US20080078506A1 - RF Coil Plasma Generation - Google Patents

RF Coil Plasma Generation Download PDF

Info

Publication number
US20080078506A1
US20080078506A1 US11/537,460 US53746006A US2008078506A1 US 20080078506 A1 US20080078506 A1 US 20080078506A1 US 53746006 A US53746006 A US 53746006A US 2008078506 A1 US2008078506 A1 US 2008078506A1
Authority
US
United States
Prior art keywords
coil
plasma
plasma chamber
conductor
power source
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US11/537,460
Inventor
Guido Fridolin Verbeck
Andrew Cordell
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FEI EFA Inc
Original Assignee
Zyvex Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zyvex Corp filed Critical Zyvex Corp
Priority to US11/537,460 priority Critical patent/US20080078506A1/en
Assigned to ZYVEX CORPORATION reassignment ZYVEX CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: VERBECK, GUIDO FRIDOLIN, IV, CORDELL, ANDREW
Assigned to ZYVEX INSTRUMENTS, LLC reassignment ZYVEX INSTRUMENTS, LLC NUNC PRO TUNC ASSIGNMENT (SEE DOCUMENT FOR DETAILS). Assignors: ZYVEX CORPORATION
Publication of US20080078506A1 publication Critical patent/US20080078506A1/en
Assigned to DCG SYSTEMS, INC. reassignment DCG SYSTEMS, INC. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: ZYVEX INSTRUMENTS, LLC
Abandoned legal-status Critical Current

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32082Radio frequency generated discharge
    • H01J37/321Radio frequency generated discharge the radio frequency energy being inductively coupled to the plasma
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/26Electron or ion microscopes; Electron or ion diffraction tubes
    • H01J37/28Electron or ion microscopes; Electron or ion diffraction tubes with scanning beams
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/02Details
    • H01J2237/022Avoiding or removing foreign or contaminating particles, debris or deposits on sample or tube
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/18Vacuum control means

