CN1959199B - Saturated water vapor generator - Google Patents

Saturated water vapor generator Download PDF

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Publication number
CN1959199B
CN1959199B CN2006101471445A CN200610147144A CN1959199B CN 1959199 B CN1959199 B CN 1959199B CN 2006101471445 A CN2006101471445 A CN 2006101471445A CN 200610147144 A CN200610147144 A CN 200610147144A CN 1959199 B CN1959199 B CN 1959199B
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CN
China
Prior art keywords
water
liquid separation
layer
vapor
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2006101471445A
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Chinese (zh)
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CN1959199A (en
Inventor
谢传欣
王慧欣
黄飞
金满平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
China Petrochemical Corp
Sinopec Qingdao Safety Engineering Institute
Original Assignee
China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
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Publication date
Application filed by China Petroleum and Chemical Corp, Sinopec Qingdao Safety Engineering Institute filed Critical China Petroleum and Chemical Corp
Priority to CN2006101471445A priority Critical patent/CN1959199B/en
Publication of CN1959199A publication Critical patent/CN1959199A/en
Application granted granted Critical
Publication of CN1959199B publication Critical patent/CN1959199B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

A saturated water steam generator used on test device is prepared as forming constant temperature water bath sealed container by electric heater, temperature controller, water supply and water drainage pipeline, setting gas-liquid separation layer at proper position in water layer top cavity of said container; submerging air inlet pipe end at water layer bottom by passing through wall of said container, setting one end of air outlet pipe at proper position in gas-liquid separation layer top cavity and connecting another end of air outlet pipe to sample reacting chamber of test device by passing it through wall of said container.

Description

Saturated water vapor generator
Technical field
The present invention relates to the improvement that there is the application apparatus of working environment in Simulated Water steam, specifically is a kind of saturated water vapor generator, and it belongs to the measuring instrument technical field of material heat endurance.
Background technology
Calorimetry instrument in accelerated speed of the prior art (abbreviates as: ARC) become one of means of testing commonly used of estimating the material heat endurance in the world, and progressively developed to being called the standard method of test direction.Yet this instrument only can be with closed system. be research object.And often be to be research object in industrial practical application with the open system.In order to expand the scope of application of ARC, make that the gas system of ARC is a research object with the open system, make it use the operating environment that more is intended for industrialized unit; This just needs to increase open gas system, joins in the ARC system.The steam generator of prior art generally is a boiler formula high temperature and high pressure steam system.Yet the working environment that Simulated Water steam exists in the ARC system does not need high temperature and high pressure steam.Technological difficulties to be solved by this invention are: satisfy the demand to the steady supply of the cryogenic gas of adjustable certain flow, also will satisfy simultaneously carrying the demand of saturated vapor secretly, also will satisfy the problem of effective solution vapor-liquid separation again.According to the situation of literature search and market survey, still there is not the experimental rig that similarly supplies the working environment that Simulated Water steam exists in the ARC system both at home and abroad.
Summary of the invention
The objective of the invention is to provide a kind of saturated water vapor generator for the open gas system of the working environment of Simulated Water steam existence in the ARC system.This generator is for satisfying ARC the demand of carrying the saturated vapor air secretly to be designed.The requirement of the steady supply of this designed generator also will satisfy ARC above-mentioned cryogenic gas to adjustable certain flow, thus satisfied the security evaluation of the operating environment in the simulation petrochemical equipment.
The objective of the invention is to realize that by following technical scheme developed a kind of saturated water vapor generator, it comprises: have electric heater, temperature controller, the water bath with thermostatic control airtight container of upper and lower water pipeline.Appropriate position in this container water layer upper cavity is provided with the vapor-liquid separation layer, the gas feed pipe end that passes this chamber wall immerses in the water layer bottom, gas outlet tube one end is arranged on the appropriate position in the vapor-liquid separation layer upper cavity, and the other end of this gas outlet tube passes in the example reaction chamber that this chamber wall is switched to system.
Described vapor-liquid separation layer, it is the glass fiber cotton layer, or be perlite matter layer, or is the asbestine layer: the thickness of this vapor-liquid separation layer is at 1-5mm.
Described water bath with thermostatic control airtight container, the temperature controlling range of its temperature controller customization is at 5-100 ℃.
Described gas, itself or be the air of certain flow, or be the nitrogen of certain flow; This gas flow scope is below the 200mL/min.
The invention has the advantages that: owing to developed a kind of saturated water vapor generator, it comprises: have electric heater, temperature controller, the water bath with thermostatic control airtight container of upper and lower water pipeline.Appropriate position in this container water layer upper cavity is provided with the vapor-liquid separation layer, the gas feed pipe end that passes this chamber wall immerses in the water layer bottom, gas outlet tube one end is arranged on the appropriate position in the vapor-liquid separation layer upper cavity, and the other end of this gas outlet tube passes in the example reaction chamber that this chamber wall is switched to system.Because electrically heated rod in the water bath with thermostatic control airtight container and temperature controller can be controlled in temperature 5-100 ℃ of water bath with thermostatic control, to obtain the temperature of the desired water vapour of experiment.When bottom that the air (or nitrogen) of certain flow is continued to feed water bath with thermostatic control via stainless steel tube, sufficient the contact arranged with the water of specified temp, increase along with the internal pressure of water bath with thermostatic control, the air of carrying water vapour (containing fine drop) secretly via glass silk flosssilk wadding layer (or for perlite matter layer, or be the asbestine layer) time, thereby tiny drop is adsorbed the effect of having played vapor-liquid separation by vapor-liquid separation layers such as glass silk flosssilk waddings, and the air (or nitrogen) of then carrying water vapour secretly leaves water bath with thermostatic control via gas outlet tube.Expand the scope of application of ARC based on the saturated water vapor generator of ARC exploitation, can simulate potential runaway reaction and quantize heat, the pressure hazard of some chemicals and mixture, promptly be used to study the thermostability and the assessment of hot harmfulness of material.
Description of drawings
Fig. 1 is the sectional structure schematic diagram of saturated water vapor generator.
The specific embodiment
Embodiments of the invention further specify as follows in conjunction with experiment and accompanying drawing thereof:
Referring to Fig. 1, the saturated water vapor generator of making, it comprises: have electric heater 4, temperature controller (not drawing among the figure), the water bath with thermostatic control airtight container 5 of upper and lower water pipeline 6,7.Appropriate position in this container water layer upper cavity is provided with the vapor-liquid separation layer 1 of glass silk floss, gas inlet tube 3 ends that pass this chamber wall immerse in the water layer bottom, gas outlet tube 2 one ends are arranged on the appropriate position in vapor-liquid separation layer 1 upper cavity, and the other end of this gas outlet tube 2 passes in the example reaction chamber (not drawing among the figure) that these container 5 walls are switched to system.
Described vapor-liquid separation layer 1, it is the glass fiber cotton layer, or is the asbestine layer; The thickness of this vapor-liquid separation layer is at 2mm.
Described water bath with thermostatic control airtight container 5, the temperature controlling range of its temperature controller customization is at 5-100 ℃.
Described gas, itself or be the air of certain flow, or be the nitrogen of certain flow; This gas flow scope is 200,150,100 or 60mL/min.
After saturated water vapor generator of the present invention completes, utilize ARC to carry out the research of spontaneous burning mechanism of FeS in sulfur, device ruuning situation is stable in the experiment, and temperature control is good, and the vapor-liquid separation effect is obvious, has reached experiment effect preferably.
Those of ordinary skill in the art can understand, and in protection scope of the present invention, makes amendment for the foregoing description, and it all is possible adding and replacing, and it does not all exceed protection scope of the present invention.

