CN101041868A - 含钴、镍和硅的铜合金 - Google Patents
含钴、镍和硅的铜合金 Download PDFInfo
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- CN101041868A CN101041868A CNA2007100890982A CN200710089098A CN101041868A CN 101041868 A CN101041868 A CN 101041868A CN A2007100890982 A CNA2007100890982 A CN A2007100890982A CN 200710089098 A CN200710089098 A CN 200710089098A CN 101041868 A CN101041868 A CN 101041868A
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- 229910000881 Cu alloy Inorganic materials 0.000 title claims abstract description 85
- 229910017052 cobalt Inorganic materials 0.000 title claims abstract description 79
- 239000010941 cobalt Substances 0.000 title claims abstract description 79
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 title claims abstract description 77
- 239000010703 silicon Substances 0.000 title claims abstract description 45
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 43
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 168
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 164
- 239000000956 alloy Substances 0.000 claims abstract description 164
- 238000000034 method Methods 0.000 claims abstract description 103
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 73
- 229910052802 copper Inorganic materials 0.000 claims abstract description 55
- 239000010949 copper Substances 0.000 claims abstract description 55
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 54
- 238000000137 annealing Methods 0.000 claims abstract description 45
- 238000005482 strain hardening Methods 0.000 claims abstract description 33
- 238000005266 casting Methods 0.000 claims abstract description 32
- 229910052709 silver Inorganic materials 0.000 claims abstract description 26
- 239000004332 silver Substances 0.000 claims abstract description 19
- 239000012535 impurity Substances 0.000 claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- 230000032683 aging Effects 0.000 claims description 94
- 239000000243 solution Substances 0.000 claims description 60
- 238000011282 treatment Methods 0.000 claims description 59
- 239000011777 magnesium Substances 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 22
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 18
- 239000000463 material Substances 0.000 claims description 17
- 238000010791 quenching Methods 0.000 claims description 17
- 239000010936 titanium Substances 0.000 claims description 17
- 229910052749 magnesium Inorganic materials 0.000 claims description 16
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 15
- 238000012545 processing Methods 0.000 claims description 15
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 14
- 229910052719 titanium Inorganic materials 0.000 claims description 14
- 229910052726 zirconium Inorganic materials 0.000 claims description 13
- 230000000171 quenching effect Effects 0.000 claims description 12
