CN101040016A - 用于罐的涂料组合物和涂覆方法 - Google Patents
用于罐的涂料组合物和涂覆方法 Download PDFInfo
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- CN101040016A CN101040016A CNA2005800349149A CN200580034914A CN101040016A CN 101040016 A CN101040016 A CN 101040016A CN A2005800349149 A CNA2005800349149 A CN A2005800349149A CN 200580034914 A CN200580034914 A CN 200580034914A CN 101040016 A CN101040016 A CN 101040016A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
Description
化学名 | 商品名 | 供应商 | 地点 |
冰甲基丙烯酸 | Rohm&Haas | Philadelphia,PA | |
丙烯酸丁酯 | Rohm&Haas | Philadelphia,PA | |
苯乙烯 | Rohm&Haas | Philadelphia,PA | |
过氧化苯甲酰 | Norac Company | Helena,AR |
丁醇 | Dow | Midland,MI | |
乙二醇丁基醚 | 丁基溶纤剂/Dowanol EB | Dow | Midland,MI |
甲基丙烯酸丁酯 | Rohm&Haas | Philadelphia,PA | |
过辛酸叔丁酯 | Arkema | Philadelphia,PA | |
丙烯酸乙酯 | Rohm&Haas | Philadelphia,PA | |
丙烯酸 | Rohm&Haas | Philadelphia,PA | |
甲基丙烯酸羟丙酯 | ROCRYL410 | Rohm&Haas | Philadelphia,PA |
甲基丙烯酸羟乙酯 | ROCRYL400 | Rohm&Haas | Philadelphia,PA |
二甲基乙醇胺 | HuntsmanChemical | Dallas,TX | |
甲基丙烯酸缩水甘油酯 | SR 379 | Sartomer,Inc | Warrington,PA |
过氧化氢 | AshlandChemical | Pittsburgh,PA | |
苯偶姻 | Estron | Calvert City,KY | |
N-异丁氧基甲基丙烯酰胺 | CYLINKIBMA单体 | Cytec Ind. | West Patterson,NJ |
戊醇 | Dow | Midland,MI | |
丙二醇丁基醚 | DOWANOLPNB | Dow | Midland,MI |
仲醇乙氧基化物 | TERGITOL15-S-7 | Dow | Midland,MI |
仲丁醇 | Dow | Midland,MI | |
聚乙烯蜡 | Slipayd 404 | Elementis | Staines,UK |
热固性酚基酚醛树脂 | SD-912B | Valspar | Minneapolis,MN |
Carnuba蜡乳液 | Michemlube160PFE | Michelman | Cincinnati,OH |
异辛醇 | AldrichChemical | Milwaukee,WI | |
聚乙烯蜡 | Lanco Glidd5118 | Lubrizol | Wickliffe,OH |
二丙二醇 | AldrichChemical | Milwaukee,WI | |
间苯二酸 | BP Amoco | Chicago,IL | |
氧化二丁锡 | Fastcat 4201 | Arkema | Philadelphia,PA |
二甲苯 | Exxon | Newark,NJ | |
偏苯三酸酐 | BP Amoco | Chicago,IL | |
铁络合物 | Hamp-OL4.5%铁 | TraylorChemical | Orlando,FL |
异抗坏血酸 | AldrichChemical | Milwaukee,WI | |
叔丁基过氧化氢 | TrigonoxA-W70 | Akzo | Philadelphia,PA |
