DE69731728D1 - Mit seltenen erden aktiviertes borat und sein vorläufer, ihr herstellungsverfahren und die boratverwendung als leuchtstoff - Google Patents

Mit seltenen erden aktiviertes borat und sein vorläufer, ihr herstellungsverfahren und die boratverwendung als leuchtstoff

Info

Publication number: DE69731728D1
Authority: DE; Germany
Prior art keywords: borate; precursor; fluorescent; rare earth; production process
Prior art date: 1996-01-17
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

DE69731728T

Other languages

English (en)

Other versions

DE69731728T2 (de

Inventor

Denis Huguenin

Pierre Macaudiere

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Rhodia Chimie SAS

Original Assignee

Rhodia Chimie SAS

Rhone Poulenc Chimie SA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1996-01-17

Filing date

1997-01-17

Publication date

2004-12-30

1997-01-17 Application filed by Rhodia Chimie SAS, Rhone Poulenc Chimie SA filed Critical Rhodia Chimie SAS

2004-12-30 Publication of DE69731728D1 publication Critical patent/DE69731728D1/de

2005-03-31 Application granted granted Critical

2005-03-31 Publication of DE69731728T2 publication Critical patent/DE69731728T2/de

2017-01-18 Anticipated expiration legal-status Critical

Status Expired - Lifetime legal-status Critical Current

Links

239000002243 precursor Substances 0.000 title abstract 5
BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 title abstract 3
238000004519 manufacturing process Methods 0.000 title 1
229910052761 rare earth metal Inorganic materials 0.000 abstract 3
-1 rare-earth borate Chemical class 0.000 abstract 3
238000000034 method Methods 0.000 abstract 2
238000002360 preparation method Methods 0.000 abstract 2
239000007864 aqueous solution Substances 0.000 abstract 1
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract 1
239000004327 boric acid Substances 0.000 abstract 1
150000001642 boronic acid derivatives Chemical class 0.000 abstract 1
238000001354 calcination Methods 0.000 abstract 1
NKCVNYJQLIWBHK-UHFFFAOYSA-N carbonodiperoxoic acid Chemical compound OOC(=O)OO NKCVNYJQLIWBHK-UHFFFAOYSA-N 0.000 abstract 1
239000006185 dispersion Substances 0.000 abstract 1
239000012429 reaction media Substances 0.000 abstract 1
239000012798 spherical particle Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7712—Borates
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
- C01B35/10—Compounds containing boron and oxygen
- C01B35/12—Borates
- C01B35/127—Borates of heavy metals
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
- C01B35/10—Compounds containing boron and oxygen
- C01B35/12—Borates
- C01B35/128—Borates containing plural metal or metal and ammonium
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7728—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing europium
- C09K11/774—Borates
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7766—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
- C09K11/778—Borates
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7783—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals one of which being europium
- C09K11/7797—Borates
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J11/00—Gas-filled discharge tubes with alternating current induction of the discharge, e.g. alternating current plasma display panels [AC-PDP]; Gas-filled discharge tubes without any main electrode inside the vessel; Gas-filled discharge tubes with at least one main electrode outside the vessel
- H01J11/20—Constructional details
- H01J11/34—Vessels, containers or parts thereof, e.g. substrates
- H01J11/42—Fluorescent layers
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L33/00—Semiconductor devices with at least one potential-jump barrier or surface barrier specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
- H01L33/48—Semiconductor devices with at least one potential-jump barrier or surface barrier specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof characterised by the semiconductor body packages
- H01L33/50—Wavelength conversion elements
- H01L33/501—Wavelength conversion elements characterised by the materials, e.g. binder
- H01L33/502—Wavelength conversion materials
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2211/00—Plasma display panels with alternate current induction of the discharge, e.g. AC-PDPs
- H01J2211/20—Constructional details
- H01J2211/34—Vessels, containers or parts thereof, e.g. substrates
- H01J2211/42—Fluorescent layers