Definitions

  • Low temperature plasmas of various ionized gases can be used to reactively etch or ash organic materials found on the surface of materials.
  • plasma cleaning, etching or ashing has been used to clean and otherwise condition the interiors of large vacuum vessels, as well as to clean and etch semiconductor wafers and other bulk materials.
  • commercially-available RF or DC plasma dry-ashing devices may be utilized for cleaning electron microscope components and specimens prior to specimen analysis.
  • glow discharge is used to produce ions that are then transformed oxygen radicals by subsequent reactions, and the radicals are fed from the plasma chamber in which they are generated, into the vacuum chamber where specimens are to be analyzed.
  • FIG. 1 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 2 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 3 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 4 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 5 is a state diagram demonstrating one or more aspects of the present disclosure
  • FIGS. 6A-6D are flow-chart diagrams each demonstrating one or more aspects of the present disclosure.
  • FIG. 1 illustrated is a block diagram of apparatus 100 according to one or more aspects of the present disclosure.
  • Embodiments of apparatus 100 within the scope of the present disclosure may include each of the components shown in FIG. 1 , multiple instances of one or more of the components shown in FIG. 1 , and/or a subset of the components shown in FIG. 1 , as well as other components not specifically described herein.
  • Apparatus 100 may include a vacuum chamber 102 , a plasma chamber 104 , and one or more RF power sources 106 .
  • the vacuum chamber 102 may be that of a scanning electron microscope (SEM) or other microscopy apparatus, and may be conventional or future-developed. However, the vacuum chamber 102 may be retrofitted to be configured to receive the plasma chamber 104 according to aspects of the present disclosure.
  • the plasma chamber 104 may be coupled or integral to the vacuum chamber 102 , and may also be of a conventional or future-developed nature, except as otherwise described herein.
  • the plasma chamber 104 is configured to generate a plasma which feeds into the vacuum chamber 102 via one or more apertures between the plasma chamber 104 and the vacuum chamber 102 , and/or other means.
  • the one or more RF power sources 106 may be configured to deliver an RF signal to a coil within the plasma chamber 104 to ignite and maintain plasma generation within the plasma chamber 104 .
  • apparatus 100 may include a conventional or future-developed electrical feedthrough 108 through which the electrical signal may be delivered from the one or more RF power sources 106 to the internal coil.
  • Apparatus 100 may also include one or more of a column 110 with an integral or attached emitter 112 .
  • the column 110 may be configured to steer and/or focus an electron beam, ion beam, and/or other beam.
  • the column 110 and/or emitter 112 may be that of an SEM or other microscopy apparatus, and may be conventional or future-developed.
  • Apparatus 100 may also include one or more of a gas inlet 114 , a flow controller 116 , a flow or pressure sensor 118 , a selector valve 120 , a first gas supply 122 , and a second gas supply 124 , each of which may be conventional and/or future-developed.
  • the flow controller 116 may be or include a flow servo and/or other components configured to regulate gas flow from the selector valve 120 through the gas inlet 114 and into the plasma chamber 104 .
  • the flow controller 116 may be manually or automatically operable.
  • the flow or pressure sensor 118 may be configured to monitor the flow rate, pressure and/or composition of plasma source gas through the flow controller 116 .
  • the selector valve 120 is manually or automatically operable to select between the first gas supply 122 and the second gas supply 124 .
  • the first and second gas supplies 122 , 124 may contain the same or different gas compositions to be utilized as plasma source gas.
  • the first gas supply 122 may contain an oxygen gas supply and the second gas supply 124 may contain an argon gas supply.
  • the selector valve 120 and/or the flow controller 116 may be configured such that gas from only one of the gas supplies 122 , 124 may flow into the plasma chamber 104 at a time, or may alternatively be configured to allow flow of various mixtures of gas from the gas supplies 122 , 124 simultaneously.
  • Apparatus 100 may also include one or more sensors 130 , 131 for detecting the presence of plasma within the plasma chamber 104 and/or for detecting a plasma concentration in the plasma chamber 104 .
  • the sensors 130 , 131 may be conventional or future-developed, and may also or alternatively be configured to detect other conditions within the plasma chamber 104 .
  • sensor 131 may be configured to detect current flow between the coil and the wall of plasma chamber 104 , the signal from which may be transmitted to a plasma detect circuit 133 for generating a signal sent to the controller 132 to indicate existence and/or concentration of plasma within the chamber 104 .
  • Apparatus 100 may also include a controller 132 (or multiple controllers hereafter referred to collectively as the controller 132 ).
  • the controller 132 may be configured to send and/or receive information to/from the sensors 130 , 131 , one or more of the RF power sources 106 , the flow controller 116 , the flow sensor 118 , and/or the selector valve 120 , and/or other components of the apparatus 100 .
  • the controller 132 may be configured to operate the plasma chamber 104 and the RF power sources 106 in an ignition state and a steady state.
  • the controller 132 may be configured to increase the pressure of the plasma chamber 104 and/or decrease the output from one or more of the RF power sources 106 when transitioning from the ignition state to the steady state.
  • the controller 132 may also or alternatively be configured to transition operation of the plasma chamber 104 and/or one or more of the RF power sources 106 between the ignition state and the steady state in response to the expiration of a predetermined time period.
  • the controller 132 may also or alternatively be configured to transition operation of the plasma chamber 104 and/or one or more of the RF power sources 106 between the ignition state and the steady state in response to detection of plasma within the plasma chamber 104 via sensor 130 and/or 131 .
  • the controller 132 may also or alternatively be configured to transition operation of the plasma chamber 104 and/or one or more of the power sources 106 between the steady state and the ignition state in response to a plasma level within the plasma chamber 104 falling below a minimum plasma level, as possibly detected by sensor 130 and/or 131 .
  • FIG. 2 illustrated is a perspective view of at least a portion of the plasma chamber 104 shown in FIG. 1 , in which a section of the plasma chamber's wall 202 has been removed for illustrative purposes.
  • the plasma chamber 104 includes a coil 204 and a conductive member 206 , as described below.
  • the plasma chamber 104 also includes an interface for coupling to the vacuum chamber 102 described above and shown in FIG. 1 .
  • the plasma chamber 104 is integral to the vacuum chamber 102 .
  • the plasma chamber 104 may be substantially cylindrical in shape, having an outer diameter ranging between about 30 mm and about 150 mm, an inner diameter ranging between about 25 mm and about 140 mm, and a length ranging between about 15 mm and about 150 mm. As shown in FIG. 2 , an end 202 a of the plasma chamber 104 may be open or otherwise have an aperture and/or other means through which plasma may feed into the vacuum chamber 102 .
  • the coil 204 comprises a conductive wire or other material that has been formed into a number of turns.
  • the coil 204 includes about 51 ⁇ 2 turns.
  • the coil 204 may have a number of turns ranging between about 4 and about 200.
  • the coil 204 may substantially comprise aluminum, copper, gold, or alloys thereof, among other compositions.
  • the coil 204 may also include an outer coating of dielectric material and/or other materials.
  • the outer diameter of the coil 204 may range between about 20 mm and about 130 mm, and the length of the coil 204 may range between about 15 mm and about 150 mm.
  • the thickness or gauge of the wire or other material forming the coil 204 may range between about 0.001′′ and about 0.25′′.
  • One end 208 of the coil 204 is connected, at least indirectly, to one or more of the RF sources 106 described above.
  • the other end 209 of the coil 204 may not be electrically connected to anything, such that the coil 204 may be electrically open-ended.
  • the coil 204 may also be electrically isolated from the plasma chamber wall 202 and/or the remainder of the plasma chamber 104 .
  • an electrical feedthrough may be employed to connect the coil 204 to the RF source 106 through the chamber wall 202 .
  • Such electrical feedthrough may also be utilized to set the position of the coil 204 within the plasma chamber 104 .
  • the conductive member 206 comprises a conductive wire or other material that is positioned between the coil 204 and the plasma chamber wall 202 .
  • the conductive member 206 may be positioned substantially parallel to the central axis 204 a of the coil 204 and/or the plasma chamber wall 202 .
  • the conductive member 206 may alternatively be omitted, such as where the internal surface of the chamber wall 202 , or a portion thereof, performs the function of the conductive member 206 . That is, the conductive member 206 may be an alternate ground to the chamber wall 202 .
  • the conductive member 206 may be employed, because it may become difficult to reduce the production of needed radicals with a single coil under certain RF power constraints. Thus, the conductive member 206 may optionally be included to better lower the radical production.
  • the conductive member 206 may substantially comprise aluminum, copper, gold, or alloys thereof, among other compositions.
  • the conductive member 206 may also include an outer coating of dielectric material and/or other materials.
  • the length of the conductive member 206 may range between about 15 mm and about 150 mm, and the thickness or gauge of the wire or other material forming the conductive member 206 may range between about 0.001′′ and about 0.25′′.
  • One end 212 of the conductive member 206 may be connected, at least indirectly, to a DC or ground potential.
  • the other end 213 of the conductive member 206 may not be electrically connected to anything, such that the conductive member 206 may be electrically open-ended.
  • the conductive member 206 may electrically isolated from the plasma chamber wall 202 and/or the remainder of the plasma chamber 104 .
  • an electrical feedthrough may be employed to connect the conductive member 206 to the DC or ground potential 210 through the chamber wall 202 .
  • Such electrical feedthrough may also be utilized to set the position of the conductive member 206 within the plasma chamber 104 .
  • the conductor may be laterally separated from the outer perimeter of the coil 204 by a distance ranging between about 0.25′′ and about 10′′, and/or by a distance ranging between about 10% and about 100% of the outer diameter of the coil 204 .
  • the plasma chamber 104 includes the open-ended coil 204 and the grounded or DC-biased conductive member 206 (shown as being grounded in FIG. 3 ).
  • the coil 204 includes about 71 ⁇ 2 turns.
  • the thickness or gauge of the material utilized to form the coil 204 is described above.
  • the gap between each neighboring pair of turns may range between 0 and about 12 mm.
  • the gap may range between about 0 and about 4 mm.
  • the pitch P may be less than about 150% of the wire thickness.
  • the pitch P may be about 110% of the wire thickness.
  • the radius R of one or more turns of the coil 204 may range between about 5 mm and about 65 mm. In the embodiment illustrated in FIG. 3 , each turn of the coil 204 has a substantially similar radius R, although in other embodiments one or more turns of the coil 204 may have a different radius R relative to other turns of the coil 204 .
  • FIG. 4 illustrated is a schematic view of another embodiment of at least a portion of the internal components of the plasma chamber 104 shown in FIGS. 1-3 , herein designated by the reference numeral 304 .
  • the plasma chamber 304 may be utilized in substantially the same manner as the plasma chamber 104 shown in FIGS. 1-3 , and may otherwise be substantially similar in composition, manufacture, and geometry to the plasma chamber 104 , except as described below.
  • the plasma chamber 304 includes an outer coil 306 and an inner coil 308 .
  • the outer coil 306 may be substantially similar in composition, manufacture, and geometry to the coil 204 described above and shown in FIGS. 2 and 3 .
  • the outer coil 306 may include an end 310 that is coupled, at least indirectly, to an RF power source, such as the RF source 106 shown in FIGS. 1 and 2 .