乙二醇 | AshlandChemical | Pittsburgh,PA | |
癸二酸 | IvanhoeIndutries | Tampa.FL | |
1,4-环己烷二甲醇(90%在水中) | CHDM-90 | Eastman | Kingsport,TN |
丁基锡酸 | Fastcat 4100 | Arkema | Philadelphia,PA |
4-羟基苯甲酸 | Acros Organics | Houston,TX |
through FisherScientific | |||
1,4-环己烷二甲醇二缩水甘油醚 | ErisysGE-22 | CVC SpecialtyChemicals | Maple Shade,NJ |
乙基三苯基碘化_ | Catalyst1201 | DeepwaterChemicals | Woodward,OK |
琥珀酸酐 | JLM Marketing | Tampa,FL | |
双酚A | Dow | Midland,MI | |
双酚A二缩水甘油醚 | Epon 828 | ResolutionPerformanceProducts | Houston,TX |
甲基异丁基酮 | Dow | Midland,MI | |
二价酸酯 | Dupont | Wilminton,DE | |
丙二醇甲基醚 | Dowanol PM | Dow | Midland,MI |
实施例1 | 第4批 | 第5批 | 第6批 | 第7批 | 第8批 | 第9批 | 第10批 | 第11批 |
MAA | 45 | 30 | 45 | 0 | 30 | 45 | 25 | 45 |
EA | 25 | 50 | 45 | 23 | 0 | 15 | 30 | 0 |
苯乙烯 | 30 | 5 | 10 | 10 | 25 | 0 | 25 | 10 |
BMA | 0 | 15 | 0 | 31 | 0 | 40 | 0 | 45 |
AA1 | 0 | 0 | 0 | 36 | 0 | 0 | 0 | 0 |
BA | 0 | 0 | 0 | 0 | 45 | 0 | 0 | 0 |
HPMA2 | 0 | 0 | 0 | 0 | 0 | 0 | 20 | 0 |
固含量 | 49.8% | 62.8% | 49.4% | 51.4% | 55.4% | 49.6% | 50.5% | 49.7% |
酸值 | 303 | 198 | 295 | 246 | 192 | 293 | 155 | 292 |
布氏粘度(cps) | 21,650 | 50,000 | 8,730 | 1,100 | 6,660 | 27,800 | 3,532 | 106,000 |
实施例1: | 第12批 | 第13批 | 第14批 | 第15批 |
MAA | 45 | 25 | 35 | 25 |
EA | 25 | 25 | 25 | 33 |
苯乙烯 | 30 | 30 | 30 | 22 |
HPMA | 0 | 20 | 10 | 20 |
固含量 | 51.2% | 50.2% | 50.0% | 50.3% |
酸值 | 301 | 171 | 234 | 169 |
布氏粘度(cps) | 25,400 | 2,820 | 6,020 | 2,220 |
实施例2 | 第4批 | 第5批 | 第6批 | 第7批 | 第8批 | 第9批 |
固含量 | 22.1% | 21.4% | 21.6% | 22.0% | 21.7% | 21.3% |
酸值 | 302 | 198 | 291 | 248 | 193 | 291 |
PH | 6.55 | 6.49 | 5.96 | 5.95 | 7.30 | 6.26 |
粘度1 | 2,060cps | 1,050cps | 1,770cps | --- | --- | 20秒 |
实施例2 | 第10批 | 第11批 | 第12批 | 第13批 | 第14批 | 第15批 |
固含量 | 21.7% | 21.7% | 22.0% | 21.3% | 21.7% | 22.2% |
酸值 | 153 | 300 | 291 | 169 | 231 | 271 |
pH | 7.29 | 6.54 | 6.37 | 6.72 | --- | 6.67 |
粘度1 | 881cps | 15秒 | 167cps | 304cps | 248cps | 1900cps |
