US3575383A - Ultrasonic cleaning system, apparatus and method therefor - Google Patents

Ultrasonic cleaning system, apparatus and method therefor Download PDF

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US3575383A
US3575383A US790764A US3575383DA US3575383A US 3575383 A US3575383 A US 3575383A US 790764 A US790764 A US 790764A US 3575383D A US3575383D A US 3575383DA US 3575383 A US3575383 A US 3575383A
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base
transducer
stud
receptacle
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/10Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
    • B08B3/12Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations

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  • one transducer fails, it must be removed from the tank by heating the bond around that particular transducer and replaced with a new transducer assembly.
  • the heating of the tank and bond around the defective transducer tends to damage the bonds on other surrounding transducer units.
  • one transducer unit is to be replaced several more than that must also be replaced and rebonded.
  • the application of heat to initially bond the unit to a liquid containing tank must be limited in order not to damage the actual vibratory transducer elements contained in the transducer unit. As a consequence the initial bond may be unsatisfactory. With the use of a higher melting point bonding compound, a more durable bond results. This is especially necessary in an ultrasonic cleaning system where the vibrator tends to loosen a bond and where heat generated by the cleaning process will also loosen bonds.
  • an ultrasonic system having receptacle means for retaining liquid which is agitated ultrasonically.
  • Such a system comprises a plurality of transducer means for converting electrical energy to mechanical vibratory energy each including a base integrally mounted on the receptacle.
  • a transducer element mechanically coupled to said base is included in the transducer means and has terminal means for coupling to a source of electrical energy.
  • the transducer means also includes fastener means for coupling the transducer means to the base, the fastener means having a portion thereof removable to allow the transducer element to be replaced and a new transducer element recoupled to the base.
  • a source of electrical energy including a plurality of oscillator means is provided each of the oscillator means being mounted in separate plug-in units associated respectively with each of the transducer means. Each of the oscillator means are coupled to respective terminals of the transducer means.
  • FIG. I is a cross-sectional of a tank of an ultrasonic cleaning system showing transducer units attached thereto;
  • FIG. 2 is a bottom view in schematic form of the tank of FIG. I and also includes a diagrammatic showing of the electrical energy sources supplying energy to the transducer units;
  • FIG. 2A is a cross-sectional view taken along the lines 2A-2A of FIG. 2;
  • FIG. 3 is an enlarged cross-sectional view showing one of the transducer units mounted to the tank of FIG. I;
  • FIG. 4 is a circuit schematic of an electrical energy source for one of the transducer units.
  • FIG. I there is illustrated a receptacle I0 containing suitable cleaning liquid II which has mounted on its bottom plate I4 eight identical transducer units 12.
  • FIG. 3 shows one of the units in detail which includes a cylindrical base III which is heat bonded to bottom plate 14 by either welding or epoxy glue.
  • Base 13 would normally be composed of a suitable metal such as aluminum.
  • Two annularly shaped piezoelectric type crystals 16 and 17 are coupled to base 13 by means of a tapered stud 15 which is screwed into a threaded receptacle I9 in the center of base 13.
  • a nut 18 on stud 15 causes a compression plate Zll to compress elements 16 and I7 together and against base 13.
  • stud I5 is screwed into receptacle 19 with a much greater torque than nut I8.
  • stud I5 may have applied to it more than 200 inch-pounds of torque while in the case of nut IS a maximum of l20-l40 inch-pounds is applied. This differential allows nut 18 to be removed while stud I5 remains in place.
  • stud I5 is threaded into base 13 before the base is bonded to receptacle I0. This allows a torque force to be used on the stud which is much greater than the relative bonding force.
  • each transducer element I6 and I7 also includes collars 16a and 17a to prevent any short circuit by stud IS.
  • a stud I5, as is apparent, in conjunction with compression plate 21 and nut I8 serve as a fastener for the transducer elements 16 and 17. Since nut 18 was applied to the stud with a lower torque it may be easily removed allowing any defective transducer elements 16 and I7 to be removed and replaced with a working element.
