WO1993012626A1 - Cerumen filter for hearing aids - Google Patents

Cerumen filter for hearing aids Download PDF

Info

Publication number
WO1993012626A1
WO1993012626A1 PCT/US1992/010231 US9210231W WO9312626A1 WO 1993012626 A1 WO1993012626 A1 WO 1993012626A1 US 9210231 W US9210231 W US 9210231W WO 9312626 A1 WO9312626 A1 WO 9312626A1
Authority
WO
WIPO (PCT)
Prior art keywords
wax guard
hearing aid
sound
outlet port
guard
Prior art date
Application number
PCT/US1992/010231
Other languages
French (fr)
Inventor
Robert J. Oliveira
Original Assignee
Oliveira Robert J
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25186897&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO1993012626(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Oliveira Robert J filed Critical Oliveira Robert J
Priority to JP5510934A priority Critical patent/JPH07501673A/en
Priority to BR9206870A priority patent/BR9206870A/en
Priority to EP93900690A priority patent/EP0619934A1/en
Priority to AU32272/93A priority patent/AU665976B2/en
Publication of WO1993012626A1 publication Critical patent/WO1993012626A1/en

Links

Classifications

    • HELECTRICITY
    • H04ELECTRIC COMMUNICATION TECHNIQUE
    • H04RLOUDSPEAKERS, MICROPHONES, GRAMOPHONE PICK-UPS OR LIKE ACOUSTIC ELECTROMECHANICAL TRANSDUCERS; DEAF-AID SETS; PUBLIC ADDRESS SYSTEMS
    • H04R25/00Deaf-aid sets, i.e. electro-acoustic or electro-mechanical hearing aids; Electric tinnitus maskers providing an auditory perception
    • H04R25/65Housing parts, e.g. shells, tips or moulds, or their manufacture
    • H04R25/652Ear tips; Ear moulds
    • H04R25/654Ear wax retarders

Definitions

  • the linered wax guard assembly shown in FIG. 7 can be distributed in a transparent plastic envelope 92, which will ensure that wax guards 30, 80, and 90 do not become prematurely detached from either liner 60 or folded liner 70.
  • a kit contain ⁇ ing a plurality of wax guards having a variety of thick ⁇ nesses of reticulated open cell foam membrane 31, 81, 91 (e.g., 1/32, 1/16, and 1/8 inch, corresponding respectively to about 0.8, 1.6, and 3.2 mm) will prove useful to hearing aid dispensers, who can then provide the appropriate wax guard for an individual hearing aid wearer.
  • this kit could consist of wax guards in which anterior attaching lobes 30a, 80a, 90a are of differ ⁇ ent dimensions

Abstract

A readily installed and replaced disposable wax guard that is affixed over the sound outlet port of an 'in the ear' hearing aid and adhered to the adjacent sides of the aid. The portion that overlies the sound outlet port is porous to sound and receptive to cerumen.