实施例3 | 第4批 | 第6批 | 第7批 | 第8批 | 第9批 | 第10批 |
丙烯酸盐 | 实施例2:第4批 | 实施例2:第4批 | 实施例2:第4批 | 实施例2:第4批 | 实施例2:第4批 | 实施例2:第4批 |
单体 | ||||||
苯乙烯 | 41.0 | 39.0 | 42.0 | 43.5 | 43.5 | 45.0 |
BA | 30.0 | 53.0 | 54.0 | 54.5 | 54.5 | 55.0 |
BMA | 21.0 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 |
GMA | 8.0 | 8.0 | 4.0 | 2.0 | 2.0 | 0.0 |
乳液评价 | 外观良好 | 外观良好 | 外观良好 | 白色-高粘度 | 白色-低转化率 | 乳液分离 |
固含量 | 31.4% | 31.3% | 31.5% | 31.7% | 28.6% | 31.2% |
粘度(4号福特杯) | 22秒 | 51秒 | 103秒 | --- | 22秒 | --- |
布氏粘度 | --- | 230cps | 610cps | 25,000cps | --- | --- |
pH | 6.95 | 7.05 | 6.88 | --- | 6.65 | --- |
实施例3: | 第11批 | 第12批 | 第13批 | 第14批 | 第15批 | 第16批 | 第17批 | 第18批 |
丙烯酸/单体比 | 73/27 | 65/35 | ||||||
单体组合物1 | 单体组合物2 | 单体组合物1 | 单体组合物2 | |||||
GMA水平 | 低 | 高 | 低 | 高 | 低 | 高 | 低 | 高 |
单体 | ||||||||
苯乙烯 | 42 | 39 | 33 | 33 | 43 | 41 | 33 | 33 |
BA | 54 | 53 | 40 | 41 | 54 | 53 | 40 | 40 |
BMA | 0 | 0 | 23 | 18 | 0 | 0 | 24 | 21 |
GMA | 4 | 8 | 4 | 8 | 3 | 6 | 3 | 6 |
固含量 | 32.0% | 31.3% | 31.6% | 31.9% | 31.6% | 32.0% | 31.7% | 32.0% |
粘度(4号福特杯) | --- | 63秒 | --- | --- | 35秒 | 210秒 | 42秒 | --- |
布氏粘度(cps) | 10,000 | --- | 10,000 | 695 | --- | --- | --- | 1.384 |
酸值 | 74.7 | 72.9 | 74.9 | 70.2 | 101 | 96.1 | 101 | 96.5 |
水基对照1 | 实施例3:第11批 | 实施例3:第12批 | 实施例3:第13批 | 实施例3:第14批 | 实施例3:第15批 | 实施例3:第16批 | 实施例3:第17批 | 实施例3:第18批 | |
细裂纹 | 无 | 无 | 无 | 无 | 无 | 无 | 轻微 | 无 | 无 |
耐MEK性 | 19 | 5 | 6 | 3 | 7 | 5 | 6 | 4 | 8 |
起毛4 | 0.343 | 0.013 | 0.020 | 0.071 | 0.003 | 0.020 | 0.013 | 0.030 | 0.013 |
水蒸煮2 | |||||||||
发白 | 9.5 | 10 | 9.5 | 9.5 | 9.5 | 9 | 10 | 8 | 10 |
粘附性 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
巴氏灭菌3 | |||||||||
发白 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
粘附性 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
罐底连续性 | |||||||||
初始 | 0 | 0.22 | 25.3 | 11.5 | 57.8 | 17.7 | 133.5 | 27.5 | 132.2 |
蒸煮之后2 | 8.4 | 31.8 | 未测试 | 31.7 | 未测试 | 未测试 | 未测试 | 34.3 | 未测试 |