  • the method of providing an ultrasonic cleaning system in accordance with the invention comprises the following steps.
  • Base I3 with its stud I5 inserted and torqued down to the desired tension is bonded to bottom plate 14.
  • the bonding process is carried out in compliance with the manufacturers instructions of the bonding compound used.
  • the base during bonding is loaded with sufficient weight to force out all air bubbles and allowed to set cold. Thereafter it is heated above the Curie point of crystals I6 and 17. With this high temperature maximum strength and adhesive force are achieved.
  • the Curie point or rating of a crystal is the temperature at which the crystal begins to lose its power rating. Once heated to this temperature the crystal permanently loses at least a portion of the rating. Thus, the crystals 16 and 17 are not placed on base 13 until the base has cooled to room temperature.
  • Crystals l6 and 17 are mechanically coupled to base 12 by tightening nut 18 on stud 15.
  • the nut is torqued to a value determined by the manufacturers specifications. For example, a crystal available from Channell Industries of Santa Barbara, California, has a free frequency of 160 kHz. This frequency is reduced to a desired 20 kHz by a torque pressure of l20l40 inch-pounds. Spot checks however should be made with an oscilloscope to verify the manufacturers specifications.
  • Each plug-in unit 27 includes an oscillator means as shown in FIG. 4 which has a transformer T to which is supplied a source of AC voltage which may, for example, be 1 l volts, ()0 hertz. This is coupled into a bridge circuit which includes diodes D1, D2. The center tap of the bridge is coupled between two identical halves of an inductance designated L2, L2. Transistors Q] and Q2 provide a push-pull oscillation circuit with feedback being provided by winding Ll through the phase shift capacitor C l. Resistors R1 and R2 couple the bases of transistors Q1 and O2 to diodes D1 and D2 and resistors R3 and R4 couple to the bases to the center tap of the bridge.
  • Output winding L3 is coupled to Ll and L2 which provides the necessary high frequency oscillatory voltage which is applied to the transducer units 12.
  • a light source 28 is mounted in parallel with a series resistor 29 to indicate an open circuit in the transducer element. This is the normal failure mode of a piezoelectric transducer element.
  • Plug-in units 27 include male and female connectors 31 (H6. 2A) which allow for easy replacement upon failure of either the current and/or associated transducer units.
  • the present invention provides an improved ultrasonic cleaning system, apparatus and method therefore in which the transducer units are easily repaired by simple removal of the nut 18. At the same time if one of the units fails, only a portion of the associated electrical power source is affected and these are also easily replaced.
  • An ultrasonic cleaning system having receptacle means for retaining liquid which is agitated ultrasonically comprising, a plurality of transducer means for converting electrical energy to mechanical vibratory energy each including a base integrally mounted on said receptacle, a transducer element mechanically coupled to said base and having terminal means for coupling to a source of electrical energy, fastener means for coupling said transducer element to said base said fastener means having a portion thereof removable to allow said transducer element to be replaced said portion being reusable to recouple a transducer element to said base, and a source of electrical energy including a plurality of separate oscillator means each mounted in separate plug-in units associated respectively with each of said transducer means, each of said oscillator means being coupled to respective terminals of said transducer means.
  • each of said oscillator means includes indicator means for indicating a malfunction of such oscillator or associated transducer means.
  • Ultrasonic cleaning apparatus comprising, a base having a relatively substantial mass and a predetermined depth, a transducer element mechanically coupled to said base and having terminal means for coupling to a source of electrical energy, fastener means for coupling said transducer element to said base including a threaded stud having one end screwed into said base less than one-half said depth by application of a predetermined torque said fastener means including a pressure plate which in conjunction with said base forms a sandwich construction with said transducer element there between said stud extending through apertures in said transducer element and pressure plate and including nut means screwed onto the other end of said stud by application of a torque less than said predetermined torque to mechanically couple said transducer element to said base.