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Microelectronics & Electronic Packaging (AREA)
Physics & Mathematics (AREA)
Plasma & Fusion (AREA)
Manufacturing & Machinery (AREA)
Computer Hardware Design (AREA)
Power Engineering (AREA)
Luminescent Compositions (AREA)

DE69731728T 1996-01-17 1997-01-17 Mit seltenen erden aktiviertes borat und sein vorläufer, ihr herstellungsverfahren und die boratverwendung als leuchtstoff Expired - Lifetime DE69731728T2 (de)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
FR9600467		1996-01-17
FR9600467A FR2743555B1 (fr)	1996-01-17	1996-01-17	Borate de terre rare et son precurseur, leurs procedes de preparation et l'utilisation du borate comme luminophore
PCT/FR1997/000069 WO1997026312A1 (fr)	1996-01-17	1997-01-17	Borate de terre rare et son precurseur, leurs procedes de preparation et l'utilisation du borate comme luminophore

Publications (2)

Publication Number	Publication Date
DE69731728D1 true DE69731728D1 (de)	2004-12-30
DE69731728T2 DE69731728T2 (de)	2005-03-31

Family

ID=9488168

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DE69731728T Expired - Lifetime DE69731728T2 (de)	1996-01-17	1997-01-17	Mit seltenen erden aktiviertes borat und sein vorläufer, ihr herstellungsverfahren und die boratverwendung als leuchtstoff

Country Status (13)

Country	Link
US (2)	US6238593B1 (de)
EP (1)	EP0874879B1 (de)
JP (1)	JP3394261B2 (de)
KR (1)	KR100467731B1 (de)
CN (1)	CN1119384C (de)
AT (1)	ATE283329T1 (de)
BR (1)	BR9707019A (de)
CA (1)	CA2243400C (de)
DE (1)	DE69731728T2 (de)
FR (1)	FR2743555B1 (de)
HU (1)	HUP9902436A3 (de)
TW (1)	TW523489B (de)
WO (1)	WO1997026312A1 (de)

Families Citing this family (31)