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 11
- 238000005096 rolling process Methods 0.000 claims description 11
- 239000006104 solid solution Substances 0.000 claims description 8
- 238000005242 forging Methods 0.000 claims description 7
- 238000001556 precipitation Methods 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- 229910052698 phosphorus Inorganic materials 0.000 claims description 6
- 229910052718 tin Inorganic materials 0.000 claims description 6
- 229910052804 chromium Inorganic materials 0.000 claims description 5
- 229910052725 zinc Inorganic materials 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- 229910052787 antimony Inorganic materials 0.000 claims description 3
- 229910052785 arsenic Inorganic materials 0.000 claims description 3
- 229910052790 beryllium Inorganic materials 0.000 claims description 3
- 229910052796 boron Inorganic materials 0.000 claims description 3
- 229910052711 selenium Inorganic materials 0.000 claims description 3
- 229910052714 tellurium Inorganic materials 0.000 claims description 3
- 229910052748 manganese Inorganic materials 0.000 claims description 2
- 229910052717 sulfur Inorganic materials 0.000 claims description 2
- 230000009467 reduction Effects 0.000 abstract description 16
- 230000008569 process Effects 0.000 abstract description 14
- 229910021332 silicide Inorganic materials 0.000 abstract description 13
- 230000000694 effects Effects 0.000 abstract description 4
- RZJQYRCNDBMIAG-UHFFFAOYSA-N [Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Zn].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn] Chemical class [Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Cu].[Zn].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Ag].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn].[Sn] RZJQYRCNDBMIAG-UHFFFAOYSA-N 0.000 abstract 1
- ZUPBPXNOBDEWQT-UHFFFAOYSA-N [Si].[Ni].[Cu] Chemical compound [Si].[Ni].[Cu] ZUPBPXNOBDEWQT-UHFFFAOYSA-N 0.000 abstract 1
- 229910021484 silicon-nickel alloy Inorganic materials 0.000 abstract 1
- 235000013495 cobalt Nutrition 0.000 description 66
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 31
- 230000035882 stress Effects 0.000 description 31
- 238000005097 cold rolling Methods 0.000 description 21
- 238000005516 engineering process Methods 0.000 description 16
- 238000003483 aging Methods 0.000 description 15
- FVBUAEGBCNSCDD-UHFFFAOYSA-N silicide(4-) Chemical compound [Si-4] FVBUAEGBCNSCDD-UHFFFAOYSA-N 0.000 description 11
- 238000005452 bending Methods 0.000 description 9
- 239000002245 particle Substances 0.000 description 8
- 229920001296 polysiloxane Polymers 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 238000005098 hot rolling Methods 0.000 description 7
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 6
- 239000011135 tin Substances 0.000 description 6
- 229910000676 Si alloy Inorganic materials 0.000 description 5