  • a method of providing an ultrasonic cleaning system having receptacle means for retaining liquid which is agitated ultrasonically and having a transducer unit with a base to which is coupled an annular transducer element by a threaded stud, pressure plate and nut comprising the steps of, providing a threaded receptacle in said base, screwing said stud into said threaded receptacle by application of a predetermined torque, thereafter bonding said base to said receptacle means, placing said annular transducer element on said base with said stud extending therethrough, mechanically coupling said element to said base by placing said pressure plate on said element and said nut on said stud and applying a torque to said nut less than said predetermined torque.

Abstract

An ultrasonic cleaning system in which at least one transducer unit includes a base bonded to the bottom of a cleaning tank each unit including a stud on which are placed two annular transducer elements, a pressure plate, and a nut. The stud is firmly fixed by tapered threads to the base so that removal of the compression nut does not disturb the stud but allows replacement of defective transducer elements. Pairs of the transducer units are associated with a single plug-in oscillator unit which supplied high frequency vibratory energy to it.

Description

United States Patent [72] Inventor John A. Coleman 1065 Bush St., San Francisco, Calif. 94109 [21] Appl. No. 790,764 122] Filed Jan. 13, 1969 [451 Patented Apr. 20, 1971 [54] ULTRASONIC CLEANING SYSTEM, APPARATUS AND METHOD THEREFOR 9 Claims, 5 Drawing Figs.
[52] US. Cl 259/72, 259/1, 134/184 [51] Int. Cl B0lf 11/02, B06b 3/00, B08b 3/10 [50] Field of Search 259/72, (Vibisonic Digest & 3), 1; 134/184, 1
[56] References Cited UNITED STATES PATENTS 3,085,185 4/1963 Jacke et a1. 259/1X 3,094,314 6/1963 Kearney et a1 259/72 3,117.768 1/1964 Carlin 3,329,408 7/1967 Branson 259/ 72 3,370,186 2/1968 Antonevicm 259/1X 3,371,233 2/1968 Cook 259/1X 3,443,797 5/1969 Branson 259/ 72 I FOREIGN PATENTS 1,543,552 9/1968 France 259/72 Primary Examiner-James Kee Chi Att0rneyFlehr, Hohbach, Test, Albritton and Herbert Patentel April 20, 1971 3,575,383
TO TRANS- DUCERS D2 mvsmoa JOHN A. COLEMAN BY 44 W01;
M FIG.4 m
ATTORNEYS ULTRASONIC CLEANING SYSTEM, APPARATUS AND METHOD 'llll-IIERIEIFOII BACKGROUND OF THE INVENTION In the past ultrasonic cleaning systems where tanks containing cleaning liquid have been agitated by transducers coupled thereto have been difficult to repair except by time consuming and expensive means. For example, at the present time ultrasonic transducer units are permanently heat bonded by epoxy type glue or welding to the bottom plate of the tank used for cleaning. For a -gallon tank there may be as many as 30 to 40 transducers. Each transducer is essentially a permanently assembled unitary assembly which must be replaced as a unit. Thus if one transducer fails, it must be removed from the tank by heating the bond around that particular transducer and replaced with a new transducer assembly. However, in removing merely one transducer the heating of the tank and bond around the defective transducer tends to damage the bonds on other surrounding transducer units. Thus from a practical aspect, when one transducer unit is to be replaced several more than that must also be replaced and rebonded.
Also during initial installation of the transducer units the application of heat to initially bond the unit to a liquid containing tank must be limited in order not to damage the actual vibratory transducer elements contained in the transducer unit. As a consequence the initial bond may be unsatisfactory. With the use of a higher melting point bonding compound, a more durable bond results. This is especially necessary in an ultrasonic cleaning system where the vibrator tends to loosen a bond and where heat generated by the cleaning process will also loosen bonds.
Another difficulty in the prior ultrasonic cleaning systems is that all of the transducer units on a single tank were supplied power from a single oscillator unit. Thus, if any single transducer unit malfunctioned placing an open or short on the circuit, this would tend to make inoperative the entire power supply for the transducer units. Thus in addition to the reheating problem to remove the bonded or integrally mounted transducer unit from the base, malfunction of a unit would also necessitate replacement of the entire electrical power source unit for all transducer units.
