 laser, the laser energy having a wavelength of about 10.6 microns.
46. The method of claim 43, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at an angle between about 45 degrees and about 90 degrees.
47. The method of claim 43, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at a substantially normal angle of incidence.
48. The method of claim 43, wherein the detecting step comprises detecting the emissive power spectrum of infrared radiation being emitted from the fusion zone by a radiation detecting device.
49. The method of claim 48, wherein the radiation detecting device comprises a mercury-cadmium-telluride detector.
50. The method of claim 43, wherein the directing step further comprises directing the laser energy to the bond site with a mirror.
51. The method of claim 50, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at a substantially normal angle of incidence.
52. The method of claim 51, wherein the directing step comprises directing laser energy as a laser beam such that the laser beam impinges on the bond site at an angle between about 45 degrees and about 90 degrees.
53. The method of claim 52, wherein the detecting step comprises detecting the emissive power spectrum with a detector positioned on axis with a portion of the laser beam that is directed to the bond site.
54. The method of claim 53, wherein the mirror is a dichroic mirror.
55. The method of claim 43, wherein the controllably adjusting step comprises operatively connecting a control system to the detector by a signal based connection and operatively connecting the control system to a laser by a signal based connection.
56. The method of claim 55, further comprising providing an output signal from the control system by using a process control algorithm for controllably adjusting the power of the laser energy in response to the electrical signal of the converting step.
57. The method of claim 56, wherein the process control algorithm is a PID control algorithm.
58. The method of claim 43, further comprising directing the laser energy to an optical system with a first mirror, refocusing the laser beam to a predetermined shape with the optical system, and directing the laser energy to the bond site with a second mirror.
59. The method of claim 58, wherein the optical system comprises a first lens and a second lens for refocusing the laser energy as a hollow cylinder.
60. The method of claim 59, wherein the first mirror is a dichroic mirror and the second mirror is a parabolic mirror.
61. The method of claim 43, further comprising improving the signal to noise ration of the detected infrared radiation by optically modulating and amplifying the infrared radiation and filtering out the radiation which is not modulated.
Applications Claiming Priority (3)
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US10/059,634 | 2002-01-28 | ||
US10/059,634 US6858104B2 (en) | 2002-01-28 | 2002-01-28 | Apparatus and method for closed-loop control of laser welder for welding polymeric catheter components |
PCT/US2003/001856 WO2003064140A2 (en) | 2002-01-28 | 2003-01-21 | Apparatus and method for closed-loop control of laser welder for welding polymeric catheter components |
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- 2003-01-21 ES ES03705862T patent/ES2320433T3/en not_active Expired - Lifetime
- 2003-01-21 DE DE60325835T patent/DE60325835D1/en not_active Expired - Lifetime
- 2003-01-21 CA CA2474622A patent/CA2474622C/en not_active Expired - Fee Related
- 2003-01-21 EP EP03705862A patent/EP1478503B1/en not_active Expired - Lifetime
- 2003-01-21 AU AU2003207643A patent/AU2003207643A1/en not_active Abandoned
- 2003-01-21 AT AT03705862T patent/ATE420759T1/en not_active IP Right Cessation
- 2003-01-21 JP JP2003563801A patent/JP2005515916A/en active Pending
- 2003-01-21 WO PCT/US2003/001856 patent/WO2003064140A2/en active Application Filing
Also Published As
Publication number | Publication date |
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DE60325835D1 (en) | 2009-03-05 |
JP2005515916A (en) | 2005-06-02 |
US20030141002A1 (en) | 2003-07-31 |
EP1478503A2 (en) | 2004-11-24 |
CA2474622C (en) | 2010-10-26 |
WO2003064140A3 (en) | 2003-11-06 |
ATE420759T1 (en) | 2009-01-15 |
EP1478503B1 (en) | 2009-01-14 |
WO2003064140A2 (en) | 2003-08-07 |
US6858104B2 (en) | 2005-02-22 |
AU2003207643A1 (en) | 2003-09-02 |
ES2320433T3 (en) | 2009-05-22 |
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