  • Another end 311 of the outer coil 306 may be open.
  • the outer coil 306 may have a number of turns ranging between about 4 and about 200, an outer diameter ranging between about 20 mm and about 130 mm, and a length ranging between about 15 mm and about 150 mm, where the gaps between each pair of neighboring turns may range between about 0 and about 12 mm.
  • the inner coil 308 may be positioned substantially coaxially within the outer coil, and may be substantially similar in composition and manufacture to the outer coil 306 .
  • the outer diameter of the inner coil 308 may range between about 10 mm and about 100 mm, and its length may range between about 15 mm and about 150 mm.
  • the inner coil 308 may have a number of turns ranging between about 5 and about 500.
  • the ratio of the outer diameter of the outer coil 306 to the outer diameter of the inner coil 308 may range between about 1.1 and about 7.
  • the ratio of the number of turns included in the outer coil 306 to the number of turns included in the inner coil 308 may range between about 1.1 and about 10.
  • the ratio of the length of the outer coil 306 to the length of the inner coil 308 may range between about 1 and about 0.5.
  • An end 312 of the inner coil 308 may be electrically coupled, at least indirectly, to an RF power source, such as the RF power source 106 shown in Figs., and 2 , whereas the other end 313 may be open.
  • the outer coil 306 and the inner coil 308 may be connected to the same RF source or to different RF sources, such that each of the coils 306 , 308 may be driven independently, and may be driven simultaneously with the same or different RF sources.
  • the ends 311 , 313 of the outer and inner coils 306 , 308 may each be electrically open.
  • the conductive member 206 shown in FIGS. 2 and 3 may not be included.
  • the plasma chamber 304 itself (such as the plasma chamber wall 202 shown in FIG. 2 ) may be electrically grounded, whether or not the conductor member 206 is included in the plasma chamber, an whether or not a single coil 204 or dual-coils 206 / 208 are included in the plasma chamber. The same holds true for the plasma chamber 104 shown in FIGS. 1-3 .
  • FIG. 5 illustrated is a state diagram 500 demonstrating one or more aspects of the present disclosure.
  • the state diagram 500 demonstrates one or more operational aspects of the plasma chamber 104 shown in FIGS. 1 and 2 , the apparatus 100 shown in FIG. 1 , and/or the coils 204 , 304 , 306 and 308 shown in FIGS. 1-4 .
  • Operation may begin in a START state 502 . Operation may then transition to an IGNITION state 504 after, for example, a start-up procedure is executed, among other possible transition-triggering events.
  • the IGNITION state 504 is utilized to ignite a plasma in the plasma chamber (such as the plasma chamber 104 or 304 shown in FIGS. 1-4 ). For example, an ignition RF power level and an ignition pressure level may be utilized in the IGNITION state 504 .
  • Operation may then transition to a STEADY state 506 upon the occurrence of the appropriate transition-triggering event.
  • the plasma chamber may be monitored to detect the presence or level of plasma. If plasma is detected when the IGNITION state 504 is active, operation may transition to the STEADY state 506 .
  • the IGNITION state 504 may only be operational for a predetermined period of time. Upon the expiration of such time period, operation may transition to the STEADY state 506 .
  • the predetermined time period may range between about 5 seconds and about 30 seconds, and may be user selectable and/or preprogrammed by the manufacturer. In an exemplary embodiment, the predetermined time period may be about 10 seconds.
  • the STEADY state 506 is utilized to maintain plasma generation within the plasma chamber.
  • a steady state RF power level and a steady state pressure level may be maintained in the STEADY state 506 .
  • the steady state RF power level may be less than the ignition RF power level, whereas the steady state pressure level may be greater than the ignition pressure level.
  • the ignition RF power level may range between about 10 W and about 20 W, whereas the steady state RF power level may range between about 1 W and about 10 W.
  • the ignition pressure level may range between about 10 mT and about 600 mT, whereas the steady state pressure level may range between about 300 mT and about 1000 mT.
  • the steady state RF power and pressure levels may be configured such that oxygen radicals and/or other radicals are generated in the plasma chamber, such that the radicals may feed into the vacuum chamber for cleaning and/or other purposes.
  • Operation in the STEADY state 506 may continue until the occurrence of the appropriate transition-triggering event.
  • one such event may be when the plasma source gas is altered, such as by switching between the first and second gas supplies 122 , 124 shown in FIG. 1 , or by altering the composition of a mixture of gas being delivered from the first and second gas supplies simultaneously. Either of such events, among others, may trigger operation to transition back to the IGNITION state 504 .
  • Another exemplary event that may trigger the transition from the STEADY state 506 to the IGNITION state 504 is the detection of plasma in the plasma chamber dropping below a threshold concentration, or the lack of plasma existence in the plasma chamber.
  • operation transitions back to the IGNITION state 504 so that plasma ignition can be repeated, at which time operation may once again transition to the STEADY state 506 .
  • Operation may also transition from the STEADY state 506 to a STOP state 508 upon the occurrence of the appropriate transition-triggering event, such as the receipt of user-input indicating that operation is to be halted.
  • method 600 a includes a step 602 in which a plasma is ignited, as described above. After the plasma is ignited, the plasma chamber pressure is increased in a step 604 to a steady state plasma generation chamber pressure. The plasma generation is then maintained during a step 606 until, as determined by decisional step 608 , plasma is no longer detected. That is, if plasma is continually detected during step 608 , then the step 606 is repeated. However, if it is determined during decisional step 608 that plasma is no longer detected, or that plasma concentration has dropped below a threshold value, then the pressure is decreased in a step 610 , and step 602 is repeated to re-ignite the plasma.
  • method 600 b includes step 602 in which plasma is ignited, as described above. After the plasma is ignited, the RF power is decreased in a step 605 to a steady state plasma generation RF power. The plasma generation is then maintained during step 606 until, as determined by decisional step 608 , plasma is no longer detected. That is, if plasma is continually detected during step 608 , then the step 606 is repeated. However, if it is determined during decisional step 608 that plasma is no longer detected, or that plasma concentration has dropped below a threshold value, then the RF power is increased in a step 611 , and step 602 is repeated to re-ignite the plasma.
  • method 600 c includes step 602 in which plasma is ignited, as described above. After the plasma is ignited, the RF power is decreased to a steady state plasma generation RF power, and the plasma chamber pressure is increased to a steady state plasma generation chamber pressure, in a step 620 . The plasma generation is then maintained during step 606 until, as determined by decisional step 608 , plasma is no longer detected. That is, if plasma is continually detected during step 608 , then the step 606 is repeated.
  • step 608 determines whether plasma is no longer detected, or that plasma concentration has dropped below a threshold value. If it is determined during decisional step 608 that plasma is no longer detected, or that plasma concentration has dropped below a threshold value, then the RF power is increased and the chamber pressure is decreased in a step 622 , and step 602 is repeated to re-ignite the plasma.
  • method 600 d includes step 602 in which plasma is ignited, as described above. After plasma ignition is attempted, decisional step 608 a is performed determine whether plasma has successfully been ignited. If plasma has not been ignited, or if plasma concentration is not at an acceptable level, then the RF power is increased and the plasma chamber pressure is decreased in step 622 . Plasma ignition is then attempted again in step 602 . This iterative process may be repeated until plasma is significantly ignited, and perhaps generated to at least a predetermined concentration, as determined by decisional step 608 a.
  • step 608 a Once plasma has been adequately ignited, as determined by decisional step 608 a, the RF power is decreased and the plasma chamber pressure is increased in step 620 . Thereafter, plasma is maintained in step 606 . However, the plasma concentration level may be periodically, continuously, or otherwise monitored. If sufficient plasma is detected, as determined by decisional step 608 b, then step 606 is repeated and the plasma generation is maintained. However, if sufficient plasma is not detected, as determined by decisional step 608 b, then the RF power is increased and the plasma chamber pressure is decreased as step 622 is repeated, and then plasma re-ignition is attempted as step 602 is repeated.
  • the plasma chamber pressure during plasma ignition and/or plasma generation may range between about 10 mT and about 10 T.
  • the plasma chamber pressure during plasma ignition is about 100 mT and the plasma chamber pressure during steady state plasma generation is about 600 mT, or the plasma chamber pressure during steady state plasma generation may be about 600% greater than the plasma chamber pressure during plasma ignition.
  • the RF power during plasma ignition and/or plasma generation may range between about 5 W and about 20 W.
  • the RF power during plasma ignition is about 20 W and the RF power during steady state plasma generation is about 10 W, or the RF power during steady state may otherwise be about 50% less than the RF power during the plasma ignition.
  • the RE frequency during plasma ignition and/or plasma generation may range between about 1 MHz and about 1 GHz.
  • the RF frequency during plasma ignition and steady state plasma generation is about 13.56 MHz.
  • the present disclosure introduces an apparatus comprising a plasma chamber, a radio frequency (RF) power source, and a coil centrally disposed in the plasma chamber.
  • the plasma chamber is configured to generate plasma that feeds a vacuum chamber adjacent the plasma chamber, and a first end of the coil is electrically coupled to the RF power source while a second end of the coil is electrically open.
  • a method of manufacturing an apparatus includes disposing a coil centrally in a plasma chamber; wherein a first end of the coil is electrically open, and wherein the plasma chamber is configured to generate plasma that feeds into a vacuum chamber adjacent the plasma chamber.
  • a radio frequency (RF) power source is then coupled to a second end of the coil.
  • Additional apparatus introduced in the present disclosure comprises a vacuum chamber, an emitter configured to emit a beam of at least one of ions and electrons into the vacuum chamber, and a plasma chamber coupled to the vacuum chamber.
  • Such apparatus also includes means for supplying a plasma source gas into the plasma chamber, a radio frequency (RF) power source, and a coil located in a substantially central portion of the plasma chamber, wherein a first end of the coil is electrically coupled to the RF power source and a second end of the coil is electrically open.
  • RF radio frequency
  • Also introduced in the present disclosure is a method of operating a plasma chamber for use with an electron or ion beam apparatus
  • the method may comprise igniting a plasma in the plasma chamber by utilizing a first radio frequency (RF) power and a first plasma chamber pressure.
  • the plasma may then be maintained by utilizing a second RF power and a second plasma chamber pressure, wherein the second RF power is substantially less than the first RF power and the second plasma chamber pressure is substantially greater than the first plasma chamber pressure.
  • RF radio frequency
  • Another method introduced in the present disclosure comprises transitioning a plasma chamber to a steady state when a first event occurs, and transitioning the chamber to an ignition state when a second event occurs.
  • the ignition state employs a greater RF power than the steady state
  • the steady state employs a greater chamber pressure than the ignition state.
  • a system introduced in the present disclosure comprises a plasma chamber, a radio frequency (RF) power source coupled to a magnetic plasma igniting means that is disposed within the plasma chamber, and a controller configured to operate the plasma chamber and the RF power source in an ignition state and a steady state, including increasing the plasma chamber's pressure and decreasing the RF power source's output when transitioning from the ignition state to the steady state.
  • RF radio frequency