- -1 and Chemical compound 0.000 description 5
- 230000008859 change Effects 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- UREBDLICKHMUKA-CXSFZGCWSA-N dexamethasone Chemical compound C1CC2=CC(=O)C=C[C@]2(C)[C@]2(F)[C@@H]1[C@@H]1C[C@@H](C)[C@@](C(=O)CO)(O)[C@@]1(C)C[C@@H]2O UREBDLICKHMUKA-CXSFZGCWSA-N 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 4
- 239000011651 chromium Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000011574 phosphorus Substances 0.000 description 4
- 239000011701 zinc Substances 0.000 description 4
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 3
- 229910000990 Ni alloy Inorganic materials 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000004881 precipitation hardening Methods 0.000 description 3
- 230000004044 response Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 229910000531 Co alloy Inorganic materials 0.000 description 2
- 229910000905 alloy phase Inorganic materials 0.000 description 2
- 238000005275 alloying Methods 0.000 description 2
- 238000009749 continuous casting Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000011133 lead Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000011669 selenium Substances 0.000 description 2
- 229910001316 Ag alloy Inorganic materials 0.000 description 1
- 229910000714 At alloy Inorganic materials 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229910000570 Cupronickel Inorganic materials 0.000 description 1
- 229910000861 Mg alloy Inorganic materials 0.000 description 1
- 229910001122 Mischmetal Inorganic materials 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 229910001128 Sn alloy Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 241000292547 Taraxacum minimum Species 0.000 description 1
- QVMHUALAQYRRBM-UHFFFAOYSA-N [P].[P] Chemical compound [P].[P] QVMHUALAQYRRBM-UHFFFAOYSA-N 0.000 description 1
- WSXTYCGGBHCYIG-UHFFFAOYSA-N [Si].[Co].[Cu] Chemical compound [Si].[Co].[Cu] WSXTYCGGBHCYIG-UHFFFAOYSA-N 0.000 description 1
- RMXTYBQNQCQHEU-UHFFFAOYSA-N ac1lawpn Chemical compound [Cr]#[Cr] RMXTYBQNQCQHEU-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium atom Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910021357 chromium silicide Inorganic materials 0.000 description 1
- 238000010835 comparative analysis Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- YOCUPQPZWBBYIX-UHFFFAOYSA-N copper nickel Chemical compound [Ni].[Cu] YOCUPQPZWBBYIX-UHFFFAOYSA-N 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000005261 decarburization Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- QNDQILQPPKQROV-UHFFFAOYSA-N dizinc Chemical compound [Zn]=[Zn] QNDQILQPPKQROV-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000013213 extrapolation Methods 0.000 description 1
