CN104210196A - Preparation method of film capable of resisting blue rays and protecting eyes - Google Patents
Preparation method of film capable of resisting blue rays and protecting eyes Download PDFInfo
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- CN104210196A CN104210196A CN201410456159.4A CN201410456159A CN104210196A CN 104210196 A CN104210196 A CN 104210196A CN 201410456159 A CN201410456159 A CN 201410456159A CN 104210196 A CN104210196 A CN 104210196A
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- coating
- mass parts
- blue light
- antireflection
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Abstract
The invention discloses a preparation method of a film capable of resisting blue rays and protecting eyes. The preparation method comprises the following steps: firstly preparing a base film, compounding a blue ray resisting coating on one surface of the base film and compounding an antireflection anti-scratch coating on the other surface of the base film, wherein the blue ray resisting coating comprises the following components: organosilicon pressure sensitive adhesive, hexamethylphosphoric triamide, butanone, benzoyl peroxide and an organosilicon leveling agent; the antireflection anti-scratch coating comprises the following components: polyurethane acrylate oligomer, dipentaerythritol pentaacrylate, a photoinitiator 184, an organosilicon leveling agent, butanone and silicon oxide water suspension with mass percent of 30%. By virtue of the components of the blue ray resisting coating, the blue ray resisting coating is capable of resisting the blue rays, and haze caused by reduction of the blue rays can not be increased; the antireflection anti-scratch coating is capable of effectively reducing the reflectivity of the protecting film and has the anti-scratch protection function.
Description
Technical field
The present invention relates to a kind of preparation method of anti-blue light film for eye.
Background technology
Nature itself does not have independent white light, after blue light and green glow, yellow light mix, presents white light.Green glow and gold-tinted energy are less, less to eye irritation, and blue light ripple is short, energy is high, in LED, computer bias light artificial light sources, has retained a large amount of blue lights, makes like this artificial light whiter, brighter, some white especially bright light is to people's sensation of blueing always, and blue light ratio that Here it is is too high to be caused.In the visible ray that the various novel artificial light sources such as all kinds of computers, television screen, electricity-saving lamp send, all contain the shortwave blue light of a large amount of irregular frequencies.Wavelength is between 400～500nm.Long term exposure, under blue light, easily causes eye injury, particularly causes macular diseases.Blue light can penetrate crystalline lens and arrive retina, and it is caused to optics infringement, accelerates the oxidation of macular area cell, produces a large amount of free radicals, causes cataract, and macular area is degenerated.
Infringement for fear of blue light to eyes, needs anti-blue light film for eye to protect eyes.Although the product that the production technology of existing anti-blue light film for eye is produced energy anti-blue light, also increases extra mist degree because reduce blue light, and can not reduce the reflectivity of diaphragm.
Summary of the invention
In order to overcome preparation method's the above-mentioned deficiency of prior art anti-blue light film for eye; the invention provides a kind of preparation method of anti-blue light film for eye; the diaphragm that the method makes can not increase extra mist degree because of reducing blue light, and can effectively reduce the reflectivity of diaphragm.
The technical scheme that the present invention solves its technical problem is: a kind of preparation method of anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 20～75 mass parts;
HMPA 0.3～5 mass parts;
Butanone 20～60 mass parts;
Benzoyl peroxide 1～10 mass parts;
Organosilicon levelling agent 0.5～5 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 45 DEG C～75 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 100 DEG C～150 DEG C, place after 10～20min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 10～30 mass parts;
Double pentaerythritol C5 methacrylate 15～40 mass parts;
Light trigger 184 0.5～7 mass parts;
Organosilicon levelling agent 0.05～2 mass parts;
30～70 parts of butanone;
Mass percent is 30% silica aqueous suspension 5～20 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Further, the organosilicon levelling agent in described anti-blue light coating is silicone oil or dimethyl silicone polymer.
Beneficial effect of the present invention is: the component of anti-blue light coating makes the anti-blue light coating can not only anti-blue light, and can not increase extra mist degree because of reducing blue light; The anti-scratch coating of antireflection not only can effectively reduce the reflectivity of diaphragm, and has anti-scratch protective effect.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is described in further detail.