OBJECTS AND SUMMARY OF THE INVENTION It is therefore a general object of the invention to provide an improved ultrasonic cleaning system;
It is another object of the invention to provide an ultrasonic cleaning system in which each transducer unit may be easily repaired without deleteriously affecting the other transducer units in the system;
It is another object of the invention to provide an ultrasonic cleaning system in which when a transducer unit malfunctions only a portion of the electrical circuit supplying oscillatory energy to the transducer unit is affected.
In accordance with the above objects there is provided an ultrasonic system having receptacle means for retaining liquid which is agitated ultrasonically. Such a system comprises a plurality of transducer means for converting electrical energy to mechanical vibratory energy each including a base integrally mounted on the receptacle. A transducer element mechanically coupled to said base is included in the transducer means and has terminal means for coupling to a source of electrical energy. The transducer means also includes fastener means for coupling the transducer means to the base, the fastener means having a portion thereof removable to allow the transducer element to be replaced and a new transducer element recoupled to the base. A source of electrical energy including a plurality of oscillator means is provided each of the oscillator means being mounted in separate plug-in units associated respectively with each of the transducer means. Each of the oscillator means are coupled to respective terminals of the transducer means.
BRIEF DESCRIPTION OF THE DRAWING FIG. I is a cross-sectional of a tank of an ultrasonic cleaning system showing transducer units attached thereto;
FIG. 2 is a bottom view in schematic form of the tank of FIG. I and also includes a diagrammatic showing of the electrical energy sources supplying energy to the transducer units;
FIG. 2A is a cross-sectional view taken along the lines 2A-2A of FIG. 2;
FIG. 3 is an enlarged cross-sectional view showing one of the transducer units mounted to the tank of FIG. I; and
FIG. 4 is a circuit schematic of an electrical energy source for one of the transducer units.
DETAILED DESCRIPTION OF THE INVENTION Referring first to FIG. I, there is illustrated a receptacle I0 containing suitable cleaning liquid II which has mounted on its bottom plate I4 eight identical transducer units 12. FIG. 3 shows one of the units in detail which includes a cylindrical base III which is heat bonded to bottom plate 14 by either welding or epoxy glue. Base 13 would normally be composed of a suitable metal such as aluminum. Two annularly shaped piezoelectric type crystals 16 and 17 are coupled to base 13 by means of a tapered stud 15 which is screwed into a threaded receptacle I9 in the center of base 13. A nut 18 on stud 15 causes a compression plate Zll to compress elements 16 and I7 together and against base 13.
In practice stud I5 is screwed into receptacle 19 with a much greater torque than nut I8. For example, stud I5 may have applied to it more than 200 inch-pounds of torque while in the case of nut IS a maximum of l20-l40 inch-pounds is applied. This differential allows nut 18 to be removed while stud I5 remains in place.
From a method standpoint stud I5 is threaded into base 13 before the base is bonded to receptacle I0. This allows a torque force to be used on the stud which is much greater than the relative bonding force.
Intermediate the elements I6 and I7 is a conductive sheet 22 which has a terminal 23 to which high frequency electrical energy is supplied. The respective opposite sides of elements 116 and I7 are conductively coated to make contact with grounded conductive layers 24 and 25. This provides a potential difference across the piezoelectric elements I6 and 17 which places them in vibration upon application of high frequency voltage to cause liquid II in the tank 10 to be agitated to thus perform a cleaning function. Each transducer element I6 and I7 also includes collars 16a and 17a to prevent any short circuit by stud IS. A stud I5, as is apparent, in conjunction with compression plate 21 and nut I8 serve as a fastener for the transducer elements 16 and 17. Since nut 18 was applied to the stud with a lower torque it may be easily removed allowing any defective transducer elements 16 and I7 to be removed and replaced with a working element.