Description

CERUMEN FILTER FOR HEARING AIDS
Background of the Invention
This invention relates to preventing cerumen, or ear wax, from interfering with the operation of sound transmission devices, especially "in the ear" hearing aids, and is particularly concerned with a novel filter for achieving that result.
The human outer ear comprises the visible exter¬ nal ear, or pinna, and a dynamic S-shaped canal that has a generally oval cross section and is about an inch (2.5 cm) long. Cerumen is secreted by the walls of the canal in the outer half inch (1.2 cm) or so and gradually moved outward; some believe that this outward movement is brought about by cilia in the walls, but more likely it is caused by the natural action of the ear canal. When a hearing aid is in¬ serted into the outer 1/4 inch (about 0.6 cm) of the canal, it becomes susceptible to cerumen, which mixes with sloughed off skin and often fouls the hearing aid's sound delivery tube, thereby reducing its efficiency. When the sound delivery tube of a hearing aid clogs with cerumen and reduces the effectiveness of sound transmission, the wearer of a hearing aid typically turns up the volume control. This in turn results in two unde¬ sirable conditions. Not only does the hearing aid battery wear out more quickly with certain types of circuit, but the likelihood of embarrassing and frequently painful feed¬ back howl also increases. Most importantly, cerumen in the sound tube of the hearing aid is the basis for large num¬ bers of costly hearing aid repairs. There have been numerous attempts to modify hearing aids to avoid the problems discussed in the preced¬ ing paragraphs. Thus, for example, U.S. Pats. No. 4,870,689 and 4,972,488 disclose a tubular passage having a series of baffles that define a "tortuous path" that the wax must travel before reaching the sound tube. U.S. Pat. No. 4,800,982 describes a hearing aid through which solvent may be pumped to remove wax buildup. U.S. Pat. No. 4,953,215 describes a hearing aid in which a domed membrane having a small central opening is provided, wax being said to accumulate in a ring around the base of the membrane.
Still others have attempted to devise some type 5 of filter to prevent ear wax from reaching the sound deliv¬ ery tube. For example, U.S. Pats. No. 3,414,685 and 4,984,277 discuss various prior art wax filters, noting the apparent difficulty in replacing them after they are soiled. In each case, the patentees' approach to the prob- 0 lem is to provide a one-piece plastic part that has numer¬ ous openings around the periphery and snaps around the sound delivery tube opening. A-somewhat similar device is shown in U.S. Pat. No. 4,553,627, where a snap-on wax guard has a cross passage through its head that intersects an axial passage in its stem; ear wax is removed by pushing a tool through the cross passage. Still others have mechani¬ cally mounted screens or other filters beyond the sound de¬ livery tube opening, but removal and replacement has been difficult, especially since persons wearing hearing aids are often advanced in years and unable either to see clear¬ ly enough or to perform fine physical actions well enough to replace the filters.
Brief Summary
The present invention provides a novel dispos- able wax guard for sound transmission devices that are in¬ serted into the ear canal, especially "in the ear" hearing aids. It is simple to install, easy to remove, and conve¬ nient to replace, even for older persons. The guard is in¬ expensive and requires no tools for installation or re- moval. In many instances, the wax guard of the invention not only assists in retaining the sound transmission device in place in the ear canal but also improves the seal be¬ tween the hearing aid and the dynamic ear canal. Although the use of the invention with such sound transmission de- ices as stethoscopes, miniaturized portable telephones, etc., is envisioned, for convenience, the major part of the description that follows will be addressed to "in the ear" hearing aids. An "in the ear" hearing aid comprises a housing containing a microphone, a battery, an amplifier, and a speaker, the housing fitting within a user's ear canal. A sound-transmitting tube extends from the speaker to an out- let port' at the portion of the housing closest to the ear drum. The present invention provides a readily installed and replaced disposable wax guard for mounting over the outlet port of the hearing aid to prevent cerumen from fouling it. This wax guard comprises a thin, strong carri- er membrane adapted to be temporarily adhered over the por¬ tion of the hearing aid nearest to the ear drum, fixed in position over the outlet port, the portion of the guard overlying the outlet port being porous to sound and recep¬ tive to cerumen and the accompanying dermal detritus from the lining of the ear canal before it can foul the sound outlet port of the hearing aid. In another aspect, the in¬ vention provides a method of modifying a conventional "in the ear" hearing aid to render it resistant to cerumen. In still another aspect, the invention provides a method of forming an improved seal between the hearing aid and the dynamic ear canal. In a further aspect, the invention pro¬ vides improved retention of small earpieces in the dynamic ear canal.
