DE909131C - Process for refining carbon black - Google Patents

Process for refining carbon black

Info

Publication number
DE909131C
DE909131C DEH9823A DEH0009823A DE909131C DE 909131 C DE909131 C DE 909131C DE H9823 A DEH9823 A DE H9823A DE H0009823 A DEH0009823 A DE H0009823A DE 909131 C DE909131 C DE 909131C
Authority
DE
Germany
Prior art keywords
carbon black
phenols
refining carbon
refining
pyrocatechol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEH9823A
Other languages
German (de)
Inventor
Dr Gerhard Lix
Dr Walter Sonneborn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Michael Huber K G
Original Assignee
Michael Huber K G
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Michael Huber K G filed Critical Michael Huber K G
Priority to DEH9823A priority Critical patent/DE909131C/en
Application granted granted Critical
Publication of DE909131C publication Critical patent/DE909131C/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C09C1/56—Treatment of carbon black ; Purification

Description

Verfahren zur Veredelung von Ruß Es gibt verschiedene Qualitäten von Ruß, welche für die weitere Verarbeitung zu hochwertigen Farben nicht geeignet sind. Ziel der Erfindung ist es, ein Verfahren zu zeigen, welches es ermöglicht, Ruß, insbesondere Gasruß, der in diesem Sinne als minderwertig zu bezeichnen ist, so zu veredeln, daß er den besten auf dem Markt befindlichen Qualitäten für Ruß für die genannten Zwecke gleichkommt.Process for upgrading carbon black There are different qualities of Soot, which is not suitable for further processing into high-quality paints. The aim of the invention is to show a method which enables carbon black, in particular carbon black, which in this sense can be described as inferior, so to refine so that it is made of the best grades for carbon black available on the market corresponds to the stated purposes.

Grundsätzlich besteht das neue Verfahren darin, daß der Ruß mit Phenolen oder deren Derivaten behandelt wird, wobei auch Mischungen von Phenolen zur Anwendung kommen können, und ebenso ist es möglich, die Phenole so, wie sie anfallen, zu verwenden, also z. B. in Form von Goudron. Insbesondere sind die Dioxybenzole geeignet und da vor allem das Brenzkatechin. Es werden damit sogar bessere Ruße erzielt, als bisher überhaupt bekannt waren. Insbesondere das Fließvermögen wird erhöht, und die mit diesem Ruß dann hergestellte Farbe wird glänzender und tiefer, insbesondere auch ausgiebiger. Die Einwirkung kann auf verschiedene Weise erfolgen, am einfachsten und ungefährlichsten ist es, in wäßriger Suspension zu arbeiten. Beispielsreise werden 5o g E-Ruß mit etwa 5o ccm Spiritus in 21 heißem Wasser suspendiert. Um eine genügend feine Verteilung zu erreichen, wird die Mischung zweimal durch eine Trichtermühle geschickt. Dann werden 7 g Brenzkatechin, in wenig Wasser gelöst, hinzugefügt. Nachdem die Mischung 2 Tage bei gewöhnlicher Temperatur gestanden hatte, wird abgesaugt und im Trockenschrank bei roo° getrocknet. Das so erhaltene Produkt hat die gewünschten Eigenschaften, und die damit hergestellte Farbe ist außerdem im Hinblick auf den ölbedarf ausgiebiger als die bekannten besten Qualitäten.Basically, the new process consists in that the carbon black with phenols or their derivatives is treated, mixtures of phenols also being used can come, and it is also possible to use the phenols as they arise, so z. B. in the form of Goudron. In particular, the dioxybenzenes are suitable and there especially the catechol. Even better carbon blacks are achieved with it than were previously known at all. In particular, the flowability is increased, and the color then produced with this carbon black becomes shinier and deeper, in particular also more extensive. The action can be done in several ways, the simplest is the easiest and the least dangerous is to work in an aqueous suspension. Sample trip 50 g of E-carbon black are suspended in about 50 cc of spirit in 21% of hot water. To a To achieve enough fine distribution, the mixture is passed through a hopper mill twice sent. Then 7 g of pyrocatechol, dissolved in a little water, are added. After this the mixture had stood for 2 days at normal temperature, is filtered off with suction and dried in a drying cabinet at roo °. The product thus obtained has the desired properties, and the color produced with it is also more extensive than the known best grades in terms of oil requirements.

Selbstverständlich kann man die Behandlung auch mit Substanzen durchführen, welche Phenole, z. B. Brenzkatechin, abspalten, genannt sei beispielsweise Holzteer, der beim Erhitzen Brenzkatechin ergibt.Of course, the treatment can also be carried out with substances which phenols, e.g. B. pyrocatechol, split off, for example wood tar, which gives catechol when heated.

Claims (2)

PATGXTANSPRUCHE: i. Verfahren zur Veredelung von Ruß, insbesondere Gasruß, dadurch gekennzeichnet, daß Ruß mit Phenolen oder deren Derivaten oder phenolhaltigen Substanzen behandelt wird. PATGX CLAIMS: i. Process for upgrading carbon black, in particular Gas black, characterized in that carbon black with phenols or their derivatives or containing phenols Substances is treated. 2. Verfahren nach Anspruch i, dadurch gekennzeichnet, daß Dioxybenzole, insbesondere Brenzkatechin, angewandt werden.2. The method according to claim i, characterized in that that dioxybenzenes, especially pyrocatechol, are used.
DEH9823A 1951-09-23 1951-09-23 Process for refining carbon black Expired DE909131C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEH9823A DE909131C (en) 1951-09-23 1951-09-23 Process for refining carbon black

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEH9823A DE909131C (en) 1951-09-23 1951-09-23 Process for refining carbon black

Publications (1)

Publication Number Publication Date
DE909131C true DE909131C (en) 1954-05-31

Family

ID=7146131

Family Applications (1)

Application Number Title Priority Date Filing Date
DEH9823A Expired DE909131C (en) 1951-09-23 1951-09-23 Process for refining carbon black

Country Status (1)

Country Link
DE (1) DE909131C (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996018456A2 (en) * 1994-12-15 1996-06-20 Cabot Corporation Gel composition containing carbonaceous compound

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996018456A2 (en) * 1994-12-15 1996-06-20 Cabot Corporation Gel composition containing carbonaceous compound
WO1996018456A3 (en) * 1994-12-15 1996-08-29 Cabot Corp Gel composition containing carbonaceous compound
US5807494A (en) 1994-12-15 1998-09-15 Boes; Ralph Ulrich Gel compositions comprising silica and functionalized carbon products
US6107350A (en) 1994-12-15 2000-08-22 Cabot Corporation Gel compositions

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