实施例3: | 第19批 | 第20批 | 第5b批 | 第21批 | 第22批 | 第23批 | 第24批 | 第25批 |
丙烯酸/单体比 | 73/27 | 65/35 | ||||||
单体组合物1 | 单体组合物2 | 单体组合物1 | 单体组合物2 | |||||
GMA水平 | 低 | 高 | 低 | 高 | 低 | 高 | 低 | 高 |
单体 | ||||||||
苯乙烯 | 42 | 39 | 33 | 33 | 43 | 41 | 33 | 33 |
BA | 54 | 53 | 40 | 41 | 54 | 53 | 40 | 40 |
BMA | 0 | 0 | 23 | 18 | 0 | 0 | 24 | 21 |
GMA | 4 | 8 | 4 | 8 | 3 | 6 | 3 | 6 |
固含量 | 31.5% | 31.6% | 31.6% | 31.4% | 31.3% | 31.6% | 31.5% | 31.7% |
粘度(4号福特杯) | 55秒 | 60秒 | 50秒 | 56秒 | 106秒 | --- | 70秒 | --- |
布氏粘度(cps) | --- | --- | --- | --- | --- | 2.624 | --- | 3.000 |
酸值 | 71.9 | 73.0 | 69.0 | 68.3 | 95.4 | 92.5 | 94.7 | 98.0 |
水基对照1 | 实施例3:第19批 | 实施例3:第20批 | 实施例3:第5b批 | 实施例3:第21批 | 实施例3:第22批 | 实施例3:第23批 | 实施例3:第24批 | 实施例3:第25批 | |
细裂纹 | 无 | 无 | 无 | 无 | 无 | 无 | 轻微 | 无 | 有 |
MEK | 19 | 4 | 7 | 4 | 10 | 6 | 11 | 4 | 6 |
起毛4 | 0.343 | 0.064 | 0.051 | 0.038 | 0.033 | 0.056 | 0.013 | 0.046 | 0.013 |
水蒸煮2 | |||||||||
发白 | 9.5 | 9.5 | 9.5 | 10 | 10 | 9.5 | 10 | 7 | 9.5 |
粘附性 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
巴氏灭菌3 | |||||||||
发白 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
粘附性 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
罐底连续性 | |||||||||
初始 | 0 | 5.5 | 2.6 | 6.0 | 12.3 | 20.2 | 61.2 | 1.9 | 93.6 |
蒸煮之后2 | 8.4 | 23.5 | 143 | 23.4 | 134.0 | 78.8 | 未测试 | 52.5 | 未测试 |
实施例3: | 第26批 | 第27批 | 第28批 | 第29批 | 第30批 | 第31批 | 第32批 | 第33批 |
丙烯酸/单体比 | 73/27 | 65/35 | ||||||
单体组合物1 | 单体组合物2 | 单体组合物1 | 单体组合物2 | |||||
GMA水平 | 低 | 高 | 低 | 高 | 低 | 高 | 低 | 高 |
单体 | ||||||||
苯乙烯 | 42 | 39 | 33 | 33 | 43 | 41 | 33 | 33 |
BA | 54 | 53 | 40 | 41 | 54 | 53 | 40 | 40 |
BMA | 0 | 0 | 23 | 18 | 0 | 0 | 24 | 21 |
GMA | 4 | 8 | 4 | 8 | 3 | 6 | 3 | 6 |
固含量 | 31.0% | 31.8% | 31.5% | 31.4% | 30.9% | 31.3% | 31.4% | 31.6% |
粘度(4号福特杯) | 40秒 | 48秒 | --- | 17秒 | 14秒 | 16秒 | 14秒 | 16秒 |
布氏粘度(cps) | --- | --- | 17,000 | --- | --- | --- | --- | --- |
酸值 | 73.5 | 68.7 | 71.2 | 68.6 | 97.0 | 93.9 | 99.3 | 93.9 |