- 230000005294 ferromagnetic effect Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000012417 linear regression Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 238000004452 microanalysis Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 150000003377 silicon compounds Chemical class 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000009718 spray deposition Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/08—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of copper or alloys based thereon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C9/00—Alloys based on copper
- C22C9/06—Alloys based on copper with nickel or cobalt as the next major constituent
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L23/00—Details of semiconductor or other solid state devices
- H01L23/48—Arrangements for conducting electric current to or from the solid state body in operation, e.g. leads, terminal arrangements ; Selection of materials therefor
- H01L23/488—Arrangements for conducting electric current to or from the solid state body in operation, e.g. leads, terminal arrangements ; Selection of materials therefor consisting of soldered or bonded constructions
- H01L23/495—Lead-frames or other flat leads
- H01L23/49579—Lead-frames or other flat leads characterised by the materials of the lead frames or layers thereon
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01R—ELECTRICALLY-CONDUCTIVE CONNECTIONS; STRUCTURAL ASSOCIATIONS OF A PLURALITY OF MUTUALLY-INSULATED ELECTRICAL CONNECTING ELEMENTS; COUPLING DEVICES; CURRENT COLLECTORS
- H01R13/00—Details of coupling devices of the kinds covered by groups H01R12/70 or H01R24/00 - H01R33/00
- H01R13/02—Contact members
- H01R13/03—Contact members characterised by the material, e.g. plating, or coating materials
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
- H01L2924/0001—Technical content checked by a classifier
- H01L2924/0002—Not covered by any one of groups H01L24/00, H01L24/00 and H01L2224/00
Abstract
Description
铸锭标号 | 钴 | 硅 | 镁 | 镍 | 镍∶钴 | (镍+钴)/硅 |
J394 | 0.89 | 0.41 | 0.05 | 1.46 | 1.64 | 5.73 |
J395 | -0- | 0.62 | 0.08 | 2.72 | -X- | 4.39 |
J401 | 1.06 | 0.62 | 0.08 | 1.67 | 1.67 | 4.40 |
J620 | 2.26 | 1.02 | 0.11 | 2.39 | 1.06 | 4.56 |
J623 | 1.06 | 0.49 | 0.11 | 1.53 | 1.44 | 5.29 |
J624 | 1.59 | 0.78 | 0.11 | 2.32 | 1.45 | 5.01 |
J658 | 0.58 | 0.60 | 0.09 | 2.00 | 3.45 | 4.30 |
J659 | 1.04 | 0.60 | 0.09 | 1.45 | 1.39 | 4.15 |
J660 | 1.55 | 0.59 | 0.08 | 1.45 | 0.94 | 5.08 |
J661 | 2.02 | 0.60 | 0.09 | 1.50 | 0.74 | 5.87 |
J662 | 1.01 | 0.59 | 0.09 | 2.00 | 1.98 | 5.10 |
J663 | 1.42 | 0.59 | 0.08 | 1.97 | 1.39 | 5.75 |
J665 | 1.44 | 0.37 | 0.09 | 1.97 | 1.37 | 9.22 |
J666 | 1.86 | 0.80 | 0.09 | 1.46 | 0.78 | 4.15 |
J667 | 2.38 | 0.82 | 0.10 | 1.51 | 0.63 | 4.74 |
J668 | 1.95 | 0.77 | 0.09 | 1.95 | 1.04 | 4.97 |
J669 | 0.98 | 0.82 | 0.09 | 3.01 | 3.07 | 4.87 |
J671 | 2.92 | 1.00 | 0.10 | 1.52 | 0.52 | 4.44 |
J672 | 2.32 | 1.00 | 0.09 | 2.38 | 1.03 | 4.70 |
J673 | 1.55 | 1.07 | 0.08 | 2.88 | 1.86 | 4.14 |