Brief Description of the Drawing
Understanding of the invention will be enhanced by referring to the accompanying drawing, in which like numbers refer to like parts in the several views, and in which:
FIG. 1 is a greatly enlarged plan view of one embodiment of the wax guard of the invention;
FIG. 2 is a cross-section of the wax guard of FIG. 1, taken along section II- = 2 - 2, looking in the di¬ rection of the arrows;
FIG. 3 is a view in .^rspective of a currently preferred embodiment of the invention;
FIG. 4 is a cross-sectional view of the wax guard of FIG. 3, taken along section lines 4-4, looking in the direction of the arrows; FIG. 5 is a plan view of the lower adhesive- coated surface of the wax guard of FIG. 3;
FIG. 6 is an enlarged and simplified drawing of a human ear, showing an "in the ear" hearing aid mounted in the ear canal, with a wax guard of the invention in place;
FIG. 7 is a greatly enlarged plan view showing three wax guards of the type shown in FIG. 3 (the exact di¬ mensions differing among the three), positioned on a re¬ lease liner, with a folded release liner protecting each of the lobes of each wax guard; and
FIG. 8 is a cross-sectional view of the assembly shown in FIG. 7, taken along section line 8 - 8, looking in the direction of the arrows.
Detailed Description
Turning first to FIGs. 1 and 2, wax guard 10 comprises thin, strong, flexible carrier membrane 11 having attaching lobes 10a, lOp, and central lobe 10c, hole 13 being located approximately in the center of lobe 10c. One side of carrier membrane 11 is provided with a layer of normally tacky and pressure-sensitive adhesive 14, which serves to affix wax guard 10 to a hearing aid, with hole 13 positioned over the sound outlet port of the hearing aid. A nonwoven mat 15 of fine fibers is held in place by adhesive 14 in the area circumjacent to hole 13. If desired, hole 13 may be covered with a mesh fabric to help retain mat 15 in place.
Carrier membrane 11 is conveniently made from a white rayon acetate taffeta woven backing, combined with a layer of pressure-sensitive adhesive 14, the mild rugosity of the backing imparting a desirable frictional property when wax guards of the invention are used as subsequently described. One adhesive-coated product suitable for use in practice of the invention is available from Minnesota Mining and Manufacturing Company (3M) under the catalog designation "1538-L Woven Medical Tape on Liner." The ad¬ hesive on this product is a hypoallergenic acrylate, making it especially suitable for practicing the present inven¬ tion. _._ Nonwoven mat 15 is desirably formed from a melt- blown mat of extremely fine oleophilic polypropylene fibers. Alternatively, the mat could be an appropriately sized disc formed from a web of oleophilic open cell foam. Turning next to FIGs. 3 - 5, wax guard 30 com¬ prises a thin, compressible, resilient, sound-transmitting, soft membrane layer 31 of reticulated open cell microporous foam. Wax guard 30 in turn comprises anterior and posteri¬ or attaching lobes 30a, 30p, and central lobe 30c. Laminated to the lower surface of foam membrane layer 31 is double-coated tape 32, comprising thin (about 0.0015-inch, or 6-micrometer) polyethylene film 33 and pressure-sensi¬ tive adhesive layers 34, 35. Central portion 36 of lobe 30σ is free from tape 32. Thus, whereas tape 32 seals foam membrane 31 and destroys its sound-transmitting ability, central portion 36 remains open and continues to retain that ability. This embodiment of the invention is thus both simple and economical to make.