Abstract

Apparatus comprising a plasma chamber, a radio frequency (RF) power source, and a coil centrally disposed in the plasma chamber. The plasma chamber is configured to generate plasma that feeds a vacuum chamber adjacent the plasma chamber, and a first end of the coil is electrically coupled to the RF power source while a second end of the coil is electrically open.

Description

    CROSS-REFERENCE TO RELATED APPLICATIONS
  • This application is related to commonly-assigned U.S. application Ser. No. XX/XXX,XXX, entitled “RF COIL PLASMA GENERATION,” Attorney Docket No. 34003.185, filed concurrently herewith.
  • BACKGROUND
  • Low temperature plasmas of various ionized gases can be used to reactively etch or ash organic materials found on the surface of materials. Such plasma cleaning, etching or ashing has been used to clean and otherwise condition the interiors of large vacuum vessels, as well as to clean and etch semiconductor wafers and other bulk materials. For example, commercially-available RF or DC plasma, dry-ashing devices may be utilized for cleaning electron microscope components and specimens prior to specimen analysis. In such devices, glow discharge is used to produce ions that are then transformed oxygen radicals by subsequent reactions, and the radicals are fed from the plasma chamber in which they are generated, into the vacuum chamber where specimens are to be analyzed.
  • BRIEF DESCRIPTION OF THE DRAWINGS
  • The present disclosure is best understood from the following detailed description when read with the accompanying figures. It is emphasized that, in accordance with the standard practice in the industry, various features are not drawn to scale. In fact, the dimensions of the various features may be arbitrarily increased or reduced for clarity of discussion.
  • FIG. 1 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 2 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 3 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 4 is a schematic view of apparatus according to one or more aspects of the present disclosure.
  • FIG. 5 is a state diagram demonstrating one or more aspects of the present disclosure,
  • FIGS. 6A-6D are flow-chart diagrams each demonstrating one or more aspects of the present disclosure.
  • DETAILED DESCRIPTION
  • It is to be understood that the following disclosure provides many different embodiments, or examples, for implementing different features of various embodiments. Specific examples of components and arrangements are described below to simplify the present disclosure. These are, of course, merely examples and are not intended to be limiting. In addition, the present disclosure may repeat reference numerals and/or letters in the various examples. This repetition is for the purpose of simplicity and clarity and does not in itself dictate a relationship between the various embodiments and/or configurations discussed,
  • Referring to FIG. 1, illustrated is a block diagram of apparatus 100 according to one or more aspects of the present disclosure. Embodiments of apparatus 100 within the scope of the present disclosure may include each of the components shown in FIG. 1, multiple instances of one or more of the components shown in FIG. 1, and/or a subset of the components shown in FIG. 1, as well as other components not specifically described herein.
  • Apparatus 100 may include a vacuum chamber 102, a plasma chamber 104, and one or more RF power sources 106. The vacuum chamber 102 may be that of a scanning electron microscope (SEM) or other microscopy apparatus, and may be conventional or future-developed. However, the vacuum chamber 102 may be retrofitted to be configured to receive the plasma chamber 104 according to aspects of the present disclosure. The plasma chamber 104 may be coupled or integral to the vacuum chamber 102, and may also be of a conventional or future-developed nature, except as otherwise described herein. The plasma chamber 104 is configured to generate a plasma which feeds into the vacuum chamber 102 via one or more apertures between the plasma chamber 104 and the vacuum chamber 102, and/or other means. The one or more RF power sources 106 may be configured to deliver an RF signal to a coil within the plasma chamber 104 to ignite and maintain plasma generation within the plasma chamber 104. For example, apparatus 100 may include a conventional or future-developed electrical feedthrough 108 through which the electrical signal may be delivered from the one or more RF power sources 106 to the internal coil.
  • Apparatus 100 may also include one or more of a column 110 with an integral or attached emitter 112. The column 110 may be configured to steer and/or focus an electron beam, ion beam, and/or other beam. For example, the column 110 and/or emitter 112 may be that of an SEM or other microscopy apparatus, and may be conventional or future-developed.
  • Apparatus 100 may also include one or more of a gas inlet 114, a flow controller 116, a flow or pressure sensor 118, a selector valve 120, a first gas supply 122, and a second gas supply 124, each of which may be conventional and/or future-developed. The flow controller 116 may be or include a flow servo and/or other components configured to regulate gas flow from the selector valve 120 through the gas inlet 114 and into the plasma chamber 104. The flow controller 116 may be manually or automatically operable. The flow or pressure sensor 118 may be configured to monitor the flow rate, pressure and/or composition of plasma source gas through the flow controller 116.
  • The selector valve 120 is manually or automatically operable to select between the first gas supply 122 and the second gas supply 124. The first and second gas supplies 122, 124 may contain the same or different gas compositions to be utilized as plasma source gas. For example, the first gas supply 122 may contain an oxygen gas supply and the second gas supply 124 may contain an argon gas supply. Of course, other compositions are also within the scope of the present disclosure. The selector valve 120 and/or the flow controller 116 may be configured such that gas from only one of the gas supplies 122, 124 may flow into the plasma chamber 104 at a time, or may alternatively be configured to allow flow of various mixtures of gas from the gas supplies 122, 124 simultaneously.
  • Apparatus 100 may also include one or more sensors 130, 131 for detecting the presence of plasma within the plasma chamber 104 and/or for detecting a plasma concentration in the plasma chamber 104. The sensors 130, 131 may be conventional or future-developed, and may also or alternatively be configured to detect other conditions within the plasma chamber 104. For example, sensor 131 may be configured to detect current flow between the coil and the wall of plasma chamber 104, the signal from which may be transmitted to a plasma detect circuit 133 for generating a signal sent to the controller 132 to indicate existence and/or concentration of plasma within the chamber 104.
  • Apparatus 100 may also include a controller 132 (or multiple controllers hereafter referred to collectively as the controller 132). The controller 132 may be configured to send and/or receive information to/from the sensors 130, 131, one or more of the RF power sources 106, the flow controller 116, the flow sensor 118, and/or the selector valve 120, and/or other components of the apparatus 100. The controller 132 may be configured to operate the plasma chamber 104 and the RF power sources 106 in an ignition state and a steady state.
  • For example, the controller 132 may be configured to increase the pressure of the plasma chamber 104 and/or decrease the output from one or more of the RF power sources 106 when transitioning from the ignition state to the steady state. The controller 132 may also or alternatively be configured to transition operation of the plasma chamber 104 and/or one or more of the RF power sources 106 between the ignition state and the steady state in response to the expiration of a predetermined time period. The controller 132 may also or alternatively be configured to transition operation of the plasma chamber 104 and/or one or more of the RF power sources 106 between the ignition state and the steady state in response to detection of plasma within the plasma chamber 104 via sensor 130 and/or 131. The controller 132 may also or alternatively be configured to transition operation of the plasma chamber 104 and/or one or more of the power sources 106 between the steady state and the ignition state in response to a plasma level within the plasma chamber 104 falling below a minimum plasma level, as possibly detected by sensor 130 and/or 131.
  • Referring to FIG. 2, illustrated is a perspective view of at least a portion of the plasma chamber 104 shown in FIG. 1, in which a section of the plasma chamber's wall 202 has been removed for illustrative purposes. The plasma chamber 104 includes a coil 204 and a conductive member 206, as described below. Although not illustrated, the plasma chamber 104 also includes an interface for coupling to the vacuum chamber 102 described above and shown in FIG. 1. Alternatively, the plasma chamber 104 is integral to the vacuum chamber 102. The plasma chamber 104 may be substantially cylindrical in shape, having an outer diameter ranging between about 30 mm and about 150 mm, an inner diameter ranging between about 25 mm and about 140 mm, and a length ranging between about 15 mm and about 150 mm. As shown in FIG. 2, an end 202 a of the plasma chamber 104 may be open or otherwise have an aperture and/or other means through which plasma may feed into the vacuum chamber 102.
