DE60227508D1 - Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung von fluorpolymeren - Google Patents
Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung von fluorpolymerenInfo
- Publication number
- DE60227508D1 DE60227508D1 DE60227508T DE60227508T DE60227508D1 DE 60227508 D1 DE60227508 D1 DE 60227508D1 DE 60227508 T DE60227508 T DE 60227508T DE 60227508 T DE60227508 T DE 60227508T DE 60227508 D1 DE60227508 D1 DE 60227508D1
- Authority
- DE
- Germany
- Prior art keywords
- chain transfer
- emulsify
- fluoropolymers
- production
- emulsion polymerization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F214/18—Monomers containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/18—Monomers containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/18—Monomers containing fluorine
- C08F14/22—Vinylidene fluoride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/18—Monomers containing fluorine
- C08F14/26—Tetrafluoroethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/22—Emulsion polymerisation
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US28817201P | 2001-05-02 | 2001-05-02 | |
| PCT/US2002/013691 WO2002088207A1 (en) | 2001-05-02 | 2002-04-30 | Emulsifier free aqueous emulsion polymerization process for making fluoropolymers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE60227508D1 true DE60227508D1 (de) | 2008-08-21 |
Family
ID=23106047
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60234513T Expired - Lifetime DE60234513D1 (de) | 2001-05-02 | 2002-04-30 | Emulgatorfreies verfahren zur herstellung von flourpolymeren durch emulsionspolymerisation in wasser |
| DE60227508T Expired - Lifetime DE60227508D1 (de) | 2001-05-02 | 2002-04-30 | Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung von fluorpolymeren |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60234513T Expired - Lifetime DE60234513D1 (de) | 2001-05-02 | 2002-04-30 | Emulgatorfreies verfahren zur herstellung von flourpolymeren durch emulsionspolymerisation in wasser |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US6693152B2 (de) |
| EP (2) | EP1383811B1 (de) |
| JP (2) | JP2004525239A (de) |
| CN (3) | CN1256355C (de) |
| AT (2) | ATE400592T1 (de) |
| CA (2) | CA2446016A1 (de) |
| DE (2) | DE60234513D1 (de) |
| WO (2) | WO2002088206A2 (de) |
Families Citing this family (86)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2446016A1 (en) * | 2001-05-02 | 2002-11-07 | 3M Innovative Properties Company | Emulsifier free aqueous emulsion polymerization process for making fluoropolymers |
| WO2002088203A2 (en) * | 2001-05-02 | 2002-11-07 | 3M Innovative Properties Company | Aqueous emulsion polymerization in the presence of ethers as chain transfer agents to produce fluoropolymers |
| US7279522B2 (en) | 2001-09-05 | 2007-10-09 | 3M Innovative Properties Company | Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant |
| JP2006504844A (ja) * | 2002-10-31 | 2006-02-09 | スリーエム イノベイティブ プロパティズ カンパニー | フッ化オレフィンと炭化水素オレフィンとのコポリマーを製造するための、乳化剤非含有水性乳化重合 |
| US6734264B1 (en) * | 2002-12-16 | 2004-05-11 | Atofina Chemicals, Inc. | Chain transfer agent |
| EP1586592B1 (de) * | 2002-12-25 | 2010-04-21 | Daikin Industries, Ltd. | Fluorpolymer und zusammensetzung |
| JP2005036189A (ja) * | 2003-07-14 | 2005-02-10 | Rohm & Haas Co | 水性ポリマー分散体の調製のための水性重合方法 |
| EP1668065A4 (de) * | 2003-09-25 | 2007-09-12 | Laurel Products Llc | Hochstabile polytetrafluorethylendispersionen und herstellungsverfahren dafür |
| ATE502062T1 (de) | 2003-10-24 | 2011-04-15 | 3M Innovative Properties Co | Wässrige dispersionen von polytetrafluorethylenteilchen |