Attention is now directed to FIG. 6, showing wax guard 30 of FIG. 3 mounted on hearing aid 50. As is shown in FIG. 6, human outer ear 40 comprises pinna 41, concha 42, ear canal 43, and ear drum 44. Positioned within the outer portion of canal 22 is hearing aid 50, which includes the conventional battery, microphone, amplifier, and speak- er (none of which are shown), with open-ended sound-trans¬ mitting tube 51 extending from the speaker to the inner end of hearing aid 50 and terminating in an outlet port. Wax guard 30 is positioned so that area 36 (which, it will be recalled, is free from pressure-sensitive adhesive tape) is mounted over the outlet port of sound transmitting tube 51, with adhesive-coated circumferential area 30c and lobes 30a and 3Op adhered, respectively, to the inner end and anteri¬ or and posterior sides of hearing aid 50 to hold wax guard 30 in place. As previously pointed out,the outer portion of canal 43 is oval rather than circular in cross section, with the longer axis extending in a generally vertical plane. This ovality is reflected in the shape of central portion 31c of wax guard 30, and lobes 30a and 30p are ac¬ cordingly intended to be mounted along the anterior and posterior sides of hearing aid 50. This positioning also provides a somewhat snugger fit between hearing aid 50 and the wall of canal 43 and helps hold hearing aid 50 in place. This is especially important when chewing or talk¬ ing causes the anterior wall of canal 43 to move in and out, which in turn causes the anterior-posterior dimension of the oval canal wall to contract and expand.
It will be noted that posterior attaching lobe 3Op is smaller than anterior attaching lobe 30a, enabling it to conform easily to the concave posterior surface of any hearing aid. This is especially important for those hearing aids that are seated in concha 42, which do not ex¬ tend to a great depth in canal 43 and have other plastic surfaces that can interfere with easy access to the concave posterior side of the canal-occupying part of the hearing aid.
Because foam membrane 31 is not only compress¬ ible but also resilient, sealing of hearing aid 50 against the wall of canal 43 can be maintained, even as the dimen¬ sions of canal 43 change during mastication or conversa- tion. This improved sealing helps correct the extremely annoying feedback problem frequently encountered by hearing aid wearers while dining with friends or talking on the telephone. Indeed, it is contemplated by the inventor that different thicknesses or surface areas of foam layer 31 can be employed to achieve the desired result. Inasmuch as im¬ proper fit is one of the most frequent complaints made by persons who have just purchased hearing aids, it is be¬ lieved that use of the wax guard of this embodiment of the invention may reduce such complaints. With respect to the improved sealing provided by the foam, attention is direct¬ ed to the prior art product ER-13R "E-A-R RING", a ring formed from foam and intended to be slipped over the distal portion of a hearing aid to "seal leaky shells" and reduce feedback. Prior art devices of this type, which are avail- able from Etymotic Research, Elk Grove Village, Illinois, USA, are not provided with pressure-sensitive adhesive (presumably because they would then be hard to install on a hearing aid) , although the use of a drop of a permanent adhesive (e.g., tetrahydrofuran, which is presumably a sol- vent for the hearing aid 50) is suggested. In the absence of adhesive, these rings have been known to remain in the ear canal after removal of the hearing aid, and if a strong adhesive is used, it will be hard to remove the ring from the hearing aid. A currently preferred material for use as foam layer 31 is a polyester urethane foam about 0.05 inch (1.3 mm) thick, having about 100 pores per lineal inch (40 pores per lineal centimeter) and a void volume of about 97%. As mentioned previously, however, somewhat greater thicknesses may be appropriate for some individuals. This foam is also oleophilic, which is considered advantageous for use as a wax guard. Foams meeting these criteria are obtainable from Foamex under the trade designation "SIF Filter Foam."
It is believed that a degree of stretchability of the foam product just described is desirable in attain¬ ing wrinkle-free conformance to hearing aids; thus, it may be feasible to provide one surface of reticulated foam di¬ rectly with an adhesive. Greater strength can be imparted, however, by laminating the foam to a fine open mesh woven or nonwoven fabric (either of which might cover hole 36, 86, 96 without interfering with sound transmission) or, as in the product just described, to a double-coated tape.