  • The coil 204 comprises a conductive wire or other material that has been formed into a number of turns. For example, in the illustrated embodiment, the coil 204 includes about 5½ turns. In other embodiments within the scope of the present disclosure, the coil 204 may have a number of turns ranging between about 4 and about 200. The coil 204 may substantially comprise aluminum, copper, gold, or alloys thereof, among other compositions. The coil 204 may also include an outer coating of dielectric material and/or other materials. The outer diameter of the coil 204 may range between about 20 mm and about 130 mm, and the length of the coil 204 may range between about 15 mm and about 150 mm. The thickness or gauge of the wire or other material forming the coil 204 may range between about 0.001″ and about 0.25″.
  • One end 208 of the coil 204 is connected, at least indirectly, to one or more of the RF sources 106 described above. The other end 209 of the coil 204 may not be electrically connected to anything, such that the coil 204 may be electrically open-ended. The coil 204 may also be electrically isolated from the plasma chamber wall 202 and/or the remainder of the plasma chamber 104. For example, an electrical feedthrough may be employed to connect the coil 204 to the RF source 106 through the chamber wall 202. Such electrical feedthrough) may also be utilized to set the position of the coil 204 within the plasma chamber 104.
  • The conductive member 206 comprises a conductive wire or other material that is positioned between the coil 204 and the plasma chamber wall 202. The conductive member 206 may be positioned substantially parallel to the central axis 204 a of the coil 204 and/or the plasma chamber wall 202. The conductive member 206 may alternatively be omitted, such as where the internal surface of the chamber wall 202, or a portion thereof, performs the function of the conductive member 206. That is, the conductive member 206 may be an alternate ground to the chamber wall 202. For example, if a controlled, reduced plasma is needed, the conductive member 206 may be employed, because it may become difficult to reduce the production of needed radicals with a single coil under certain RF power constraints. Thus, the conductive member 206 may optionally be included to better lower the radical production.
  • The conductive member 206 may substantially comprise aluminum, copper, gold, or alloys thereof, among other compositions. The conductive member 206 may also include an outer coating of dielectric material and/or other materials. The length of the conductive member 206 may range between about 15 mm and about 150 mm, and the thickness or gauge of the wire or other material forming the conductive member 206 may range between about 0.001″ and about 0.25″.
  • One end 212 of the conductive member 206 may be connected, at least indirectly, to a DC or ground potential. The other end 213 of the conductive member 206 may not be electrically connected to anything, such that the conductive member 206 may be electrically open-ended. The conductive member 206 may electrically isolated from the plasma chamber wall 202 and/or the remainder of the plasma chamber 104. For example, an electrical feedthrough may be employed to connect the conductive member 206 to the DC or ground potential 210 through the chamber wall 202. Such electrical feedthrough may also be utilized to set the position of the conductive member 206 within the plasma chamber 104. The conductor may be laterally separated from the outer perimeter of the coil 204 by a distance ranging between about 0.25″ and about 10″, and/or by a distance ranging between about 10% and about 100% of the outer diameter of the coil 204.
  • Referring to FIG. 3, illustrated is a schematic diagram of at least a portion of the plasma chamber 104 shown in FIGS. I and 2 demonstrating one or more aspects of the present disclosure. As in the embodiment shown in FIG. 2, the plasma chamber 104 includes the open-ended coil 204 and the grounded or DC-biased conductive member 206 (shown as being grounded in FIG. 3).
  • In the embodiment illustrated in FIG. 3 the coil 204 includes about 7½ turns. The thickness or gauge of the material utilized to form the coil 204 is described above. The gap between each neighboring pair of turns may range between 0 and about 12 mm. For example, the gap may range between about 0 and about 4 mm. The pitch P may be less than about 150% of the wire thickness. For example, the pitch P may be about 110% of the wire thickness.
  • The radius R of one or more turns of the coil 204 may range between about 5 mm and about 65 mm. In the embodiment illustrated in FIG. 3, each turn of the coil 204 has a substantially similar radius R, although in other embodiments one or more turns of the coil 204 may have a different radius R relative to other turns of the coil 204.
  • Referring to FIG. 4, illustrated is a schematic view of another embodiment of at least a portion of the internal components of the plasma chamber 104 shown in FIGS. 1-3, herein designated by the reference numeral 304. The plasma chamber 304 may be utilized in substantially the same manner as the plasma chamber 104 shown in FIGS. 1-3, and may otherwise be substantially similar in composition, manufacture, and geometry to the plasma chamber 104, except as described below.
  • The plasma chamber 304 includes an outer coil 306 and an inner coil 308. The outer coil 306 may be substantially similar in composition, manufacture, and geometry to the coil 204 described above and shown in FIGS. 2 and 3. For example, the outer coil 306 may include an end 310 that is coupled, at least indirectly, to an RF power source, such as the RF source 106 shown in FIGS. 1 and 2. Another end 311 of the outer coil 306 may be open. The outer coil 306 may have a number of turns ranging between about 4 and about 200, an outer diameter ranging between about 20 mm and about 130 mm, and a length ranging between about 15 mm and about 150 mm, where the gaps between each pair of neighboring turns may range between about 0 and about 12 mm.
  • The inner coil 308 may be positioned substantially coaxially within the outer coil, and may be substantially similar in composition and manufacture to the outer coil 306. The outer diameter of the inner coil 308 may range between about 10 mm and about 100 mm, and its length may range between about 15 mm and about 150 mm. The inner coil 308 may have a number of turns ranging between about 5 and about 500.
  • The ratio of the outer diameter of the outer coil 306 to the outer diameter of the inner coil 308 may range between about 1.1 and about 7. The ratio of the number of turns included in the outer coil 306 to the number of turns included in the inner coil 308 may range between about 1.1 and about 10. The ratio of the length of the outer coil 306 to the length of the inner coil 308 may range between about 1 and about 0.5.
  • An end 312 of the inner coil 308 may be electrically coupled, at least indirectly, to an RF power source, such as the RF power source 106 shown in Figs., and 2, whereas the other end 313 may be open. The outer coil 306 and the inner coil 308 may be connected to the same RF source or to different RF sources, such that each of the coils 306, 308 may be driven independently, and may be driven simultaneously with the same or different RF sources.
  • The ends 311, 313 of the outer and inner coils 306, 308, respectively, may each be electrically open. In embodiments in which both of the outer and inner coils 306, 308 are included within the plasma chamber 304, the conductive member 206 shown in FIGS. 2 and 3 may not be included. However, the plasma chamber 304 itself (such as the plasma chamber wall 202 shown in FIG. 2) may be electrically grounded, whether or not the conductor member 206 is included in the plasma chamber, an whether or not a single coil 204 or dual-coils 206/208 are included in the plasma chamber. The same holds true for the plasma chamber 104 shown in FIGS. 1-3.
  • Referring to FIG. 5, illustrated is a state diagram 500 demonstrating one or more aspects of the present disclosure. The state diagram 500 demonstrates one or more operational aspects of the plasma chamber 104 shown in FIGS. 1 and 2, the apparatus 100 shown in FIG. 1, and/or the coils 204, 304, 306 and 308 shown in FIGS. 1-4.
  • Operation may begin in a START state 502. Operation may then transition to an IGNITION state 504 after, for example, a start-up procedure is executed, among other possible transition-triggering events. The IGNITION state 504 is utilized to ignite a plasma in the plasma chamber (such as the plasma chamber 104 or 304 shown in FIGS. 1-4). For example, an ignition RF power level and an ignition pressure level may be utilized in the IGNITION state 504.
  • Operation may then transition to a STEADY state 506 upon the occurrence of the appropriate transition-triggering event. For example, the plasma chamber may be monitored to detect the presence or level of plasma. If plasma is detected when the IGNITION state 504 is active, operation may transition to the STEADY state 506. Alternatively, or additionally, the IGNITION state 504 may only be operational for a predetermined period of time. Upon the expiration of such time period, operation may transition to the STEADY state 506. For example, the predetermined time period may range between about 5 seconds and about 30 seconds, and may be user selectable and/or preprogrammed by the manufacturer. In an exemplary embodiment, the predetermined time period may be about 10 seconds.
  • The STEADY state 506 is utilized to maintain plasma generation within the plasma chamber. For example, a steady state RF power level and a steady state pressure level may be maintained in the STEADY state 506. The steady state RF power level may be less than the ignition RF power level, whereas the steady state pressure level may be greater than the ignition pressure level. The ignition RF power level may range between about 10 W and about 20 W, whereas the steady state RF power level may range between about 1 W and about 10 W. The ignition pressure level may range between about 10 mT and about 600 mT, whereas the steady state pressure level may range between about 300 mT and about 1000 mT. The steady state RF power and pressure levels may be configured such that oxygen radicals and/or other radicals are generated in the plasma chamber, such that the radicals may feed into the vacuum chamber for cleaning and/or other purposes.