| ATE529451T1 (de) * | 2003-11-17 | 2011-11-15 | 3M Innovative Properties Co | Wässrige ptfe-dispersionen mit einem niedrigen gehalt an fluorierten emulgatoren |
| PL1570917T3 (pl) * | 2004-03-01 | 2009-10-30 | 3M Innovative Properties Co | Sposób powlekania substratu dyspersją fluoropolimeru |
| US20100028339A1 (en) * | 2004-03-29 | 2010-02-04 | Cheng Jin Q | Compositions including triciribine and trastuzumab and methods of use thereof |
| ITMI20041253A1 (it) * | 2004-06-22 | 2004-09-22 | Solvay Solexis Spa | Gel di fluoroelastomeri |
| ITMI20041251A1 (it) * | 2004-06-22 | 2004-09-22 | Solvay Solexis Spa | Gel di perfluoroelastomeri |
| US8080621B2 (en) * | 2005-06-10 | 2011-12-20 | Arkema Inc. | Aqueous process for making fluoropolymers |
| US8338518B2 (en) * | 2005-06-10 | 2012-12-25 | Arkema Inc. | Aqueous process for making a stable fluoropolymer dispersion |
| US8765890B2 (en) | 2005-06-10 | 2014-07-01 | Arkema Inc. | Aqueous process for making fluoropolymers |
| US20060281845A1 (en) * | 2005-06-10 | 2006-12-14 | Ramin Amin-Sanayei | Aqueous process for making fluoropolymers |
| GB2427170A (en) * | 2005-06-17 | 2006-12-20 | 3M Innovative Properties Co | Fluoropolymer film having glass microspheres |
| GB0514387D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
| GB0514398D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant |
| GB0525978D0 (en) * | 2005-12-21 | 2006-02-01 | 3M Innovative Properties Co | Fluorinated Surfactants For Making Fluoropolymers |
| US20070015937A1 (en) * | 2005-07-15 | 2007-01-18 | 3M Innovative Properties Company | Process for recovery of fluorinated carboxylic acid surfactants from exhaust gas |
| US20080015304A1 (en) * | 2006-07-13 | 2008-01-17 | Klaus Hintzer | Aqueous emulsion polymerization process for producing fluoropolymers |
| GB0523853D0 (en) | 2005-11-24 | 2006-01-04 | 3M Innovative Properties Co | Fluorinated surfactants for use in making a fluoropolymer |
| GB2430437A (en) * | 2005-09-27 | 2007-03-28 | 3M Innovative Properties Co | Method of making a fluoropolymer |
| US7649067B2 (en) * | 2005-10-19 | 2010-01-19 | Wacker Polymers, L.P. | Process of making a vinyl ester based polymer latex composition |
| US20070100062A1 (en) * | 2005-10-28 | 2007-05-03 | Lyons Donald F | Process for the manufacture of fluoroelastomers having bromine or lodine atom cure sites |
| GB2432836A (en) * | 2005-12-01 | 2007-06-06 | 3M Innovative Properties Co | Fluorinated surfactant |
| US20070135577A1 (en) * | 2005-12-09 | 2007-06-14 | Shefelbine Terri A | Intermediate elastomer compositions |
| US7728087B2 (en) | 2005-12-23 | 2010-06-01 | 3M Innovative Properties Company | Fluoropolymer dispersion and method for making the same |
| US20070276103A1 (en) * | 2006-05-25 | 2007-11-29 | 3M Innovative Properties Company | Fluorinated Surfactants |
| US7754795B2 (en) * | 2006-05-25 | 2010-07-13 | 3M Innovative Properties Company | Coating composition |
| US8119750B2 (en) | 2006-07-13 | 2012-02-21 | 3M Innovative Properties Company | Explosion taming surfactants for the production of perfluoropolymers |
| WO2008024601A1 (en) * | 2006-08-24 | 2008-02-28 | 3M Innovative Properties Company | Solvent slurry process for producing high solids fluoropolymers |
| US7678859B2 (en) | 2006-09-14 | 2010-03-16 | 3M Innovative Properties Company | Preparation and stabilization of fluoropolymer dispersions |
| BRPI0807109A2 (pt) * | 2007-02-16 | 2014-05-06 | 3M Innovative Properties Co | Sistema e processo para a remoção de fluoroquiímicos da água |