Attention is now directed to FIG. 7, which de¬ picts the manner in which wax guards of the invention can be mounted for distribution to hearing aid dispensers or wearers of "in the ear" hearing aids. Three wax guards 30, 80, 90 are shown removably mounted on a conventional sheet of release liner 60, the adhesive-coated surface of posterior attaching lobes 3Op, 80p, 90p, and central lobe 30c, 80c, 90c being in contact with the release surface of liner 60. Anterior attaching lobes 30a, 80a, 90a are lift¬ ed above the surface of release liner 60, with folded re¬ lease liner 70 contacting the adhesive-coated surface of lobes 30a, 80a, 90a. Liner 70 has two wings, 70a and 70b, the adhesive-coated surface of lobes 30a, 80a, 90a being in contact with wing 70a. When wax guard 30, 80, or 90 is to be mounted on hearing aid 50, the distal portion of wing 70b is grasped (preferably along with lobe 30a, 80a, or 90a, as appropriate), and the remainder of wax guard 30, 80, or 90, peeled from release liner 60. Center lobe 30c, 80c, or 90c is then positioned over and circumferentially adhered to the sound outlet end of hearing aid 50 and ex¬ posed lobe 3Op, 8Op, or 9Op then adhered to the posterior side of hearing aid 50. Wing 70a of folded release liner 70 is then removed from lobe 30a, 80a, or 90a while the latter is being adhered to the anterior side of hearing aid 50.
For convenience, the linered wax guard assembly shown in FIG. 7 can be distributed in a transparent plastic envelope 92, which will ensure that wax guards 30, 80, and 90 do not become prematurely detached from either liner 60 or folded liner 70. It is contemplated that a kit contain¬ ing a plurality of wax guards having a variety of thick¬ nesses of reticulated open cell foam membrane 31, 81, 91 (e.g., 1/32, 1/16, and 1/8 inch, corresponding respectively to about 0.8, 1.6, and 3.2 mm) will prove useful to hearing aid dispensers, who can then provide the appropriate wax guard for an individual hearing aid wearer. Alternatively, as shown in FIG. 7, this kit could consist of wax guards in which anterior attaching lobes 30a, 80a, 90a are of differ¬ ent dimensions
As still another alternative, single adhesive- coated lobes of different dimensions could be incorporated in a kit; although these lobes would not function as wax guards, they could still be used to determine the appropri¬ ate degree of sealing to reduce or eliminate feedback caused by canal shape change resulting from jaw motion. Once the appropriate size has been determined, the adhe¬ sive-coated lobe could be used until it is soiled, after which it would be replaced with a fresh lobe. It is fur¬ ther contemplated that, when using the feedback suppressing aspect of the invention, shape-retaining retarded recovery materials such as plasticized polyvinyl chloride (cf. U.S. Pat. Re. 29,487) or polyurethane (cf. U.S. Pat. No. 4,880,076) would be more efficient than the open cell reticulated foam used for wax entrapment and hence could be used in thinner sections.
Those skilled in the art will readily appreciate that the foregoing description is not intended to be ex- haustive, and numerous variations of the invention can be made without departing from the spirit of what has been taught. Thus, for example, although wax guards having two attaching lobes are currently preferred, it would be feasi¬ ble to have four, the additional lobes attaching to the su- 5 perior and inferior surfaces of the hearing aid. The greater the number of lobes, however, the greater the dif¬ ficulty in attaching the wax guard. It should be possible to prepare a wax guard having a single attaching lobe (preferably the anterior lobe), the adhesive border on the 10 center lobe holding it in place over the sound outlet port. It may also be possible to prepare a product that has a single continuous lobe, resulting in a construction resem¬ bling that of a condom.
Similarly, the utility of the invention is not 15 limited to hearing aids, but is readily adaptable to any type of sound transmitting device that intrudes into the ear canal.
At the present time, the preferred dimensions of wax guard 30 are about 18.5 mm from the distal end of lobe 20 30a to the distal end of lobe 30p, lobe 30a being about 7.4 mm long and 6.6 mm wide. Lobe 3Op is about 4.8 mm long and 5.6 mm wide. Central lobe 30c is about 8.9 mm wide. Although these exact dimensions and shapes are not criti¬ cal, such products are suitable for mounting on all known 25 "in the ear" hearing aids. Wax guards having the shape of wax guard 10 are useful on most hearing aids, although they may be somewhat difficult to install smoothly on hearing aids that fit into concha 42 and do not penetrate as far into canal 43 as hearing aids that fit almost entirely into 30 canal 43.
Although numerous pressure-sensitive adhesives may be used to mount wax guard 10 or 30 on hearing aid 50, acry¬ late types are presently preferred; acrylate adhesives (e.g., a 95:5 isooctyl acrylate:acrylic acid copolymer) ad- 35 here well to the acrylate polymers used to make most hear¬ ing aids. Acrylate adhesives also tend not to irritate skin with which they may come in contact.