  • Operation in the STEADY state 506 may continue until the occurrence of the appropriate transition-triggering event. For example, one such event may be when the plasma source gas is altered, such as by switching between the first and second gas supplies 122, 124 shown in FIG. 1, or by altering the composition of a mixture of gas being delivered from the first and second gas supplies simultaneously. Either of such events, among others, may trigger operation to transition back to the IGNITION state 504. Another exemplary event that may trigger the transition from the STEADY state 506 to the IGNITION state 504 is the detection of plasma in the plasma chamber dropping below a threshold concentration, or the lack of plasma existence in the plasma chamber. In either case, operation transitions back to the IGNITION state 504 so that plasma ignition can be repeated, at which time operation may once again transition to the STEADY state 506. Operation may also transition from the STEADY state 506 to a STOP state 508 upon the occurrence of the appropriate transition-triggering event, such as the receipt of user-input indicating that operation is to be halted.
  • Referring to FIGS. 6A-6D, illustrated are various embodiments of methods operable in conjunction with the apparatus described above and shown in FIGS. 1-5. In FIG. 6A, method 600 a includes a step 602 in which a plasma is ignited, as described above. After the plasma is ignited, the plasma chamber pressure is increased in a step 604 to a steady state plasma generation chamber pressure. The plasma generation is then maintained during a step 606 until, as determined by decisional step 608, plasma is no longer detected. That is, if plasma is continually detected during step 608, then the step 606 is repeated. However, if it is determined during decisional step 608 that plasma is no longer detected, or that plasma concentration has dropped below a threshold value, then the pressure is decreased in a step 610, and step 602 is repeated to re-ignite the plasma.
  • In FIG. 6B, method 600 b includes step 602 in which plasma is ignited, as described above. After the plasma is ignited, the RF power is decreased in a step 605 to a steady state plasma generation RF power. The plasma generation is then maintained during step 606 until, as determined by decisional step 608, plasma is no longer detected. That is, if plasma is continually detected during step 608, then the step 606 is repeated. However, if it is determined during decisional step 608 that plasma is no longer detected, or that plasma concentration has dropped below a threshold value, then the RF power is increased in a step 611, and step 602 is repeated to re-ignite the plasma.
  • In FIG. 6C, method 600 c includes step 602 in which plasma is ignited, as described above. After the plasma is ignited, the RF power is decreased to a steady state plasma generation RF power, and the plasma chamber pressure is increased to a steady state plasma generation chamber pressure, in a step 620. The plasma generation is then maintained during step 606 until, as determined by decisional step 608, plasma is no longer detected. That is, if plasma is continually detected during step 608, then the step 606 is repeated. However, if it is determined during decisional step 608 that plasma is no longer detected, or that plasma concentration has dropped below a threshold value, then the RF power is increased and the chamber pressure is decreased in a step 622, and step 602 is repeated to re-ignite the plasma.
  • In FIG. 6D, method 600 d includes step 602 in which plasma is ignited, as described above. After plasma ignition is attempted, decisional step 608 a is performed determine whether plasma has successfully been ignited. If plasma has not been ignited, or if plasma concentration is not at an acceptable level, then the RF power is increased and the plasma chamber pressure is decreased in step 622. Plasma ignition is then attempted again in step 602. This iterative process may be repeated until plasma is significantly ignited, and perhaps generated to at least a predetermined concentration, as determined by decisional step 608 a.
  • Once plasma has been adequately ignited, as determined by decisional step 608 a, the RF power is decreased and the plasma chamber pressure is increased in step 620. Thereafter, plasma is maintained in step 606. However, the plasma concentration level may be periodically, continuously, or otherwise monitored. If sufficient plasma is detected, as determined by decisional step 608 b, then step 606 is repeated and the plasma generation is maintained. However, if sufficient plasma is not detected, as determined by decisional step 608 b, then the RF power is increased and the plasma chamber pressure is decreased as step 622 is repeated, and then plasma re-ignition is attempted as step 602 is repeated.
  • In each of the above-described methods 600 a-600 d, and others within the scope of the present disclosure, the plasma chamber pressure during plasma ignition and/or plasma generation (steady state) may range between about 10 mT and about 10 T. In an exemplary embodiment, the plasma chamber pressure during plasma ignition is about 100 mT and the plasma chamber pressure during steady state plasma generation is about 600 mT, or the plasma chamber pressure during steady state plasma generation may be about 600% greater than the plasma chamber pressure during plasma ignition.
  • Additionally, in each of the above-described methods 600 a-600 d, and others within the scope of the present disclosure, the RF power during plasma ignition and/or plasma generation (steady state) may range between about 5 W and about 20 W. In an exemplary embodiment, the RF power during plasma ignition is about 20 W and the RF power during steady state plasma generation is about 10 W, or the RF power during steady state may otherwise be about 50% less than the RF power during the plasma ignition.
  • Moreover, in each of the above-described methods 600 a-600 d, and others within the scope of the present disclosure, the RE frequency during plasma ignition and/or plasma generation (steady state) may range between about 1 MHz and about 1 GHz. In an exemplary embodiment, the RF frequency during plasma ignition and steady state plasma generation is about 13.56 MHz.
  • It should be evident from the description above that the present disclosure introduces an apparatus comprising a plasma chamber, a radio frequency (RF) power source, and a coil centrally disposed in the plasma chamber. The plasma chamber is configured to generate plasma that feeds a vacuum chamber adjacent the plasma chamber, and a first end of the coil is electrically coupled to the RF power source while a second end of the coil is electrically open.
  • A method of manufacturing an apparatus is also introduced in the present disclosure, and includes disposing a coil centrally in a plasma chamber; wherein a first end of the coil is electrically open, and wherein the plasma chamber is configured to generate plasma that feeds into a vacuum chamber adjacent the plasma chamber. A radio frequency (RF) power source is then coupled to a second end of the coil.
  • Additional apparatus introduced in the present disclosure comprises a vacuum chamber, an emitter configured to emit a beam of at least one of ions and electrons into the vacuum chamber, and a plasma chamber coupled to the vacuum chamber. Such apparatus also includes means for supplying a plasma source gas into the plasma chamber, a radio frequency (RF) power source, and a coil located in a substantially central portion of the plasma chamber, wherein a first end of the coil is electrically coupled to the RF power source and a second end of the coil is electrically open.
  • Also introduced in the present disclosure is a method of operating a plasma chamber for use with an electron or ion beam apparatus The method may comprise igniting a plasma in the plasma chamber by utilizing a first radio frequency (RF) power and a first plasma chamber pressure. The plasma may then be maintained by utilizing a second RF power and a second plasma chamber pressure, wherein the second RF power is substantially less than the first RF power and the second plasma chamber pressure is substantially greater than the first plasma chamber pressure.
  • Another method introduced in the present disclosure comprises transitioning a plasma chamber to a steady state when a first event occurs, and transitioning the chamber to an ignition state when a second event occurs. In such a method, the ignition state employs a greater RF power than the steady state, and the steady state employs a greater chamber pressure than the ignition state.
  • A system introduced in the present disclosure comprises a plasma chamber, a radio frequency (RF) power source coupled to a magnetic plasma igniting means that is disposed within the plasma chamber, and a controller configured to operate the plasma chamber and the RF power source in an ignition state and a steady state, including increasing the plasma chamber's pressure and decreasing the RF power source's output when transitioning from the ignition state to the steady state.
  • The foregoing outlines features of several embodiments so that those skilled in the art may better understand the aspects of the present disclosure. Those skilled in the art should appreciate that they may readily use the present disclosure as a basis for designing or modifying other processes and structures for carrying out the same purposes and/or achieving the same advantages of the embodiments introduced herein. Those skilled in the art should also realize that such equivalent constructions do not depart from the spirit and scope of the present disclosure, and that they may make various changes, substitutions and alterations herein without departing from the spirit and scope of the present disclosure.