水基对照1 | 实施例3:第26批 | 实施例3:第27批 | 实施例3:第28批 | 实施例3:第29批 | 实施例3:第30批 | 实施例3:第31批 | 实施例3:第32批 | 实施例3:第33批 | |
细裂纹 | 无 | 轻微 | 无 | 无 | 有 | 有 | 有 | 有 | 有 |
MEK | 19 | 7 | 8 | 3 | 12 | 3 | 5 | 7 | 6 |
起毛4 | 0.343 | 0.046 | 0.043 | 0.013 | 0.025 | 0.013 | 0.013 | 0.020 | 0.013 |
水蒸煮2 | |||||||||
发白 | 9.5 | 9.5 | 10.0 | 9.5 | 10 | 2 | 10 | 3 | 9.5 |
粘附性 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
巴氏灭菌3 | |||||||||
发白 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
粘附性 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 |
罐底连续性 | |||||||||
初始 | 0 | 82.4 | 107.4 | 12.2 | 215.6 | 178.9 | 315.9 | 161.5 | 336.9 |
蒸煮之后2 | 8.4 | 未测试 | 未测试 | 未测试 | 未测试 | 未测试 | 未测试 | 未测试 | 未测试 |
实施例3: | 第5b批 | 第34批 | 第35批 |
GMA水平 | 4% | 12% | 20% |
单体 | |||
苯乙烯 | 33 | 33 | 33 |
BA | 40 | 42 | 44 |
BMA | 23 | 13 | 3 |
GMA | 4 | 12 | 20 |
固含量 | 31.6% | 31.8% | 32.0% |
粘度(4号福特杯) | 50秒 | --- | --- |
布氏粘度(cps) | --- | 1,070 | 33,950 |
酸值 | 69.0 | 59.5 | 44.9 |
实施例3: | 第36批 | 第37批 | 第38批 | 第39批 | 第40批 | 第41批 | 第42批 |
IBMA水平 | 0% | 4% | 5% | 6% | 7% | 8% | 12% |
单体 | |||||||
苯乙烯 | 33 | 26 | 26 | 26 | 26 | 26 | 26 |
BA | 40 | 45 | 46 | 46 | 46 | 47 | 48 |
BMA | 23 | 21 | 19 | 18 | 17 | 15 | 10 |
GMA | 4 | 4 | 4 | 4 | 4 | 4 | 4 |
IBMA1 | 0 | 4 | 5 | 6 | 7 | 8 | 12 |
固含量% | 31.4% | 31.6% | 30.9% | 30.4% | 30.4% | 30.0% | 29.8% |
粘度(4号福特杯) | 22秒 | 17秒 | 18秒 | 16秒 | 16秒 | 16秒 | 17秒 |
酸值 | 38.1 | 40.1 | 40.9 | 39.5 | 40.5 | 41.0 | 40.4 |
实施例3 | 第36批 | 第37批 | 第38批 | 第39批 | 第40批 | 第41批 | 第42批 |
IBMA水平 | 0% | 4% | 5% | 6% | 7% | 8% | 12% |
罐底连续性 | |||||||
初始 | 3 | 1.5 | 1.1 | 1.0 | 0.4 | 0.9 | 0.7 |
蒸煮之后 | 19 | 12 | 4.3 | 6.5 | 6.6 | 9.3 | 31 |
实施例4 | 第1批 | 第2批 |
组成(份) | ||
实施例3:第4批 | 62 | 65 |
丁醇 | 6 | 5 |
丁基溶纤剂 | 3 | 0 |
戊醇 | 1 | 0 |
Dowanol PNB1 | 0 | 5 |
TERGITOL 15-S-72 | 0 | 1 |
去离子水 | 28 | 24 |
配制剂固含量,% | 20 | 21 |
粘度,4号福特杯 | 20秒 | 30秒 |
VOC,kg/l-H2O | 0.358 | 0.358 |
实施例4 | 第1批 | 第2批 |
金属暴露 | ||
初始 | 2mA | 3mA |