| US20080264864A1 (en) * | 2007-04-27 | 2008-10-30 | 3M Innovative Properties Company | PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT |
| CN101050250B (zh) * | 2007-05-18 | 2010-05-19 | 上海三爱富新材料股份有限公司 | 稳定的水性含氟聚合物分散乳液及其制备方法 |
| US7960480B2 (en) * | 2007-05-21 | 2011-06-14 | Dupont Performance Elastomers L.L.C. | Process for coagulating fluoroelastomers |
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| JP2008297529A (ja) * | 2007-06-04 | 2008-12-11 | Daikin Ind Ltd | ビニリデンフルオライド系重合体の製造方法 |
| JP5453250B2 (ja) * | 2007-06-06 | 2014-03-26 | スリーエム イノベイティブ プロパティズ カンパニー | フッ素化エーテル組成物及びフッ素化エーテル組成物の使用方法 |
| JP5532532B2 (ja) * | 2007-06-25 | 2014-06-25 | ダイキン工業株式会社 | 低分子量ポリテトラフルオロエチレン水性分散液及びその製造方法 |
| KR101595137B1 (ko) * | 2008-02-29 | 2016-02-17 | 쓰리엠 이노베이티브 프로퍼티즈 캄파니 | 낮은 카르보닐 말단기 비를 갖는 퍼플루오로엘라스토머 |
| US20090281261A1 (en) * | 2008-05-09 | 2009-11-12 | E. I. Du Pont De Nemours And Company | Abatement of Fluoroether Carboxylic Acids or Salts Employed in Fluoropolymer Resin Manufacture |
| BRPI0915955A2 (pt) * | 2008-07-18 | 2019-02-26 | 3M Innovative Proferties Company | compostos fluorados de éter e métodos para uso dos mesmos |
| GB0814955D0 (en) | 2008-08-18 | 2008-09-24 | 3M Innovative Properties Co | Azide-containing fluoropolymers and their preparation |
| JP2012509937A (ja) * | 2008-11-25 | 2012-04-26 | スリーエム イノベイティブ プロパティズ カンパニー | フッ素化エーテルウレタン及びその使用方法 |
| WO2010080473A1 (en) | 2008-12-18 | 2010-07-15 | 3M Innovative Properties Company | Method of contacting hydrocarbon-bearing formations with fluorinated ether compositions |
| EP2415788B1 (de) * | 2009-03-31 | 2014-04-30 | Daikin Industries, Ltd. | Polytetrafluorethylenpulver mit geringem molekulargewicht und zubereitungsverfahren dfür |
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| JP5968310B2 (ja) * | 2010-06-24 | 2016-08-10 | スリーエム イノベイティブ プロパティズ カンパニー | 有機乳化剤を含まない重合性組成物、並びにそのポリマー及び製造方法 |
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| CN103210003B (zh) | 2010-11-09 | 2016-09-07 | 纳幕尔杜邦公司 | 减弱含烃表面活性剂在含氟单体含水分散体聚合反应中的调聚性能 |
| US9255164B2 (en) | 2010-11-09 | 2016-02-09 | The Chemours Company Fc, Llc | Aqueous polymerization of perfluoromonomer using hydrocarbon surfactant |
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| GB201021790D0 (en) * | 2010-12-23 | 2011-02-02 | 3M Innovative Properties Co | Fluoropolymer compostions and purification methods thereof |
| JP2014508210A (ja) | 2011-03-16 | 2014-04-03 | アーケマ・インコーポレイテッド | ２，３，３，３−テトラフルオロプロペン含有フルオロポリマーの合成 |
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| EP2928933B1 (de) | 2012-12-04 | 2019-12-25 | 3M Innovative Properties Company | Hoch fluorierte polymere |
| CN104211840B (zh) * | 2013-06-04 | 2016-02-17 | 山东东岳高分子材料有限公司 | 一种含氟聚合反应的低毒性乳化剂及含氟聚合物的制备方法 |
| CN106414510B (zh) | 2013-11-26 | 2018-11-30 | 得凯莫斯公司弗罗里达有限公司 | 采用聚环氧烷在含氟单体的水相聚合中成核 |
| CN103694396B (zh) * | 2013-12-27 | 2016-03-02 | 中昊晨光化工研究院有限公司 | 一种高分子含氟橡胶及其制备方法和应用 |
| CN103724511B (zh) * | 2013-12-30 | 2016-06-15 | 山东华夏神舟新材料有限公司 | 一种油封用氟橡胶的制备方法 |
| US10087322B2 (en) | 2014-08-22 | 2018-10-02 | 3M Innovative Properties Company | Fluorothermoplastic polymer |
| EP3183299B1 (de) | 2014-08-22 | 2020-11-25 | 3M Innovative Properties Company | Fluorthermoplastische polymerzusammensetzungen |
| KR101520343B1 (ko) * | 2014-10-16 | 2015-05-19 | 주식회사 한나노텍 | 가공조제 및 가공조제용 마스터배치 |
| CN105754027B (zh) * | 2014-12-15 | 2019-03-22 | 浙江蓝天环保高科技股份有限公司 | 一种偏氟乙烯聚合物、其制备方法及应用 |
| TWI627192B (zh) * | 2015-03-13 | 2018-06-21 | 村田製作所股份有限公司 | Atomic layer deposition inhibiting material |
| US11643484B2 (en) * | 2015-03-16 | 2023-05-09 | Arkema Inc. | Modified fluoropolymers |