J676 | 1.86 | 0.71 | 0.10 | 1.45 | 0.78 | 4.66 |
J684 | 2.02 | 0.72 | 0.10 | 1.53+0.23Ti | 0.76 | 4.93 |
J686 | 1.92 | 0.71 | 0.11 | 1.50+0.28Ag | 0.78 | 4.82 |
J687 | 1.82 | 0.69 | 0.11 | 1.46+0.14Zr | 0.80 | 4.75 |
铸锭标号 | 钴 | 硅 | 镁 | 镍 | 镍∶钴 | (镍+钴)/硅 |
J716 | 1.73 | 0.74 | 0.10 | 1.72 | 0.99 | 4.60 |
J717 | 1.13 | 0.72 | 0.08 | 2.41 | 2.13 | 4.92 |
J718 | 0.51 | 0.73 | 0.09 | 3.08 | 6.04 | 4.92 |
J719 | 2.67 | 0.73 | 0.09 | -0- | -0- | 3.65 |
J720 | 1.83 | 0.73 | 0.09 | 0.96 | 0.52 | 3.82 |
J721 | 1.37 | 0.73 | 0.09 | 1.45 | 1.06 | 3.86 |
J722 | 0.89 | 0.73 | 0.09 | 1.93 | 2.17 | 3.86 |
J723 | 0.55 | 0.70 | 0.10 | 2.27 | 4.13 | 4.03 |
J724 | -0- | 0.69 | 0.07 | 2.82 | -X- | 4.09 |
J727 | 0.43 | 0.71 | 0.09 | 1.73 | 4.02 | 3.03 |
J728 | 0.70 | 0.72 | 0.10 | 1.52 | 2.17 | 3.08 |
J729 | 0.95 | 0.75 | 0.10 | 1.14 | 1.20 | 2.79 |
J730 | 0.66 | 0.73 | 0.10 | 0.68 | 1.03 | 1.84 |
J731 | -0- | 0.49 | 0.10 | 2.44 | -X- | 4.98 |
J737 | 1.14 | 0.38 | 0.10 | 0.55 | 0.48 | 4.45 |
J738 | 1.32 | 0.44 | 0.10 | 0.68 | 0.52 | 4.55 |
J739 | 1.60 | 0.56 | 0.10 | 0.82 | 0.51 | 4.32 |
J740 | 2.06 | 0.71 | 0.10 | 0.98 | 0.48 | 4.28 |
J741 | 2.23 | 0.81 | 0.11 | 1.10 | 0.49 | 4.11 |
J742 | 2.57 | 0.94 | 0.08 | 1.24 | 0.48 | 4.05 |
J743 | 2.92 | 1.13 | 0.09 | 1.40 | 0.48 | 3.82 |
J772 | 4.35 | 1.40 | 0.09 | 1.92 | 0.44 | 4.48 |
J824 | 1.80 | 0.60 | 0.12 | 0.77 | 0.43 | 4.28 |
J834 | 1.77 | 0.60 | -0- | 0.76+0.20Ag | 0.43 | 4.22 |
J835 | 1.88 | 0.64 | -0- | 0.75 | 0.40 | 4.11 |
J836 | 1.86 | 0.63 | 0.10 | 0.75+0.21Ag | 0.40 | 4.14 |
J910 | 0.64 | 0.56 | 0.09 | 1.79 | 2.80 | 3.86 |
铸锭标号 | 钴 | 硅 | 镁 | 镍 | 镍∶钴 | (镍+钴)/硅 |
J954 | 1.17 | 0.60 | -0- | 1.22+0.052Ag | 1.04 | 3.98 |
J955 | 1.18 | 0.59 | -0- | 1.21+0.099Ag | 1.03 | 4.05 |
J956 | 1.17 | 0.59 | -0- | 1.22+0.19Ag | 1.04 | 4.05 |
J969 | 1.04 | 0.61 | 0.001 | 1.37 | 1.32 | 3.95 |
J970 | 1.05 | 0.62 | 0.01 | 1.37 | 1.30 | 3.90 |
J971 | 1.04 | 0.62 | 0.021 | 1.38 | 1.33 | 3.90 |
J972 | 1.05 | 0.63 | 0.033 | 1.38 | 1.31 | 3.86 |
J973 | 1.05 | 0.62 | 0.044 | 1.39 | 1.32 | 3.94 |
J981 | 1.05 | 0.63 | 0.016 | 1.40+0.053Ag | 1.33 | 3.78 |
J982 | 1.06 | 0.62 | 0.025 | 1.39+0.099Ag | 1.31 | 3.95 |
J983 | 1.07 | 0.63 | 0.023 | 1.40+0.195Ag | 1.31 | 4.05 |
J984 | 1.06 | 0.63 | 0.017 | 1.39+0.39Ag | 1.31 | 3.89 |
J989 | 0.66 | 0.61 | 0.08 | 1.83 | 2.77 | 4.08 |
RN503014 | 1.97 | 0.74 | 0.09 | 1.48 | 0.75 | 4.60 |
铸锭标号 | 固溶热处理 | 晶体平均尺寸(微米) |
本发明的合金 | ||
J401 | 850℃/60秒950℃/60秒 | 616 |
J667 | 925℃/60秒950℃/60秒975℃/60秒 | 555 |
J671 | 925℃/60秒950℃/60秒975℃/60秒 | 555 |
J719 | 900℃/60秒950℃/60秒1000℃/60秒 | 7814 |
J720 | 900℃/60秒950℃/60秒1000℃/60秒 | 6820 |
J721 | 900℃/60秒950℃/60秒1000℃/60秒 | 8830 |
J722 | 900℃/60秒950℃/60秒1000℃/60秒 | 91343 |
铸锭标号 | 固溶热处理 | 晶体平均尺寸(微米) |
本发明的合金 | ||
J723 | 900℃/60秒950℃/60秒1000℃/60秒 | 91239 |
RN503014 | 925℃/60秒950℃/60秒975℃/60秒 | 568 |
对照例 | ||
J724Co=0 | 800℃/60秒840℃/60秒900℃/60秒950℃/60秒1000℃/60秒 | 7960140250 |