Stress concentrations in the piezoelectric elements are relieved by the circular configuration of base 13 and the provision of the stud 15 in the center of the base. This is because no sharp comers are present and stresses that are present are uniformly distributed.
The method of providing an ultrasonic cleaning system in accordance with the invention comprises the following steps. Base I3 with its stud I5 inserted and torqued down to the desired tension is bonded to bottom plate 14. The bonding process is carried out in compliance with the manufacturers instructions of the bonding compound used. The base during bonding is loaded with sufficient weight to force out all air bubbles and allowed to set cold. Thereafter it is heated above the Curie point of crystals I6 and 17. With this high temperature maximum strength and adhesive force are achieved.
The Curie point or rating of a crystal is the temperature at which the crystal begins to lose its power rating. Once heated to this temperature the crystal permanently loses at least a portion of the rating. Thus, the crystals 16 and 17 are not placed on base 13 until the base has cooled to room temperature.
Crystals l6 and 17 are mechanically coupled to base 12 by tightening nut 18 on stud 15. The nut is torqued to a value determined by the manufacturers specifications. For example, a crystal available from Channell Industries of Santa Barbara, California, has a free frequency of 160 kHz. This frequency is reduced to a desired 20 kHz by a torque pressure of l20l40 inch-pounds. Spot checks however should be made with an oscilloscope to verify the manufacturers specifications.
Each plug-in unit 27 includes an oscillator means as shown in FIG. 4 which has a transformer T to which is supplied a source of AC voltage which may, for example, be 1 l volts, ()0 hertz. This is coupled into a bridge circuit which includes diodes D1, D2. The center tap of the bridge is coupled between two identical halves of an inductance designated L2, L2. Transistors Q] and Q2 provide a push-pull oscillation circuit with feedback being provided by winding Ll through the phase shift capacitor C l. Resistors R1 and R2 couple the bases of transistors Q1 and O2 to diodes D1 and D2 and resistors R3 and R4 couple to the bases to the center tap of the bridge. Output winding L3 is coupled to Ll and L2 which provides the necessary high frequency oscillatory voltage which is applied to the transducer units 12. A light source 28 is mounted in parallel with a series resistor 29 to indicate an open circuit in the transducer element. This is the normal failure mode of a piezoelectric transducer element. Plug-in units 27 include male and female connectors 31 (H6. 2A) which allow for easy replacement upon failure of either the current and/or associated transducer units.
The following component values and specifications will provide an ultrasonic generator with a frequency of kilohertz and power capacity of 250 watts:
R3, R4-470 ohms Tl300 Volt-amperes, l9 volts each side of center tap T2Ll=l 1 turns 018 wire L2=24 turns 016 wire with tap at center L3=98 turns 020 wire Thus, the present invention provides an improved ultrasonic cleaning system, apparatus and method therefore in which the transducer units are easily repaired by simple removal of the nut 18. At the same time if one of the units fails, only a portion of the associated electrical power source is affected and these are also easily replaced.
lclaim:
1. An ultrasonic cleaning system having receptacle means for retaining liquid which is agitated ultrasonically comprising, a plurality of transducer means for converting electrical energy to mechanical vibratory energy each including a base integrally mounted on said receptacle, a transducer element mechanically coupled to said base and having terminal means for coupling to a source of electrical energy, fastener means for coupling said transducer element to said base said fastener means having a portion thereof removable to allow said transducer element to be replaced said portion being reusable to recouple a transducer element to said base, and a source of electrical energy including a plurality of separate oscillator means each mounted in separate plug-in units associated respectively with each of said transducer means, each of said oscillator means being coupled to respective terminals of said transducer means.
2. An ultrasonic cleaning system as in claim 1 in which said bases are affixed to said receptacle by a bonding process in which heat is applied.
3. An ultrasonic cleaning system as in claim 1 in which said fastener means includes a stud having a removable nut and in which said base is threaded to receive said stud.
4. An ultrasonic cleaning system as in claim 1 in which each of said oscillator means includes indicator means for indicating a malfunction of such oscillator or associated transducer means.