Claims (46)

1. An apparatus, comprising:
a plasma chamber configured to generate plasma that feeds a vacuum chamber adjacent the plasma chamber;
a radio frequency (RF) power source; and
a coil centrally disposed in the plasma chamber, wherein a first end of the coil is electrically coupled to the RF power source and a second end of the coil is electrically open.
2. The apparatus of claim 1 further comprising a conductor disposed between the coil's outer perimeter and an inner wall of the plasma chamber wherein the conductor is substantially parallel to a central axis of the coil and laterally separated from the coil's outer perimeter, and wherein the conductor is electrically biased at a predetermined potential.
3. The apparatus of claim 2 wherein the conductor is electrically grounded.
4. The apparatus of claim 2 wherein the conductor is laterally separated from the coil's outer perimeter by a distance ranging between about 0.25″ and about 10″.
5. The apparatus of claim 2 wherein the conductor is laterally separated from the coil's outer perimeter by a distance ranging between about 10% of the coil's outer diameter and about 100% of the coil's outer diameter.
6. The apparatus of claim 1 wherein the coil has a number of turns ranging between about 4 and about 200.
7. The apparatus of claim 1 wherein the coil has a wire thickness and a pitch, wherein the pitch is less than about 150% of the wire thiclkness.
8. The apparatus of claim 7 wherein the pitch is about 110% of the wire thickness.
9. The apparatus of claim 1 wherein the coil has a wire thickness ranging between about 0.001″ and about 0.25″.
10. The apparatus of claim 1 wherein the coil substantially comprises aluminum.
11. The apparatus of claim 1 wherein the RF power source is a first RF power source and the coil is a first coil, the apparatus further comprising:
a second RF power source; and
a second coil smaller in diameter than the first coil and centrally disposed within the first coil's inner diameter, wherein a first end of the second coil is electrically coupled to the second RF power source and a second end of the second coil is electrically open.
12. The apparatus of claim 1 further comprising:
a gas inlet coupled to the plasma chamber and configured to allow flow of a plasma source gas into the plasma chamber; and
a feedthrough coupled to one of the plasma chamber and the vacuum chamber, through which an RF signal from the RF power source external to the plasma and vacuum chambers is deliverable to the coil inside the plasma chamber through at least one electrical conductor extending between the feedthrough and the coil.
13. The apparatus of claim 1 further comprising the vacuum chamber.
14. The apparatus of claim 13 wherein the apparatus is an electron microscope.
15. The apparatus of claim 13 wherein the apparatus is a scanning electron microscope (SEM).
16. A method of manufacturing an apparatus, comprising:
disposing a coil centrally in a plasma chamber, wherein a first end of the coil is electrically open, and wherein the plasma chamber is configured to generate plasma that feeds into a vacuum chamber adjacent the plasma chamber; and
coupling a radio frequency (RF) power source to a second end of the coil.
17. The method of claim 16 further comprising disposing a conductor between the coil's outer perimeter and an inner wall of the plasma chamber, such that the conductor is substantially parallel to a central axis of the coil and laterally separated from the coil's outer perimeter, and wherein the conductor is configured to be electrically biased at a predetermined potential.
18. The method of claim 17 wherein the conductor is electrically grounded.
19. The method of claim 17 wherein the disposed conductor is laterally separated from the coil's outer perimeter by a distance ranging between about 0.25″ and about 10″.
20. The method of claim 17 wherein the disposed conductor is laterally separated from the coil's outer perimeter by a distance ranging between about 10% of the coil's outer diameter and about 100% of the coil's outer diameter.
21. The method of claim 16 wherein the coil has a number of turns ranging between about 4 and about 200.
22. The method of claim 16 wherein the coil has a wire thickness and a pitch, wherein the pitch is less than about 150% of the wire thickness.
23. The method of claim 22 wherein the pitch is about 110% of the wire thickness.
24. The method of claim 16 wherein the coil has a wire thickness ranging between about 0.001″ and about 0.25″.
25. The method of claim 16 wherein the coil substantially comprises aluminum.
26. The method of claim 16 wherein the RF power source is a first RF power source and the coil is a first coil, the method further comprising:
disposing a second coil centrally within the first coil's inner diameter, wherein the second coil is smaller in diameter than the first coil and a first end of the second coil is electrically open; and
coupling a second RF power source to a second end of the second coil.
27. The method of claim 16 further comprising:
establishing an electrical connection between the coil and a feedthrough coupled to one of the plasma chamber and the vacuum chamber, such that an RF signal from the RF power source external to the plasma and vacuum chambers is deliverable to the coil inside the plasma chamber.
28. The method of claim 16 further comprising coupling the plasma chamber to the vacuum chamber.
29. The method of claim 16 wherein the apparatus is an electron microscope.
30. The method of claim 16 wherein the apparatus is a scanning electron microscope (SEM).
31. An apparatus, comprising:
a vacuum chamber;
an emitter configured to emit a beam of at least one of ions and electrons into the vacuum chamber;
a plasma chamber coupled to the vacuum chamber;
means for supplying a plasma source gas into the plasma chamber;
a radio frequency (RF) power source; and
a coil located in a substantially central portion of the plasma chamber, wherein a first end of the coil is electrically coupled to the RF power source and a second end of the coil is electrically open.
32. The apparatus of claim 31 wherein the plasma source gas supplying means includes a flow controller configured to regulate pressure inside the plasma chamber.
33. The apparatus of claim 31 wherein the plasma source gas supplying means includes a valve configured to select between a plurality of different plasma source gas supplies.
34. The apparatus of claim 31 wherein the emitter includes a column configured to provide at least one of focusing and steering of the beam before the beam enters the vacuum chamber.
35. The apparatus of claim 31 further comprising a conductor disposed between the coil's outer perimeter and an inner wall of the plasma chamber, wherein the conductor is substantially parallel to a central axis of the coil and laterally separated from the coil's outer perimeter, and wherein the conductor is electrically biased at a predetermined potential.
36. The apparatus of claim 35 wherein the conductor is electrically grounded.
37. The apparatus of claim 35 wherein the conductor is laterally separated from the coil's outer perimeter by a distance ranging between about 0.25″ and about 10″.
38. The apparatus of claim 35 wherein the conductor is laterally separated from the coil's outer perimeter by a distance ranging between about 10% of the coil's outer diameter and about 100% of the coil's outer diameter.
39. The apparatus of claim 31 wherein the coil has a number of turns ranging between about 4 and about 200.
40. The apparatus of claim 31 wherein the coil has a wire thickness and a pitch, wherein the pitch is less than about 150% of the wire thiciness.
41. The apparatus of claim 40 wherein the pitch is about 110% of the wire thickness.
42. The apparatus of claim 31 wherein the coil has a wire thickness ranging between about 0.001″ and about 0.25″.
43. The apparatus of claim 31 wherein the coil substantially comprises aluminum.
44. The apparatus of claim 31 wherein the RF power source is a first RF power source and the coil is a first coil, the apparatus further comprising:
a second RF power source; and
a second coil centrally located within the first coil, wherein a first end of the second coil is electrically coupled to the second RF power source and a second end of the second coil is electrically open.
45. The apparatus of claim 31 wherein the apparatus is an electron microscope.
46. The apparatus of claim 31 wherein the apparatus is a scanning electron microscope (SEM).
US11/537,460 2006-09-29 2006-09-29 RF Coil Plasma Generation Abandoned US20080078506A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US11/537,460 US20080078506A1 (en) 2006-09-29 2006-09-29 RF Coil Plasma Generation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US11/537,460 US20080078506A1 (en) 2006-09-29 2006-09-29 RF Coil Plasma Generation

Publications (1)

Publication Number Publication Date
US20080078506A1 true US20080078506A1 (en) 2008-04-03

Family

ID=39272845

Family Applications (1)

Application Number Title Priority Date Filing Date
US11/537,460 Abandoned US20080078506A1 (en) 2006-09-29 2006-09-29 RF Coil Plasma Generation

Country Status (1)

Country Link
US (1) US20080078506A1 (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080087841A1 (en) * 2006-10-17 2008-04-17 Zyvex Corporation On-chip reflectron and ion optics
EP2482304A1 (en) * 2011-01-26 2012-08-01 Ping-Li Lai Plasma Reaction Method and Plasma Reaction Device
US20130256266A1 (en) * 2012-03-30 2013-10-03 Andreas Fischer Methods and apparatuses for effectively reducing gas residence time in a plasma processing chamber
US20160163519A1 (en) * 2013-10-08 2016-06-09 XEI Scientic, Inc. Method and apparatus for plasma ignition in high vacuum chambers
US9551743B2 (en) 2006-07-18 2017-01-24 Dcg Systems, Inc. Apparatus and method for combined micro-scale and nano-scale C-V, Q-V, and I-V testing of semiconductor materials
US9891280B2 (en) 2013-06-24 2018-02-13 Fei Efa, Inc. Probe-based data collection system with adaptive mode of probing controlled by local sample properties
CN109030404A (en) * 2018-08-24 2018-12-18 代广斌 A kind of scattering formula Terahertz near-field microscope based on radio-frequency electronics method
US10290469B2 (en) * 2013-06-17 2019-05-14 Applied Materials, Inc. Enhanced plasma source for a plasma reactor
US10539589B2 (en) 2014-06-25 2020-01-21 Fei Efa, Inc. Through process flow intra-chip and inter-chip electrical analysis and process control using in-line nanoprobing

Citations (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2782682A (en) * 1953-05-29 1957-02-26 Browning Iben Micromanipulators
US4610475A (en) * 1984-09-06 1986-09-09 Microflex Technology, Inc. Piezoelectric polymer micromanipulator
US4850779A (en) * 1985-02-15 1989-07-25 Tekscan Limited Manipulator for handling objects within a sealed chamber
US4982140A (en) * 1989-10-05 1991-01-01 General Electric Company Starting aid for an electrodeless high intensity discharge lamp
US5036252A (en) * 1988-04-26 1991-07-30 Hauzer Holding Bv Radio frequency ion beam source
US5270552A (en) * 1991-08-22 1993-12-14 Hitachi, Ltd. Method for separating specimen and method for analyzing the specimen separated by the specimen separating method
US5332275A (en) * 1991-11-27 1994-07-26 Microscience Group, Inc. Microgripper
US5338997A (en) * 1988-04-29 1994-08-16 Fraunhofer Gesellschaft Zur Foerderung Der Angewandten Forschung E.V. Micromanipulator for moving objects
US5571366A (en) * 1993-10-20 1996-11-05 Tokyo Electron Limited Plasma processing apparatus
US5683537A (en) * 1993-10-04 1997-11-04 Tokyo Electron Limited Plasma processing apparatus
US5685942A (en) * 1994-12-05 1997-11-11 Tokyo Electron Limited Plasma processing apparatus and method
US5727915A (en) * 1995-03-29 1998-03-17 Nikon Corporation Master input apparatus for microgripper and microgripper system provided with the master input apparatus
US5795429A (en) * 1993-01-12 1998-08-18 Tokyo Electron Limited Plasma processing apparatus
US5895084A (en) * 1997-02-19 1999-04-20 Mauro; George Cam operated microgripper
US6105589A (en) * 1999-01-11 2000-08-22 Vane; Ronald A. Oxidative cleaning method and apparatus for electron microscopes using an air plasma as an oxygen radical source
US6116187A (en) * 1998-05-22 2000-09-12 Nissin Electric Co., Ltd. Thin film forming apparatus
US6420722B2 (en) * 2000-05-22 2002-07-16 Omniprobe, Inc. Method for sample separation and lift-out with one cut
US6452315B1 (en) * 2000-02-08 2002-09-17 Ronald A. Vane Compact RF plasma device for cleaning electron microscopes and vacuum chambers
US6576900B2 (en) * 2000-05-19 2003-06-10 Imago Scientific Instruments Methods of sampling specimens for microanalysis
US6610257B2 (en) * 1999-01-11 2003-08-26 Ronald A. Vane Low RF power electrode for plasma generation of oxygen radicals from air
US6664552B2 (en) * 2000-11-06 2003-12-16 Hitachi, Ltd. Method and apparatus for specimen fabrication
US20040009669A1 (en) * 2002-07-10 2004-01-15 Nec Electronics Corporation Method of removing polymer and apparatus for doing the same
US6777674B2 (en) * 2002-09-23 2004-08-17 Omniprobe, Inc. Method for manipulating microscopic particles and analyzing
US20050183667A1 (en) * 2004-02-20 2005-08-25 John Keller Magnetically enhanced, inductively coupled plasma source for a focused ion beam system