坠落损坏之后 | 2mA | 7mA |
耐MEK性 | <2 | <2 |
水蒸煮1 | ||
发白 | 无 | 无 |
粘附性 | 优异 | 优异 |
综合萃取2 | 0.25ppm | 3.8ppm |
实施例4 | 第3批 | 第4批 |
组成(份) | ||
实施例3:第4批 | 62.8 | 0 |
实施例3:第7批 | 0 | 62.8 |
去离子水 | 22.1 | 22.1 |
丁醇 | 5.9 | 5.3 |
丁基溶纤剂 | 2.9 | 2.9 |
戊醇 | 1.3 | 1.3 |
仲丁醇 | 0 | 0.5 |
去离子水 | 5.0 | 5.1 |
二甲基乙醇胺 | 根据需要 | 根据需要 |
配制剂固含量% | 20.7% | 20.4% |
粘度(4号福特杯) | 20秒 | 16秒 |
水基对照1 | 实施例4:第3批 | 实施例4:第4批 | |
涂层重量,mg/can | 124 | 123 | 121 |
金属暴露 | |||
初始 | 0.9mA | 2.2mA | 0.5mA |
坠落损坏之后 | 1.3mA | 2.9mA | 1.2mA |
耐MEK性 | 20-50 | 2-5 | <1 |
对圆顶的冲击 | 10 | 10 | 10 |
耐异丙醇性 | >100 | >100 | 5-10 |
水蒸煮2 | |||
发白 | 7 | 10 | 10 |
粘附性 | 10 | 10 | 10 |
Joy洗涤剂测试 | |||
发白 | 7 | 10 | 10 |
粘附性 | 10 | 10 | 10 |
综合萃取3 | <0.1ppm4 | <0.1ppm4 | <0.1ppm4 |
水基对照1 | 实施例5第1批 | |||
烘烤 | 10秒达到400_(204℃) | 10秒达到435_(224℃) | 10秒达到400_(204℃) | 10秒达到435_(224℃) |
耐MEK性 | 23 | 35 | 4 | 4 | ||||
起毛2 | 0.500 | 0.193 | 0.018 | 0.010 | ||||
Dowfax3 | ||||||||
发白 | 4 | 9 | 4 | 9 | ||||
粘附性 | 10 | 10 | 10 | 10 | ||||
巴氏灭菌4 | ||||||||
发白 | 6 | 9 | 5 | 10 | ||||
粘附性 | 10 | 10 | 10 | 10 | ||||
水蒸煮5 | ||||||||
发白 | 6.5 | 10 | 5.5 | 10 | ||||
粘附性 | 10 | 10 | 10 | 10 | ||||
罐底连续性 | 初始 | 之后 | 初始 | 之后 | 初始 | 之后 | 初始 | 之后 |
巴氏灭菌4 | 0.13 | 0.33 | 0.06 | 0.28 | 2.76 | 21.35 | 1.5 | 17.9 |
水蒸煮5 | 0.016 | 2.22 | 0.06 | 0.52 | 4.16 | 22.9 | 1.4 | 17.55 |
实施例5 | 第2批 | 第3批 | 第4批 |
实施例3第5批 | 95.7 | 0 | 0 |
实施例3第34批 | 0 | 95.7 | 0 |
实施例3第35批 | 0 | 0 | 95.7 |
酚醛树脂1 | 2.3 | 2.3 | 2.3 |
SLIPAYD 404 | 1.5 | 1.5 | 1.5 |
Michem Lube 160PFE2 | 0.5 | 0.5 | 0.5 |
水/溶剂3 | 达23%固含量 | 达23%固含量 | -- |
去离子水 | -- | -- | 达到23%固含量 |
实施例5 | 第2批 | 第3批 | 第4批 |
GMA水平 | 4% | 12% | 20% |
罐底连续性 | |||
初始 | 2 | 49 | 149 |
蒸煮之后1 | 21 | 193 | 304 |
实施例5第5批 | |
组成 | |
实施例3,第38批 | 90.80 |
Dowanol PNP1 | 2.425 |
Dowanol DPNB1 | 2.425 |
异辛醇 | 1.54 |
Michem Lube 160PFE | 0.57 |
Lanco Glidd 51182 | 2.24 |
固含量(%) | 27.5-29.5 |
粘度(4号福特杯) | 20秒-30秒 |
水基对照1 | 实施例5第5批 | |||||||