Embodiment mono-
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 50 mass parts;
HMPA 3 mass parts;
Butanone 40 mass parts;
Benzoyl peroxide 5 mass parts;
Silicone oil 2.5 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 60 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 130 DEG C, place after 15min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 20 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 25 mass parts;
Light trigger 184 4 mass parts;
Silicone oil 1 mass parts;
50 parts of butanone;
Mass percent is 30% silica aqueous suspension 15 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Embodiment bis-
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 30 mass parts;
HMPA 0.3 mass parts;
Butanone 50 mass parts;
Benzoyl peroxide 3 mass parts;
Dimethyl silicone polymer 5 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 70 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 120 DEG C, place after 16min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 15 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 30 mass parts;
Light trigger 184 1 mass parts;
Silicone oil 0.08 mass parts;
45 parts of butanone;
Mass percent is 30% silica aqueous suspension 6 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Embodiment tri-
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 40 mass parts;
HMPA 2 mass parts;
Butanone 20 mass parts;
Benzoyl peroxide 7 mass parts;
Silicone oil 0.5 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 45 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 110 DEG C, place after 10min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 12 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 20 mass parts;
Light trigger 184 5 mass parts;
Dimethyl silicone polymer 0.05 mass parts;
35 parts of butanone;
Mass percent is 30% silica aqueous suspension 20 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Embodiment tetra-
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 20 mass parts;
HMPA 0.5 mass parts;
Butanone 60 mass parts;
Benzoyl peroxide 1 mass parts;
Dimethyl silicone polymer 3 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 55 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 140 DEG C, place after 19min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 10 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 15 mass parts;
Light trigger 184 3.5 mass parts;
Dimethyl silicone polymer 1.1 mass parts;
30 parts of butanone;
Mass percent is 30% silica aqueous suspension 5 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Embodiment five
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 75 mass parts;
HMPA 4 mass parts;
Butanone 35 mass parts;
Benzoyl peroxide 10 mass parts;
Silicone oil 1 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 50 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 100 DEG C, place after 17min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 25 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 22 mass parts;
Light trigger 184 0.5 mass parts;
Silicone oil 1.5 mass parts;
40 parts of butanone;
Mass percent is 30% silica aqueous suspension 12 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Embodiment six
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 60 mass parts;
HMPA 5 mass parts;
Butanone 45 mass parts;
Benzoyl peroxide 4 mass parts;
Silicone oil 3.5 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 75 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 125 DEG C, place after 20min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 30 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 40 mass parts;
Light trigger 184 7 mass parts;
Silicone oil 1.7 mass parts;
70 parts of butanone;
Mass percent is 30% silica aqueous suspension 10 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Embodiment seven
A preparation method for anti-blue light film for eye, first prepares basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 70 mass parts;
HMPA 1 mass parts;
Butanone 30 mass parts;
Benzoyl peroxide 8 mass parts;
Dimethyl silicone polymer 4 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 65 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 150 DEG C, place after 12min and take out, on the one side of basement membrane is compound anti-blue light coating;
The preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 28 mass parts that the model that ancient cooking vessel good photochemical Science and Technology Ltd. in Shenzhen produces is DH-408;
Double pentaerythritol C5 methacrylate 35 mass parts;
Light trigger 184 6 mass parts;
Dimethyl silicone polymer 2 mass parts;
60 parts of butanone;
Mass percent is 30% silica aqueous suspension 18 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
Claims (2)
1. a preparation method for anti-blue light film for eye, is characterized in that: first prepare basement membrane, in the compound anti-blue light coating of one side of basement membrane, in the anti-scratch coating of the compound antireflection of another side of basement membrane;
The preparation method of described anti-blue light coating is:
The component of this anti-blue light coating is:
Organic pressure-sensitive gel 20～75 mass parts;
HMPA 0.3～5 mass parts;
Butanone 20～60 mass parts;
Benzoyl peroxide 1～10 mass parts;
Organosilicon levelling agent 0.5～5 mass parts;
Above-mentioned raw material are mixed, stir 20 minutes, ultrasonic wave froth breaking obtains anti-blue light glue for 1 hour again, one side by above-mentioned anti-blue light glue-coating at described basement membrane, then inserted temperature and be in the baking oven of 45 DEG C～75 DEG C, until butanone all volatilizees, then to be inserted temperature be in the baking oven of 100 DEG C～150 DEG C, place after 10～20min and take out, on the one side of basement membrane is compound anti-blue light coating;
?the preparation method of the anti-scratch coating of antireflection is:
The component of the anti-scratch coating of this antireflection is:
Polyurethane acrylic ester oligomer 10～30 mass parts;
Double pentaerythritol C5 methacrylate 15～40 mass parts;
Light trigger 184 0.5～7 mass parts;
Organosilicon levelling agent 0.05～2 mass parts;
30～70 parts of butanone;
Mass percent is 30% silica aqueous suspension 5～20 mass parts;
Above-mentioned raw materials is mixed, stir 20min, more ultrasonic wave froth breaking obtains the anti-scratch masking liquid of antireflection for 1 hour, anti-scratch this antireflection masking liquid is coated on to the another side of described basement membrane, 90 DEG C to dry 1.5 minutes of the coating forming after, with 200mj/cm
2light quantity irradiate dry coating be cured and form antireflection anti-scratch coating by ultraviolet ray.