J394Si=0.41% | 850℃/60秒880℃/60秒950℃/60秒 | 91134 |
合金 | 硅(wt.%) | 镍+钴(wt.%) | 屈服强度 | 导电率(%IACS) | 90°MBR/t | ||
(ksi) | MPa) | GW | BW | ||||
本发明合金 | |||||||
J739 | 0.56 | 2.42 | 110 | 758 | 52.7 | 2.2 | 2.2 |
J740 | 0.71 | 3.04 | 113 | 779 | 52.8 | 2.7 | 2.3 |
J741 | 0.81 | 3.33 | 116 | 800 | 52.5 | 2.2 | 2.5 |
J742 | 0.94 | 3.81 | 118 | 814 | 51.7 | 2.3 | 3.9 |
J743 | 1.13 | 4.32 | 118 | 814 | 51.0 | 3.0 | 3.9 |
对照例 | |||||||
J737 | 0.38 | 1.69 | 104 | 717 | 56.5 | N.D. | N.D. |
J738 | 0.44 | 2.00 | 108 | 745 | 54.1 | 2.0 | 2.3 |
J772 | 1.40 | 6.27 | 121 | 834 | 47.0 | 3.9 | 3.9 |
合金 | 镍∶钴比值 | 成品尺寸时的性能 | ||
屈服强度 | 导电率(%IACS) | |||
(ksi) | (MPa) | |||
J719 | -0- | 104.8 | 722.6 | 54.0 |
J720 | 0.52 | 113.0 | 779.1 | 47.7 |
J721 | 1.06 | 115.3 | 795.0 | 46.8 |
J722 | 2.17 | 116.6 | 804.0 | 45.3 |
J723 | 4.13 | 114.9 | 792.2 | 45.6 |
合金 | (Ni+Co)/Si | 成品尺寸时的性能 | ||
屈服强度 | 导电性(%IACS) | |||
(MPa) | (ksi) | |||
J730 | 1.84 | 648.1 | 94.0 | 29.6 |
J729 | 2.79 | 732.9 | 106.3 | 38.4 |
J727 | 3.03 | 708.1 | 102.7 | 36.7 |
J728 | 3.08 | 737.8 | 107.0 | 36.8 |
J722 | 3.86 | 804.0 | 116.6 | 45.3 |
J721 | 3.86 | 795.0 | 115.3 | 46.8 |
J723 | 4.03 | 792.2 | 114.9 | 45.6 |
J673 | 4.14 | 850.8 | 123.4 | 45.9 |
J659 | 4.15 | 790.9 | 114.7 | 49.2 |
J666 | 4.15 | 805.3 | 116.8 | 49.9 |
J716 | 4.60 | 805.3 | 116.8 | 47.7 |
J672 | 4.70 | 809.5 | 117.4 | 44.3 |
J669 | 4.87 | 852.2 | 123.6 | 43.0 |
J717 | 4.92 | 829.5 | 120.3 | 45.5 |
J718 | 4.92 | 854.3 | 123.9 | 45.8 |
J668 | 4.97 | 812.2 | 117.8 | 46.3 |
J660 | 5.08 | 772.9 | 112.1 | 47.7 |
合金 | (Ni+Co)/Si | 成品尺寸时的性能 | ||
屈服强度 | 导电性(%IACS) | |||
(MPa) | (ksi) | |||
J662 | 5.10 | 808.1 | 117.2 | 47.8 |
J663 | 5.75 | 790.1 | 114.7 | 41.7 |
J661 | 5.87 | 746.7 | 108.3 | 40.9 |
J665 | 9.22 | 673.6 | 97.7 | 33.3 |
合金 | 组成 | 固溶退火温度(℃) | 成品尺寸时的性能 | ||
屈服强度 | 导电性(%IACS) | ||||
(ksi) | (MPa) | ||||
J676 | 1.86-Co1.45-Ni0.71-Si0.10Mg | 900℃950℃975℃ | 110113115 | 758779793 | 49.647.545.9 |
J686 | 1.92-Co1.50-Ni0.71-Si0.11-Mg0.28-Ag | 900℃950℃975℃ | 103114117 | 710786807 | 53.048.747.8 |
J684 | 2.02-Co1.53-Ni0.72-Si0.10-Mg0.23-Ti | 900℃950℃975℃ | 104115116 | 717793800 | 54.050.347.7 |
J687 | 1.82-Co1.46-Ni0.69-Si0.11-Mg0.14-Zr | 900℃950℃975℃ | 104115119 | 717793821 | 54.049.648.8 |
合金 | 组成 | 固溶退火温度(℃) | 成品尺寸时的性能 | ||
屈服强度 | 导电性(%IACS) | ||||
(ksi) | (MPa) | ||||
J835 | 1.88-Co0.75-Ni0.64-Si | 975℃ | 111 | 765 | 54.5 |
J834 | 1.77-Co0.76-Ni0.60-Si0.20-Ag | 975℃ | 116 | 800 | 53.5 |
J836 | 1.86-Co0.75-Ni0.63-Si0.21-Ag0.10-Mg | 975℃ | 114.5 | 789 | 52.8 |
合金 | 3000小时后残余应力百分数 | ||||
105℃-L | 150℃-L | 150℃-T | 175℃-L | 200℃-L | |
J835 | 89.5 | 80.2 | --- | 72.4 | 66.2 |
J824 | 96.3 | 90.0 | --- | 82.1 | 78.1 |
J834 | --- | 89.1 | --- | --- | --- |
J836 | 97.1 | 91.2 | --- | 83.5 | 79.4 |
J969 | 91.3 | 79.5 | 77.1 | 66.9 | 63.2 |
J970 | 93.1 | 82.9 | 80.4 | 73.9 | 66.4 |
J971 | 93.8 | 85.0 | 83.7 | 78.7 | 68.4 |
J972 | 94.3 | 84.8 | 83.8 | 75.9 | 70.7 |