Claims (4)

1. saturated water vapor generator, it comprises: have electric heater, temperature controller, the water bath with thermostatic control airtight container of upper and lower water pipeline, it is characterized in that: the appropriate position in this container water layer upper cavity is provided with the vapor-liquid separation layer, the gas feed pipe end that passes this chamber wall immerses in the water layer bottom, and gas outlet tube one end is arranged on the appropriate position in the vapor-liquid separation layer upper cavity, and the other end of this gas outlet tube passes in the example reaction chamber that this chamber wall is switched to system.
2. according to the described saturated water vapor generator of claim 1, it is characterized in that: described vapor-liquid separation layer, it is the glass fiber cotton layer, or be perlite matter layer, or is the asbestine layer; The thickness of this vapor-liquid separation layer is at 1-5mm.
3. according to the described saturated water vapor generator of claim 1, it is characterized in that: described water bath with thermostatic control airtight container, the temperature controlling range of its temperature controller customization is at 5-100 ℃.
4. according to the described saturated water vapor generator of claim 1, it is characterized in that: described gas, itself or be the air of certain flow, or be the nitrogen of certain flow; This gas flow scope is below 200mL/min.
CN2006101471445A 2006-08-23 2006-11-04 Saturated water vapor generator Expired - Fee Related CN1959199B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2006101471445A CN1959199B (en) 2006-08-23 2006-11-04 Saturated water vapor generator

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN200610068570 2006-08-23
CN200610068570.X 2006-08-23
CN2006101471445A CN1959199B (en) 2006-08-23 2006-11-04 Saturated water vapor generator

Publications (2)

Publication Number Publication Date
CN1959199A CN1959199A (en) 2007-05-09
CN1959199B true CN1959199B (en) 2010-05-26

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CN2006101471445A Expired - Fee Related CN1959199B (en) 2006-08-23 2006-11-04 Saturated water vapor generator

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Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102213407B (en) * 2011-04-15 2013-04-03 北京科技大学 Device for generating saturated steam with controllable steam pressure

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3952181A (en) * 1974-08-05 1976-04-20 Reed Hugh T Humidifier
EP0263049A2 (en) * 1986-06-23 1988-04-06 S.O.R. Internacional, S.A. Improvements made in a device to achieve water ebulliency
CN2212708Y (en) * 1995-04-19 1995-11-15 徐国汉 Ultra-mini steam generator
CN2223134Y (en) * 1995-05-16 1996-03-27 阎冰声 Gas-liquid separator
CN1673614A (en) * 2005-04-17 2005-09-28 曲景春 Simple electric heating high pure steam generator

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3952181A (en) * 1974-08-05 1976-04-20 Reed Hugh T Humidifier
EP0263049A2 (en) * 1986-06-23 1988-04-06 S.O.R. Internacional, S.A. Improvements made in a device to achieve water ebulliency
CN2212708Y (en) * 1995-04-19 1995-11-15 徐国汉 Ultra-mini steam generator
CN2223134Y (en) * 1995-05-16 1996-03-27 阎冰声 Gas-liquid separator
CN1673614A (en) * 2005-04-17 2005-09-28 曲景春 Simple electric heating high pure steam generator

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