5. Ultrasonic cleaning apparatus comprising, a base having a relatively substantial mass and a predetermined depth, a transducer element mechanically coupled to said base and having terminal means for coupling to a source of electrical energy, fastener means for coupling said transducer element to said base including a threaded stud having one end screwed into said base less than one-half said depth by application of a predetermined torque said fastener means including a pressure plate which in conjunction with said base forms a sandwich construction with said transducer element there between said stud extending through apertures in said transducer element and pressure plate and including nut means screwed onto the other end of said stud by application of a torque less than said predetermined torque to mechanically couple said transducer element to said base.
6. Apparatus as in claim 5 where said base is cylindrical and said stud is centered on the axis of said base.
7. A method of providing an ultrasonic cleaning system having receptacle means for retaining liquid which is agitated ultrasonically and having a transducer unit with a base to which is coupled an annular transducer element by a threaded stud, pressure plate and nut comprising the steps of, providing a threaded receptacle in said base, screwing said stud into said threaded receptacle by application of a predetermined torque, thereafter bonding said base to said receptacle means, placing said annular transducer element on said base with said stud extending therethrough, mechanically coupling said element to said base by placing said pressure plate on said element and said nut on said stud and applying a torque to said nut less than said predetermined torque.
8. A method as in claim 7 in which the bonding force holding said base to said receptacle means is less than said predetermined torque.
9. A method as in claim 7 in which said base is bonded to said receptacle at a temperature greater than the Curie point of said transducer element and said element is placed on said base with said base at a substantially lower temperature.

Claims (9)

1. An ultrasonic cleaning system having receptacle mEans for retaining liquid which is agitated ultrasonically comprising, a plurality of transducer means for converting electrical energy to mechanical vibratory energy each including a base integrally mounted on said receptacle, a transducer element mechanically coupled to said base and having terminal means for coupling to a source of electrical energy, fastener means for coupling said transducer element to said base said fastener means having a portion thereof removable to allow said transducer element to be replaced said portion being reusable to recouple a transducer element to said base, and a source of electrical energy including a plurality of separate oscillator means each mounted in separate plug-in units associated respectively with each of said transducer means, each of said oscillator means being coupled to respective terminals of said transducer means.
2. An ultrasonic cleaning system as in claim 1 in which said bases are affixed to said receptacle by a bonding process in which heat is applied.
3. An ultrasonic cleaning system as in claim 1 in which said fastener means includes a stud having a removable nut and in which said base is threaded to receive said stud.
4. An ultrasonic cleaning system as in claim 1 in which each of said oscillator means includes indicator means for indicating a malfunction of such oscillator or associated transducer means.
5. Ultrasonic cleaning apparatus comprising, a base having a relatively substantial mass and a predetermined depth, a transducer element mechanically coupled to said base and having terminal means for coupling to a source of electrical energy, fastener means for coupling said transducer element to said base including a threaded stud having one end screwed into said base less than one-half said depth by application of a predetermined torque said fastener means including a pressure plate which in conjunction with said base forms a sandwich construction with said transducer element there between said stud extending through apertures in said transducer element and pressure plate and including nut means screwed onto the other end of said stud by application of a torque less than said predetermined torque to mechanically couple said transducer element to said base.
6. Apparatus as in claim 5 where said base is cylindrical and said stud is centered on the axis of said base.
7. A method of providing an ultrasonic cleaning system having receptacle means for retaining liquid which is agitated ultrasonically and having a transducer unit with a base to which is coupled an annular transducer element by a threaded stud, pressure plate and nut comprising the steps of, providing a threaded receptacle in said base, screwing said stud into said threaded receptacle by application of a predetermined torque, thereafter bonding said base to said receptacle means, placing said annular transducer element on said base with said stud extending therethrough, mechanically coupling said element to said base by placing said pressure plate on said element and said nut on said stud and applying a torque to said nut less than said predetermined torque.
8. A method as in claim 7 in which the bonding force holding said base to said receptacle means is less than said predetermined torque.