J973 | 94.1 | 85.8 | 83.3 | 77.0 | 68.1 |
J981 | 93.9 | 85.8 | 83.4 | 76.7 | 68.4 |
J954 | 86.3 | 75.7 | --- | 66.8 | 56.2 |
J982 | 95.6 | 87.2 | 85.0 | 77.1 | 70.6 |
J955 | 88.3 | 76.8 | --- | 64.3 | 57.0 |
J983 | 95.8 | 88.6 | 87.8 | 78.3 | 72.6 |
J956 | 92.9 | 82.7 | --- | 71.0 | 65.1 |
J984 | 97.3 | 90.0 | 88.7 | 76.3 | 72.0 |
合金 | 固溶退火 | 屈服强度 | 极限抗拉强度 | %延伸率 | %IACS | ||
(MPa) | (ksi) | (MPa) | (ksi) | ||||
J395厚0.20mm(0.008英寸)35%冷轧并时效 | 800℃/60秒840℃/60秒880℃/60秒 | 738758758 | 107110110 | 779807807 | 113117117 | 964 | 39.736.836.9 |
J394厚0.20mm(0.008英寸)35%冷轧并时效 | 800℃/60秒840℃/60秒880℃/60秒 | 579586607 | 848588 | 607621648 | 889094 | 666 | 47.645.041.7 |
J401厚0.20mm(0.008英寸)35%冷轧并时效 | 800℃/60秒840℃/60秒880℃/60秒 | 641648676 | 939498 | 676683717 | 9899104 | 887 | 43.041.639.9 |
RN503014厚0.30mm(0.012英寸)25%冷轧并时效 | 950℃/60秒 | 696 | 101 | 738 | 107 | 3 | 35.6 |
J719厚0.30mm(0.012英寸)25%冷轧并时效 | 950℃/60秒 | 634 | 92 | 669 | 97 | 6 | 43.7 |
合金 | 固溶退火 | 屈服强度 | 极限抗拉强度 | %延伸率 | %IACS | ||
(MPa) | (ksi) | (MPa) | (ksi) | ||||
J395(无Co) | 850℃/60秒950℃/60秒 | 696703 | 101102 | 758758 | 110110 | 77 | 46.146.5 |
J394 | 850℃/60秒950℃/60秒 | 641745 | 93108 | 676779 | 98113 | 65 | 50.346.9 |
J401 | 850℃/60秒950℃/60秒 | 683807 | 99117 | 717841 | 104122 | 45 | 49.245.7 |
RN5030140.41mm | 925℃/60秒 | 710765 | 103111 | 745800 | 108116 | 65 | 49.848.8 |
合金 | 固溶退火 | 屈服强度 | 极限抗拉强度 | %延伸率 | %LACS | ||
(MPa) | (ksi) | (MPa) | (ksi) | ||||
(0.012英寸厚) | 950℃/60秒975℃/60秒 | 827 | 120 | 869 | 126 | 6 | 46.1 |
J719(无Ni) | 900℃/60秒950℃/60秒 | 662731 | 96106 | 690758 | 100110 | 65 | 55.452.7 |
合金 | 固溶温度(℃) | %冷轧压下量 | 第二次时效温度(℃) | 性能 | |||||
屈服强度 | 导电率(%LACS) | ||||||||
第一次时效后 | 第二次时效后 | 第一次时效后 | 第二次时效后 | ||||||
(MPa) | (ksi) | (MPa) | (ksi) | ||||||
J3950钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃400℃ | 575.0575.0604.0604.0 | 83.483.487.687.6 | 633.0658.5659.2678.5 | 91.895.595.698.4 | 40.840.840.940.9 | 48.346.250.045.8 |
J3980.52钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃400℃ | 540.6540.6624.7624.7 | 78.478.490.690.6 | 675.7708.1748.9775.0 | 98.0102.7108.6112.4 | 43.843.840.040.0 | 48.747.043.943.4 |
J3940.89钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃450℃ | 446.8446.8544.0544.0 | 64.864.878.978.9 | 625.4655.7699.1708.1 | 90.795.1101.4102.7 | 47.247.243.243.2 | 52.851.148.447.4 |
J6231.06钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃400℃ | 454.4454.4545.4545.4 | 65.965.979.179.1 | 609.5648.1711.6757.1 | 88.494.0103.2109.8 | 46.146.142.542.5 | 50.148.845.145.4 |
J4011.06钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃400℃ | 490.2490.2603.3603.3 | 71.171.187.587.5 | 644.0665.4749.5777.8 | 93.496.5108.7112.8 | 44.144.140.440.4 | 51.047.946.544.6 |
合金 | 固溶温度(℃) | %冷轧压下量 | 第二次时效温度(℃) | 性能 | |||||
屈服强度 | 导电率(%LACS) | ||||||||
第一次时效后 | 第二次时效后 | 第一次时效后 | 第二次时效后 | ||||||
(MPa) | (ksi) | (MPa) | (ksi) | ||||||