烘烤 | 10秒达到400_(204℃) | 10秒达到420_(215℃) | 10秒达到400_(204℃) | 10秒达到420_(215℃) | ||||
耐MEK性 | 34 | 40 | 10 | 8 | ||||
起毛4 | 0.178 | 0.094 | 0.074 | 0.038 | ||||
铅笔硬度 | 3H-4H | 3H | HB | HB | ||||
COF | 0.068 | 0.076 | 0.068 | 0.075 | ||||
巴氏灭菌2 | ||||||||
发白 | 10 | 10 | 9 | 10 | ||||
粘附性 | 10 | 10 | 10 | 10 | ||||
水蒸煮3 | ||||||||
发白 | 9 | 10 | 8 | 9 | ||||
粘附性 | 10 | 10 | 10 | 10 | ||||
罐底连续性 | 初始 | 之后 | 初始 | 之后 | 初始 | 之启 | 初始 | 之后 |
巴氏灭菌2 | 0.0 | 0.1 | 1.1 | 17.6 | 0.5 | 0.7 | 0.5 | 4.3 |
水蒸煮3 | 0.05 | 0.15 | 1.4 | 11.2 | 0.15 | 0.35 | 0.78 | 10.5 |
水基对照1 | 实施例6 | |
耐MEK性 | 22 | 11 |
起毛4 | 0.102 | 0.013 |
巴氏灭菌2 | ||
发白 | 10 | 9.5 |
粘附性 | 10 | 10 |
水蒸煮3 |
发白 | 10 | 10 |
粘附性 | 10 | 10 |
罐底连续性 | ||
初始 | 1.35 | 0.25 |
巴氏灭菌2 | 2.38 | 1.35 |
表24 | |
饮料罐内部喷涂的涂料组合物 | |
组成(份) | 实施例8 |
实施例7的物质 | 62.8 |
去离子水 | 25.3 |
丁基溶纤剂 | 5.1 |
戊醇 | 3.1 |
丁醇 | 0.7 |
去离子水 | 3.0 |
添加去离子水到18.5%固含量 | |
配制剂固含量,% | 18.5% |
粘度,4号福特杯 | 46秒 |
表25 | ||
内部喷涂薄膜性能 | ||
水基对照1 | 实施例8 | |
金属暴露 | ||
初始 | 2mA | 1mA |
坠落损坏之后 | 2mA | 5mA |
水蒸煮3 | ||
发白 | 无 | 无 |
粘附性 | 优异 | 优异 |
表26 | ||||||
在420_(215℃)下固化的实施例9阶段D的对比测试 | ||||||
水基对照1 | 溶剂基对照2 | 实施例9阶段D | ||||
MEK | 44 | 34 | 38 | |||
起毛3 | 0.0457 | 0.0457 | 0.000 | |||
COF | 0.061 | 0.066 | 0.063 | |||
巴氏灭菌4 | ||||||
发白 | 10 | 10 | 8-96 | |||
粘附性 | 10 | 10 | 10 | |||
水蒸煮5 | ||||||
发白 | 10 | 10 | 4-106 | |||
粘附性 | 10 | 10 | ||||
罐底连续性 | 初始 | 之后 | 初始 | 之后 | 初始 | 之启 |
巴氏灭菌 | 0.08 | 0.12 | 0.0 | 0.30 | 0.0 | 0.5 |
水蒸煮 | 0.10 | 0.4 | 0.02 | 0.72 | 0.27 | 1.2 |
表27 |
在440_(227℃)下固化的实施例9阶段D的对比测试 |
水基对照1 | 溶剂基对照2 | 实施例9阶段D | ||||
MEK | 52 | 37 | 40 | |||
起毛3 | 0.0559 | 0.0356 | 0.000 | |||
COF | 0.059 | 0.065 | 0.063 | |||
巴氏灭菌4 | ||||||
发白 | 10 | 10 | 8-106 | |||
粘附性 | 10 | 10 | 10 | |||
水蒸煮5 | ||||||
发白 | 10 | 10 | 6-106 | |||
粘附性 | 10 | 10 | ||||
罐底连续性 | 初始 | 之后 | 初始 | 之后 | 初始 | 之后 |
巴氏灭菌 | 0.0 | 0.48 | 0.07 | 0.23 | 0.1 | 0.8 |
水蒸煮 | 0.05 | 0.4 | 0.25 | 1.5 | 0.35 | 0.8 |
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