9. A method as in claim 7 in which said base is bonded to said receptacle at a temperature greater than the Curie point of said transducer element and said element is placed on said base with said base at a substantially lower temperature.
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US5178173A (en) * 1991-08-01 1993-01-12 Robert J. Pace Ultrasonic contact lens cleaning device
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US5998908A (en) * 1996-05-09 1999-12-07 Crest Ultrasonics Corp. Transducer assembly having ceramic structure
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US20040124745A1 (en) * 2002-09-23 2004-07-01 Goodson J. Michael Sleeved ultrasonic transducer
US20040251780A1 (en) * 2003-05-09 2004-12-16 Goodson J. Michael Advanced ceramics in ultrasonic transducerized devices
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US20050122003A1 (en) * 2003-11-05 2005-06-09 Goodson J. M. Ultrasonic processing method and apparatus with multiple frequency transducers
US20060275883A1 (en) * 2003-02-27 2006-12-07 Andreas Rathgeber Method and device for blending small quantities of liquid in microcavities
US20070182285A1 (en) * 2004-11-05 2007-08-09 Goodson J M Megasonic processing apparatus with frequency sweeping of thickness mode transducers
US20070264161A1 (en) * 2003-02-27 2007-11-15 Advalytix Ag Method and Device for Generating Movement in a Thin Liquid Film
US20080170464A1 (en) * 2005-08-23 2008-07-17 Olympus Corporation Analyzing apparatus, supply apparatus, agitation apparatus, and agitation method
US20080240992A1 (en) * 2005-10-14 2008-10-02 Olympus Corporation Stirrer,vessel, and analyzer
US20110132575A1 (en) * 2009-12-07 2011-06-09 Goodson J Michael Cleaning Industrial Heat Exchangers Through Utilization of Thicknenss Mode Ultrasonics
US20110188337A1 (en) * 2003-02-27 2011-08-04 Beckman Coulter, Inc. Method and device for generating movement in a thin liquid film
US20150224460A1 (en) * 2012-08-20 2015-08-13 Christopher T. Banus Vibration-assisted apparatus for mixing immiscible liquids and for mixing powders with liquids or with other powders

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US4064886A (en) * 1975-11-20 1977-12-27 Riwoplan Medizin-Technische Einrichtungs-Gesellschaft Mbh Apparatus for cleansing endoscopes
US4114194A (en) * 1976-04-22 1978-09-12 Clairol, Inc. Ultrasonic cleaner
US4193818A (en) * 1978-05-05 1980-03-18 American Sterilizer Company Combined ultrasonic cleaning and biocidal treatment in a single pressure vessel
EP0225113A2 (en) * 1985-11-19 1987-06-10 Westinghouse Electric Corporation Magnetostrictive transducer apparatus
EP0225113A3 (en) * 1985-11-19 1988-12-14 Westinghouse Electric Corporation Magnetostrictive transducer apparatus
US4797550A (en) * 1987-11-06 1989-01-10 Consolidation Coal Company Fiber optic detector for flotation cell processing
US5178173A (en) * 1991-08-01 1993-01-12 Robert J. Pace Ultrasonic contact lens cleaning device
US5441062A (en) * 1991-10-07 1995-08-15 Sollac Method and device for pickling the edge portions of a sheet immersed in a reactive solution, in particular a hot rolled sheet
US6653760B1 (en) 1996-05-09 2003-11-25 Crest Ultrasonics Corporation Ultrasonic transducer using third harmonic frequency
US5998908A (en) * 1996-05-09 1999-12-07 Crest Ultrasonics Corp. Transducer assembly having ceramic structure
US5748566A (en) * 1996-05-09 1998-05-05 Crest Ultrasonic Corporation Ultrasonic transducer
US6106374A (en) * 1998-07-16 2000-08-22 International Business Machines Corporation Acoustically agitated delivery