* Cited by examiner, † Cited by third party
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US7166470B2 (en)	1994-10-18	2007-01-23	Symyx Technologies, Inc.	Formation of combinatorial arrays of materials using solution-based methodologies
FR2743555B1 (fr) *	1996-01-17	1998-02-27	Rhone Poulenc Chimie	Borate de terre rare et son precurseur, leurs procedes de preparation et l'utilisation du borate comme luminophore
JP2001513828A (ja)	1997-02-24	2001-09-04	スーペリアマイクロパウダーズリミテッドライアビリティカンパニー	酸素含有蛍光粉体、該蛍光粉体の製造方法、該蛍光粉体を利用してなる装置
US6197218B1 (en)	1997-02-24	2001-03-06	Superior Micropowders Llc	Photoluminescent phosphor powders, methods for making phosphor powders and devices incorporating same
EP1030339B1 (de) *	1997-11-06	2004-05-19	Matsushita Electric Industrial Co., Ltd.	Lumineszenzmittel, pulverförmiges lumineszenzmittel, plasma-anzeigetafel und herstellungsverfahren dersleben
EP0932185A1 (de) *	1997-12-23	1999-07-28	Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH	Signallampe und Leuchtstoffe dazu
US6042747A (en) *	1998-01-22	2000-03-28	Matsushita Electric Industrial Co., Ltd.	Method of preparing high brightness, small particle red-emitting phosphor
US6004481A (en) *	1998-03-27	1999-12-21	Matsushita Electric Industrial Co., Ltd.	Small particle terbium activated yttrium gadolinium borate phosphors and method of making
CN1179593C (zh) *	1998-04-23	2004-12-08	三菱电机株式会社	移动无线通信系统、发射机和接收机以及移动无线通信方法
FR2782995B1 (fr) *	1998-09-03	2000-10-06	Rhodia Chimie Sa	Borate de lanthane, de lutecium, d'yttrium ou de gadolinium comprenant deux dopants et son precurseur, utilisation dans les systemes a plasma ou a rayons x
US6284155B1 (en)	1999-10-23	2001-09-04	Matsushita Electric Industrial Co., Ltd.	Method for making small particle red emitting phosphors
JP3581921B2 (ja) *	1999-11-29	2004-10-27	独立行政法人産業技術総合研究所	無機共沈体粒子の製造方法
FR2803281B1 (fr) *	1999-12-29	2002-03-29	Rhodia Terres Rares	Procede de preparation de borates de terre rare et utilisation des borates obtenus en luminescence
US6585911B2 (en) *	2000-04-20	2003-07-01	Osram Sylvania Inc.	Method of making a borate phosphor having a discrete particle morphology
JP2002226853A (ja) *	2001-02-01	2002-08-14	Shin Etsu Chem Co Ltd	希土類元素ホウ酸塩及びその製造方法
DE10105916A1 (de) *	2001-02-09	2002-08-22	Siemens Ag	Amorphe organische 1,3,2-Dioxaborinluminophore, Verfahren zu deren Herstellung und Verwendung davon
US6596397B2 (en) *	2001-04-06	2003-07-22	Shin-Etsu Chemical Co., Ltd.	Thermal spray particles and sprayed components
DE10223988A1 (de) *	2002-05-29	2003-12-18	Siemens Ag	Leuchtstoffpulver, Verfahren zum Herstellen des Leuchtstoffpulvers und Leuchtstoffkörper mit dem Leuchtstoffpulver
US7534377B2 (en) *	2002-07-12	2009-05-19	State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University	Borate crystals for optical frequency conversion
US6805813B1 (en) *	2003-05-09	2004-10-19	Osram Sylvania Inc.	High brightness green-emitting phosphor
US8038904B2 (en) *	2004-04-14	2011-10-18	Deep Photonics Corporation	Method and structure for non-linear optics
US8062420B2 (en) *	2004-04-14	2011-11-22	State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University	Nonlinear optical crystals and their manufacture and use
FR2892113B1 (fr) *	2005-10-13	2007-12-14	Rhodia Recherches & Tech	Borate de terre rare submicronique, son procede de preparation et son utilisation comme luminophore
FR2896791B1 (fr) *	2006-01-30	2008-10-10	Rhodia Recherches & Tech	Dispersion colloidale d'un borate de terre rare, son procede de preparation et son utilisation comme luminophore
CN101605867B (zh) *	2006-10-03	2013-05-08	渲染材料公司	金属硅酸盐卤化物磷光体以及使用它们的led照明器件
KR101421719B1 (ko) *	2007-09-18	2014-07-30	삼성전자주식회사	금속 하이드록시 탄산염을 이용한 나노 형광체의 제조방법및 그로부터 제조된 나노 형광체
CN101705518B (zh) *	2008-10-08	2013-03-13	中国科学院上海硅酸盐研究所	掺Bi碱土硼酸盐晶体及其制备方法和应用
EP2468690B1 (de) *	2010-12-23	2015-04-22	Centre National de la Recherche Scientifique (CNRS)	Leuchtstoffzusammensetzung für UV-sichtbare Lichtumwandlung und damit hergestellter Lichtwandler
CN113215659A (zh) *	2020-01-21	2021-08-06	德州学院	一种稀土硼酸盐晶体材料及其制备方法和应用
TR202004482A1 (tr) *	2020-03-23	2021-10-21	Vertratech Kimya Sanayi Ve Ticaret Ltd Sirketi	Amorf ve nano yapılı lutesyum borat hekzahidratın sentezi ve kararlı kolloidal dispersiyonlarını hazırlama yöntemi
CN112473646B (zh) *	2020-12-23	2023-01-31	唐山学院	一种由多片层花瓣构成的花球状ErBO3光催化剂的制备方法