J6241.59钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃400℃ | 495.1495.1586.8586.8 | 71.871.885.185.1 | 637.1679.2758.5784.0 | 92.498.5110.0113.7 | 44.244.239.739.7 | 47.446.842.042.0 |
J6202.26钴 | 850℃950℃ | 15%25%15%25% | 450℃400℃450℃400℃ | 523.3523.3647.4647.9 | 75.975.993.993.9 | 656.4697.1787.4824.6 | 95.2101.1114.2119.6 | 45.545.540.440.4 | 48.848.344.343.5 |
工艺1 | 工艺2 | 工艺3 | 工艺4 |
时效 | 冷轧25% | 冷轧50% | 第一次时效 |
时效 | 时效 | 冷轧25% | |
第二次时效 |
工艺 | 屈服强度最大时 | 导电性最高时 | ||||
屈服强度 | 导电性(%IACS) | 屈服强度 | 导电性(%IACS) | |||
(MPa) | (ksi) | (MPa) | (ksi) | |||
1 | 586 | 85 | 45 | 496 | 72 | 49 |
2 | 738 | 107 | 42 | 579 | 84 | 49 |
3 | 758 | 110 | 41 | 545 | 79 | 50 |
4 | 827 | 120 | 45 | 758 | 110 | 50 |
工艺 | 屈服强度 | 导电性(%IACS) | MBR/t | ||
(MPa) | (ksi) | ||||
好路径 | 差路径 | ||||
J910 | 789.5 | 114.5 | 51.8 | ||
J989-A | 650.9 | 94.4 | 45.5 | 2.2 | 3.9 |
J989-B | 810.9 | 117.6 | 51.4 | 2.2 | 8.8 |
第一次时效温度(℃) | 第二次时效温度(℃) | 第二次时效时间(小时) | 成品尺寸时的性能 | |||
屈服强度 | 导电率(%IACS) | Δ%IACS | ||||
(MPa) | (ksi) | |||||
475 | 无 | 无 | 768.1 | 111.4 | 36.8 | --- |
475 | 400 | 3 | 778..4 | 112.9 | 40.7 | 3.9 |
475 | 400 | 6 | 792.2 | 114.9 | 40.9 | 4.1 |
475 | 425 | 6 | 777.8 | 112.8 | 40.7 | 3.9 |
475 | 450 | 3 | 779.8 | 113.1 | 39.8 | 3.0 |
525 | 无 | 无 | 766.7 | 111.2 | 41.2 | --- |
525 | 400 | 3 | 771.6 | 111.9 | 46.9 | 5.7 |
525 | 400 | 6 | 755.0 | 109.5 | 49.4 | 8.2 |
525 | 425 | 6 | 763.3 | 110.7 | 50.1 | 8.9 |
525 | 450 | 3 | 757.1 | 109.8 | 48.2 | 7.0 |
铸锭 | 第二次时效退火 | 屈服强度(MPa)(ksi) | 抗拉强度(MPa)(ksi) | 延伸率(%) | 导电率(%IACS) | 90°MBR/t | |
好路径 | 差路径 | ||||||
J724 | 400℃/3小时 | 656.495.2 | 712.9103.4 | 8 | 47.6 | --- | --- |
J724 | 425℃/6小时 | 655.895.1 | 716.4103.9 | 8 | 52.5 | 1.5 | 0.9 |
J731 | 400℃/3小时 | 666.796.7 | 714.3103.6 | 8 | 52.1 | --- | --- |
J731 | 425℃/6小时 | 655.095.0 | 709.5102.9 | 8 | 55,8 | 1.4 | 1.3 |
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AU2003247661A8 (en) | 2004-01-23 |
KR20080111170A (ko) | 2008-12-22 |
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CN1671877A (zh) | 2005-09-21 |
CN101792872A (zh) | 2010-08-04 |
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WO2004005560A2 (en) | 2004-01-15 |
TWI327601B (en) | 2010-07-21 |
CA2490799A1 (en) | 2004-01-15 |
EP1520054B1 (en) | 2016-10-26 |
CN102816980A (zh) | 2012-12-12 |
MXPA05000148A (es) | 2005-04-11 |
CN101792872B (zh) | 2016-03-16 |
US20040079456A1 (en) | 2004-04-29 |
KR20050061401A (ko) | 2005-06-22 |
CA2490799C (en) | 2012-01-24 |
ES2605354T3 (es) | 2017-03-14 |
US8257515B2 (en) | 2012-09-04 |
JP2005532477A (ja) | 2005-10-27 |
EP1520054A4 (en) | 2007-03-07 |
US8430979B2 (en) | 2013-04-30 |
US20140014239A1 (en) | 2014-01-16 |
TW200419001A (en) | 2004-10-01 |
EP1520054B8 (en) | 2017-07-26 |
CN1323188C (zh) | 2007-06-27 |
JP2011157630A (ja) | 2011-08-18 |
JP2014095150A (ja) | 2014-05-22 |
AU2003247661A1 (en) | 2004-01-23 |
US20060076090A1 (en) | 2006-04-13 |
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