US7341697B2 (en) * 2002-03-01 2008-03-11 Ngk Insulators, Ltd. Reaction cell and operation method thereof
US20040005722A1 (en) * 2002-03-01 2004-01-08 Ngk Insulators, Ltd. Reaction cell and operation method thereof
US20080050285A1 (en) * 2002-03-01 2008-02-28 Ngk Insulators, Ltd. Reaction cell and operation method thereof
US6924585B2 (en) 2002-09-23 2005-08-02 The Crest Group, Inc. Sleeved ultrasonic transducer
US20040124745A1 (en) * 2002-09-23 2004-07-01 Goodson J. Michael Sleeved ultrasonic transducer
US8303778B2 (en) 2003-02-27 2012-11-06 Beckman Coulter, Inc. Method and device for generating movement in a thin liquid film
US20060275883A1 (en) * 2003-02-27 2006-12-07 Andreas Rathgeber Method and device for blending small quantities of liquid in microcavities
US8038337B2 (en) * 2003-02-27 2011-10-18 Beckman Coulter, Inc. Method and device for blending small quantities of liquid in microcavities
US20070264161A1 (en) * 2003-02-27 2007-11-15 Advalytix Ag Method and Device for Generating Movement in a Thin Liquid Film
US20110188337A1 (en) * 2003-02-27 2011-08-04 Beckman Coulter, Inc. Method and device for generating movement in a thin liquid film
US20040251780A1 (en) * 2003-05-09 2004-12-16 Goodson J. Michael Advanced ceramics in ultrasonic transducerized devices
US20050109368A1 (en) * 2003-09-08 2005-05-26 Goodson J. M. Cleaning tank with sleeved ultrasonic transducer
US7495371B2 (en) 2003-09-08 2009-02-24 The Crest Group, Inc. Cleaning tank with sleeved ultrasonic transducer
US7247977B2 (en) 2003-11-05 2007-07-24 Goodson J Michael Ultrasonic processing method and apparatus with multiple frequency transducers
US20070283985A1 (en) * 2003-11-05 2007-12-13 Goodson J M Ultrasonic Processing Method and Apparatus with Multiple Frequency Transducers
US20050122003A1 (en) * 2003-11-05 2005-06-09 Goodson J. M. Ultrasonic processing method and apparatus with multiple frequency transducers
US20070283979A1 (en) * 2003-11-05 2007-12-13 Goodson J M Ultrasonic Processing Method and Apparatus with Multiple Frequency Transducers
US7598654B2 (en) 2004-11-05 2009-10-06 Goodson J Michael Megasonic processing apparatus with frequency sweeping of thickness mode transducers
US20100012148A1 (en) * 2004-11-05 2010-01-21 Goodson J Michael Megasonic processing apparatus with frequency sweeping of thickness mode transducers
US20070182285A1 (en) * 2004-11-05 2007-08-09 Goodson J M Megasonic processing apparatus with frequency sweeping of thickness mode transducers
US8310131B2 (en) 2004-11-05 2012-11-13 Megasonic Sweeping, Inc. Megasonic processing apparatus with frequency sweeping of thickness mode transducers
US20080170464A1 (en) * 2005-08-23 2008-07-17 Olympus Corporation Analyzing apparatus, supply apparatus, agitation apparatus, and agitation method
US20080240992A1 (en) * 2005-10-14 2008-10-02 Olympus Corporation Stirrer,vessel, and analyzer
TWI393595B (en) * 2006-03-17 2013-04-21 Michale Goodson J Megasonic processing apparatus with frequencey sweeping of thickness mode transducers
US20110132575A1 (en) * 2009-12-07 2011-06-09 Goodson J Michael Cleaning Industrial Heat Exchangers Through Utilization of Thicknenss Mode Ultrasonics
US20150224460A1 (en) * 2012-08-20 2015-08-13 Christopher T. Banus Vibration-assisted apparatus for mixing immiscible liquids and for mixing powders with liquids or with other powders
US9975096B2 (en) * 2012-08-20 2018-05-22 Christopher T. Banus Vibration-assisted apparatus for mixing immiscible liquids and for mixing powders with liquids or with other powders

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