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AT258368B (de) *	1963-12-31	1967-11-27	Philips Nv	Leuchtschirm
SU385498A1 (ru) *	1970-07-28	1978-02-05	Siryachenko R G	Способ получени ортоборатов иттри и редкоземельных элементов
JPS5254690A (en) *	1975-10-31	1977-05-04	Dainippon Toryo Co Ltd	Gas discharge luminous element
NL174368C (nl) *	1976-07-13	1984-06-01	Philips Nv	Luminescerend scherm alsmede lagedrukkwikdampontladingslamp voorzien van een dergelijk scherm.
US4246246A (en) *	1977-12-10	1981-01-20	Agency Of Industrial Science & Technology, Ministry Of International Trade & Industry	Method for manufacture of hydrated borates
US5325016A (en) *	1992-06-22	1994-06-28	General Electric Company	Mercury vapor lamp with terbium-activated gadolinium borate luminescent layer
US6132642A (en) *	1994-07-01	2000-10-17	Sarnoff Corporation	Method of preparing small particle size phosphors
FR2743555B1 (fr) *	1996-01-17	1998-02-27	Rhone Poulenc Chimie	Borate de terre rare et son precurseur, leurs procedes de preparation et l'utilisation du borate comme luminophore

1996
- 1996-01-17 FR FR9600467A patent/FR2743555B1/fr not_active Expired - Fee Related
1997
- 1997-01-17 JP JP52573997A patent/JP3394261B2/ja not_active Expired - Fee Related
- 1997-01-17 KR KR10-1998-0705479A patent/KR100467731B1/ko not_active IP Right Cessation
- 1997-01-17 US US09/101,731 patent/US6238593B1/en not_active Expired - Lifetime
- 1997-01-17 BR BR9707019A patent/BR9707019A/pt not_active Application Discontinuation
- 1997-01-17 CN CN97192271A patent/CN1119384C/zh not_active Expired - Fee Related
- 1997-01-17 HU HU9902436A patent/HUP9902436A3/hu unknown
- 1997-01-17 WO PCT/FR1997/000069 patent/WO1997026312A1/fr active IP Right Grant
- 1997-01-17 CA CA002243400A patent/CA2243400C/fr not_active Expired - Fee Related
- 1997-01-17 EP EP97900649A patent/EP0874879B1/de not_active Expired - Lifetime
- 1997-01-17 AT AT97900649T patent/ATE283329T1/de not_active IP Right Cessation
- 1997-01-17 DE DE69731728T patent/DE69731728T2/de not_active Expired - Lifetime
- 1997-01-22 TW TW086100652A patent/TW523489B/zh not_active IP Right Cessation
2000
- 2000-12-22 US US09/742,344 patent/US6596196B2/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
ATE283329T1 (de)	2004-12-15
HUP9902436A3 (en)	2003-02-28
CN1211273A (zh)	1999-03-17
US6238593B1 (en)	2001-05-29
EP0874879B1 (de)	2004-11-24
US6596196B2 (en)	2003-07-22
BR9707019A (pt)	1999-07-20
KR100467731B1 (ko)	2005-05-16
HUP9902436A1 (hu)	1999-11-29
DE69731728T2 (de)	2005-03-31
US20020048543A1 (en)	2002-04-25
KR19990077332A (ko)	1999-10-25
WO1997026312A1 (fr)	1997-07-24
CA2243400A1 (fr)	1997-07-24
TW523489B (en)	2003-03-11
FR2743555B1 (fr)	1998-02-27
JP3394261B2 (ja)	2003-04-07
EP0874879A1 (de)	1998-11-04
FR2743555A1 (fr)	1997-07-18
CA2243400C (fr)	2004-12-14
JPH11503712A (ja)	1999-03-30
CN1119384C (zh)	2003-08-27

Legal Events

Date	Code	Title	Description
2005-12-22	8364	No opposition during term of opposition

Publication	Publication Date	Title
DE69731728D1 (de)	2004-12-30	Mit seltenen erden aktiviertes borat und sein vorläufer, ihr herstellungsverfahren und die boratverwendung als leuchtstoff
Lenggoro et al.	2001	Synthesis of LaPO4: Ce, Tb phosphor particles by spray pyrolysis
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