Patent Citations (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2782682A (en) * 1953-05-29 1957-02-26 Browning Iben Micromanipulators
US4610475A (en) * 1984-09-06 1986-09-09 Microflex Technology, Inc. Piezoelectric polymer micromanipulator
US4850779A (en) * 1985-02-15 1989-07-25 Tekscan Limited Manipulator for handling objects within a sealed chamber
US5036252A (en) * 1988-04-26 1991-07-30 Hauzer Holding Bv Radio frequency ion beam source
US5338997A (en) * 1988-04-29 1994-08-16 Fraunhofer Gesellschaft Zur Foerderung Der Angewandten Forschung E.V. Micromanipulator for moving objects
US4982140A (en) * 1989-10-05 1991-01-01 General Electric Company Starting aid for an electrodeless high intensity discharge lamp
US5270552A (en) * 1991-08-22 1993-12-14 Hitachi, Ltd. Method for separating specimen and method for analyzing the specimen separated by the specimen separating method
US5332275A (en) * 1991-11-27 1994-07-26 Microscience Group, Inc. Microgripper
US5795429A (en) * 1993-01-12 1998-08-18 Tokyo Electron Limited Plasma processing apparatus
US5683537A (en) * 1993-10-04 1997-11-04 Tokyo Electron Limited Plasma processing apparatus
US5571366A (en) * 1993-10-20 1996-11-05 Tokyo Electron Limited Plasma processing apparatus
US5685942A (en) * 1994-12-05 1997-11-11 Tokyo Electron Limited Plasma processing apparatus and method
US5727915A (en) * 1995-03-29 1998-03-17 Nikon Corporation Master input apparatus for microgripper and microgripper system provided with the master input apparatus
US5895084A (en) * 1997-02-19 1999-04-20 Mauro; George Cam operated microgripper
US6116187A (en) * 1998-05-22 2000-09-12 Nissin Electric Co., Ltd. Thin film forming apparatus
US6105589A (en) * 1999-01-11 2000-08-22 Vane; Ronald A. Oxidative cleaning method and apparatus for electron microscopes using an air plasma as an oxygen radical source
US6610257B2 (en) * 1999-01-11 2003-08-26 Ronald A. Vane Low RF power electrode for plasma generation of oxygen radicals from air
US6452315B1 (en) * 2000-02-08 2002-09-17 Ronald A. Vane Compact RF plasma device for cleaning electron microscopes and vacuum chambers
US6576900B2 (en) * 2000-05-19 2003-06-10 Imago Scientific Instruments Methods of sampling specimens for microanalysis
US6420722B2 (en) * 2000-05-22 2002-07-16 Omniprobe, Inc. Method for sample separation and lift-out with one cut
US6664552B2 (en) * 2000-11-06 2003-12-16 Hitachi, Ltd. Method and apparatus for specimen fabrication
US20040009669A1 (en) * 2002-07-10 2004-01-15 Nec Electronics Corporation Method of removing polymer and apparatus for doing the same
US6777674B2 (en) * 2002-09-23 2004-08-17 Omniprobe, Inc. Method for manipulating microscopic particles and analyzing
US20050183667A1 (en) * 2004-02-20 2005-08-25 John Keller Magnetically enhanced, inductively coupled plasma source for a focused ion beam system

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9551743B2 (en) 2006-07-18 2017-01-24 Dcg Systems, Inc. Apparatus and method for combined micro-scale and nano-scale C-V, Q-V, and I-V testing of semiconductor materials
US20080087841A1 (en) * 2006-10-17 2008-04-17 Zyvex Corporation On-chip reflectron and ion optics
US7605377B2 (en) * 2006-10-17 2009-10-20 Zyvex Corporation On-chip reflectron and ion optics
EP2482304A1 (en) * 2011-01-26 2012-08-01 Ping-Li Lai Plasma Reaction Method and Plasma Reaction Device
CN102625562A (en) * 2011-01-26 2012-08-01 赖秉豊 Plasma reaction method and apparatus
US9299541B2 (en) * 2012-03-30 2016-03-29 Lam Research Corporation Methods and apparatuses for effectively reducing gas residence time in a plasma processing chamber
KR20140140627A (en) * 2012-03-30 2014-12-09 램 리써치 코포레이션 Methods and apparatuses for effectively reducing gas residence time in a plasma processing chamber
US20130256266A1 (en) * 2012-03-30 2013-10-03 Andreas Fischer Methods and apparatuses for effectively reducing gas residence time in a plasma processing chamber
KR102065803B1 (en) 2012-03-30 2020-02-11 램 리써치 코포레이션 Methods and apparatuses for effectively reducing gas residence time in a plasma processing chamber
US10290469B2 (en) * 2013-06-17 2019-05-14 Applied Materials, Inc. Enhanced plasma source for a plasma reactor
US9891280B2 (en) 2013-06-24 2018-02-13 Fei Efa, Inc. Probe-based data collection system with adaptive mode of probing controlled by local sample properties
US20160163519A1 (en) * 2013-10-08 2016-06-09 XEI Scientic, Inc. Method and apparatus for plasma ignition in high vacuum chambers
US10539589B2 (en) 2014-06-25 2020-01-21 Fei Efa, Inc. Through process flow intra-chip and inter-chip electrical analysis and process control using in-line nanoprobing
CN109030404A (en) * 2018-08-24 2018-12-18 代广斌 A kind of scattering formula Terahertz near-field microscope based on radio-frequency electronics method

Similar Documents

Publication Publication Date Title
US20080078506A1 (en) RF Coil Plasma Generation
US20080078745A1 (en) RF Coil Plasma Generation
US11658011B2 (en) Plasma processing apparatus
US6796269B2 (en) Apparatus and method for monitoring plasma processing apparatus
US9362131B2 (en) Fast atomic layer etch process using an electron beam
US6774570B2 (en) RF plasma processing method and RF plasma processing system
KR100337718B1 (en) Method of injecting semiconductor wafer ions, non-raster injection device, method of injecting into semiconductor wafer with surface, and workpiece processing method and device
CN101800161B (en) Plasma etching method and plasma etching apparatus
US8298433B2 (en) Methods for removing an edge polymer from a substrate
JPH09251935A (en) Plasma igniter, semiconductor producing apparatus using plasma and plasma igniting method for semiconductor device
KR101026459B1 (en) An ignition apparatus for atmospheric plasma and an ignition method using the same
JP2009504393A (en) Microwave plasma reactor
KR100733844B1 (en) Plasma generating apparatus using neutral beam and plasma generating method
JP2005276618A (en) Device and method for generating microplasma
JP6499754B2 (en) Ion milling apparatus and ion milling method
JP2008536012A (en) Device for plasma and / or coating treatment of workpieces
US8703249B2 (en) Techniques for reducing arcing-related damage in a clamping ring of a plasma processing system
JPWO2019012906A1 (en) Plasma generator, emission spectrometer and mass spectrometer equipped with the same, and apparatus state determination method
US11501976B2 (en) Substrate processing method and substrate processing apparatus
KR101568722B1 (en) Plasma reactor and control method thereof
TWI775166B (en) Plasma processing apparatus and method for processing substrates
JP4324541B2 (en) Plasma processing equipment
JPH07105893A (en) Ion beam treating device, and method for working it
JP2008130430A (en) High-frequency ionization source
JP2006100630A (en) Apparatus and method of plasma processing

Legal Events

Date Code Title Description
AS Assignment

Owner name: ZYVEX CORPORATION, TEXAS

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:VERBECK, GUIDO FRIDOLIN, IV;CORDELL, ANDREW;REEL/FRAME:018526/0275;SIGNING DATES FROM 20061019 TO 20061020

AS Assignment

Owner name: ZYVEX INSTRUMENTS, LLC, TEXAS

Free format text: NUNC PRO TUNC ASSIGNMENT;ASSIGNOR:ZYVEX CORPORATION;REEL/FRAME:019353/0363

Effective date: 20070521

AS Assignment

Owner name: DCG SYSTEMS, INC.,CALIFORNIA

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:ZYVEX INSTRUMENTS, LLC;REEL/FRAME:024338/0893

Effective date: 20100211

STCB Information on status: application discontinuation

Free format text: ABANDONED -- FAILURE TO RESPOND TO AN OFFICE ACTION