| EP3322742A1 (de) * | 2015-07-13 | 2018-05-23 | 3M Innovative Properties Company | Fluorierte blockcopolymere |
| EP3386890B1 (de) * | 2015-12-10 | 2022-04-27 | ContiTech Transportbandsysteme GmbH | Wärmebeständiges förderband |
| CN106046206B (zh) * | 2016-07-26 | 2017-09-22 | 金华永和氟化工有限公司 | 一种制备可熔性含氟聚合物的水乳液聚合方法 |
| WO2018031604A1 (en) | 2016-08-10 | 2018-02-15 | 3M Innovative Properties Company | A fluorinated pressure sensitive adhesives and articles thereof |
| CN110494516B (zh) * | 2017-04-11 | 2022-11-04 | 索尔维特殊聚合物意大利有限公司 | 用于制造氟聚合物的方法 |
| FR3071500B1 (fr) * | 2017-09-27 | 2020-05-15 | Arkema France | Synthese de latex de poly(fluorure de vinylidene) sans tensioactif par polymerisation en emulsion raft |
| US20210070897A1 (en) * | 2018-03-16 | 2021-03-11 | Arkema Inc. | High solids, surfactant-free fluoropolymer |
| WO2020109926A1 (en) | 2018-11-29 | 2020-06-04 | 3M Innovative Properties Company | Composite film, method of making the same, and article including the same |
| CN110078855B (zh) * | 2019-04-22 | 2020-07-14 | 中昊晨光化工研究院有限公司 | 一种含氟聚合物及其制备方法 |
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| WO2023099974A1 (en) | 2021-12-01 | 2023-06-08 | 3M Innovative Properties Company | Semi-fluorinated thermoplastic copolymers and passive cooling articles including the same |
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-
2002
- 2002-04-30 CA CA002446016A patent/CA2446016A1/en not_active Abandoned
- 2002-04-30 US US10/136,876 patent/US6693152B2/en not_active Expired - Lifetime
- 2002-04-30 US US10/474,523 patent/US7074862B2/en not_active Expired - Lifetime
- 2002-04-30 CA CA002445998A patent/CA2445998A1/en not_active Abandoned
- 2002-04-30 AT AT02766881T patent/ATE400592T1/de not_active IP Right Cessation
- 2002-04-30 JP JP2002585503A patent/JP2004525239A/ja active Pending
- 2002-04-30 AT AT02725867T patent/ATE449799T1/de not_active IP Right Cessation
- 2002-04-30 EP EP02725867A patent/EP1383811B1/de not_active Expired - Lifetime
- 2002-04-30 CN CNB02809199XA patent/CN1256355C/zh not_active Expired - Fee Related
- 2002-04-30 DE DE60234513T patent/DE60234513D1/de not_active Expired - Lifetime
- 2002-04-30 WO PCT/US2002/013641 patent/WO2002088206A2/en active Application Filing
- 2002-04-30 CN CNB028091248A patent/CN1223619C/zh not_active Expired - Fee Related
- 2002-04-30 DE DE60227508T patent/DE60227508D1/de not_active Expired - Lifetime
- 2002-04-30 CN CNB2005100545432A patent/CN1290880C/zh not_active Expired - Fee Related
- 2002-04-30 JP JP2002585504A patent/JP2004528451A/ja active Pending
- 2002-04-30 WO PCT/US2002/013691 patent/WO2002088207A1/en active Application Filing
- 2002-04-30 EP EP02766881A patent/EP1392744B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| US20040132939A1 (en) | 2004-07-08 |
| WO2002088206A3 (en) | 2003-01-03 |
| JP2004525239A (ja) | 2004-08-19 |
| CN1505645A (zh) | 2004-06-16 |
| US7074862B2 (en) | 2006-07-11 |
| CA2445998A1 (en) | 2002-11-07 |
| US6693152B2 (en) | 2004-02-17 |
| CN1256355C (zh) | 2006-05-17 |
| WO2002088207A1 (en) | 2002-11-07 |
| CA2446016A1 (en) | 2002-11-07 |
| EP1392744B1 (de) | 2008-07-09 |
| WO2002088206A2 (en) | 2002-11-07 |
| ATE400592T1 (de) | 2008-07-15 |
| JP2004528451A (ja) | 2004-09-16 |
| CN1660915A (zh) | 2005-08-31 |
| EP1392744A1 (de) | 2004-03-03 |
| US20020198334A1 (en) | 2002-12-26 |
| CN1505644A (zh) | 2004-06-16 |
| DE60234513D1 (de) | 2010-01-07 |
| ATE449799T1 (de) | 2009-12-15 |
| EP1383811B1 (de) | 2009-11-25 |
| EP1383811A2 (de) | 2004-01-28 |
| CN1290880C (zh) | 2006-12-20 |
| CN1223619C (zh) | 2005-10-19 |
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