2. the preparation method of anti-blue light film for eye as claimed in claim 1, is characterized in that: the organosilicon levelling agent in described anti-blue light coating is silicone oil or dimethyl silicone polymer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410456159.4A CN104210196B (en) | 2014-09-10 | 2014-09-10 | A kind of preparation method of anti-blue light film for eye |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410456159.4A CN104210196B (en) | 2014-09-10 | 2014-09-10 | A kind of preparation method of anti-blue light film for eye |
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| CN104210196A true CN104210196A (en) | 2014-12-17 |
| CN104210196B CN104210196B (en) | 2016-04-20 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104730728A (en) * | 2015-03-23 | 2015-06-24 | 温州朗目光学有限公司 | Novel driving lens and manufacture method thereof |
| CN105860883A (en) * | 2014-12-31 | 2016-08-17 | 斯迪克新型材料（江苏）有限公司 | Protection film with resistance to blue light |
| CN106010348A (en) * | 2014-12-31 | 2016-10-12 | 苏州斯迪克新材料科技股份有限公司 | OCA (optically clear adhesive) optical protecting tape for electronic products |
| CN106966606A (en) * | 2017-03-10 | 2017-07-21 | 江苏好的节能光电科技有限公司 | A kind of preparation method of solar energy glass surface anti-reflection film |
| CN109553790A (en) * | 2017-09-25 | 2019-04-02 | 安徽屹珹新材料科技有限公司 | A kind of anti-blue light film and preparation method thereof |
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| CN103935097A (en) * | 2014-04-10 | 2014-07-23 | 宁波惠之星新材料科技有限公司 | Blue-proof hardening film |
| CN103991255A (en) * | 2014-05-22 | 2014-08-20 | 太湖金张科技股份有限公司 | Blue-light-prevention screen protective membrane and preparation method thereof |
| JP2014162033A (en) * | 2013-02-22 | 2014-09-08 | Waseda Univ | Transparent conductive body and production method of transparent conductive body |
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| US7851065B2 (en) * | 2008-05-27 | 2010-12-14 | Innovation & Infinity Global Corp. | Extreme low resistivity light attenuation anti-reflection coating structure in order to increase transmittance of blue light and method for manufacturing the same |
| JP2014162033A (en) * | 2013-02-22 | 2014-09-08 | Waseda Univ | Transparent conductive body and production method of transparent conductive body |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105860883A (en) * | 2014-12-31 | 2016-08-17 | 斯迪克新型材料（江苏）有限公司 | Protection film with resistance to blue light |
| CN106010348A (en) * | 2014-12-31 | 2016-10-12 | 苏州斯迪克新材料科技股份有限公司 | OCA (optically clear adhesive) optical protecting tape for electronic products |
| CN104730728A (en) * | 2015-03-23 | 2015-06-24 | 温州朗目光学有限公司 | Novel driving lens and manufacture method thereof |
| CN104730728B (en) * | 2015-03-23 | 2018-02-06 | 温州朗目光学有限公司 | A kind of manufacture method of driving glasses slice |
| CN106966606A (en) * | 2017-03-10 | 2017-07-21 | 江苏好的节能光电科技有限公司 | A kind of preparation method of solar energy glass surface anti-reflection film |
| CN109553790A (en) * | 2017-09-25 | 2019-04-02 | 安徽屹珹新材料科技有限公司 | A kind of anti-blue light film and preparation method thereof |
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|---|---|
| CN104210196B (en) | 2016-04-20 |
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