Claims

What is claimed is as follows :
1 1. For use in connection with a sound transmit -
XI ting device of the type in which a housing containing a
3 sound transmitting tube having a sound outlet port con-
4- fronting the ear drum, said device fitting within a user ' s
5 ear canal,
:6 a readily installed and replaced disposable wax guard
77 for mounting over the sound outlet port to prevent cerumen
8 from fouling said outlet port, comprising a thin, flexible
9 carrier membrane adapted to be temporarily adhered in posi-
10 tion over the portion of the sound transmitting device
11 nearest to the ear drum, the portion of said guard overly-
12 ing said outlet port being porous to sound and receptive
13 to cerumen.
1 2. For use in connection with an "in the ear"
2 hearing aid of the type in which a housing containing a mi-
3 crophone, an amplifier, and a speaker fit within the user's
4 ear canal, with a sound-transmitting tube extending from
5 adjacent the speaker to a sound outlet port at the portion
6 of the housing nearest to the ear drum,
7 a disposable wax guard for mounting over the sound
8 outlet port to prevent cerumen from fouling said outlet
9 port, comprising a thin, flexible carrier membrane 10 adapted to be temporarily adhered in position over said H outlet port, the portion of said guard overlying said out- 2 let port being porous to sound and oleophilic, so as to be I receptive to cerumen.
1 3. The wax guard of claim 2 wherein the membrane
2 is compressible, resilient open cell foam, one side of said
3 membrane being provided with a normally tacky and pressure- 4- sensitive adhesive layer except in that portion adapted to 5 overlie the sound outlet port of the hearing aid. 4. The wax guard of claim 3 wherein the normally tacky and pressure-sensitive adhesive layer-is in the form of a double-coated tape.
5. The wax guard of claim 2 wherein the sound- porous portion of the membrane is a hole having a slightly larger diameter than that of the outlet port and a mat of nonwoven fibers overlies said hole and is adhered to the circumjacent portions of said membrane.
6. The wax guard of claim 5 wherein the nonwoven mat is oleophilic.
7. The wax guard of claim 5 wherein the nonwoven mat consists essentially of blown microfibers.
8. The wax guard of claim 7 wherein the blown microfibers are polypropylene.
9. The wax guard of claim 6 wherein the membrane is provided with a normally tacky and pressure-sensitive adhesive so that it can be removably attached to the hear- ing aid housing.
10. The wax guard of claim 2 wherein the mem- brane is configured to have a plurality of lobes that can be removably adhered to the hearing aid housing.
11. The wax guard of claim 10 wherein there are only two lobes and they are adapted to adhere respectively to the anterior and posterior sides of the hearing aid.
12. The wax guard of claim 8 wherein the blown microfibers are polypropylene.
13. An "in the ear" hearing aid having a sound outlet port, the wax guard of claim 3 being mounted over said outlet port.
14. The wax guard of claim 3 wherein the mem- brane is configured to have a plurality of lobes that can be removably adhered to the hearing aid housing.
15. The wax guard of claim 14 wherein there are only two lobes, and they are adapted to adhere respectively to the anterior and posterior sides of the hearing aid.
16. The wax guard of claim 15 wherein the two lobes are of unequal size.
17. A release liner having removably adhered to the face thereof the wax guard of claim 16.
18. The product of claim 17 wherein one lobe of the wax guard is removably adhered to a folded release liner and the remainder of the wax guard is adhered to a conventional release liner.
19. The product of claim 18 wherein the larger lobe is adhered to the folded liner.
20. A kit comprising a plurality of the products of claim 18, the dimensions of the open cell foam membrane being different on the individual guards.
21. A method of providing better sealing between an "in the ear" hearing aid and the ear canal in which said hearing aid is mounted comprising temporarily adhering a resilient foam material to the surface of the hearing aid that confronts the anterior wall of the ear canal.
22. The method of claim 21 wherein the resilient foam material is characterized by retarded recovery.
PCT/US1992/010231 1991-12-09 1992-11-27 Cerumen filter for hearing aids WO1993012626A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP5510934A JPH07501673A (en) 1991-12-09 1992-11-27 Earwax filter for hearing aids
BR9206870A BR9206870A (en) 1991-12-09 1992-11-27 Cerumen filter in hearing aids
EP93900690A EP0619934A1 (en) 1991-12-09 1992-11-27 Cerumen filter for hearing aids
AU32272/93A AU665976B2 (en) 1991-12-09 1992-11-27 Cerumen filter for hearing aids

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US80357691A 1991-12-09 1991-12-09
US803,576 1991-12-09

Publications (1)

Publication Number Publication Date
WO1993012626A1 true WO1993012626A1 (en) 1993-06-24

Family

ID=25186897

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1992/010231 WO1993012626A1 (en) 1991-12-09 1992-11-27 Cerumen filter for hearing aids

Country Status (7)

Country Link
US (1) US5401920A (en)
EP (1) EP0619934A1 (en)
JP (1) JPH07501673A (en)
AU (1) AU665976B2 (en)
BR (1) BR9206870A (en)
CA (1) CA2122727A1 (en)
WO (1) WO1993012626A1 (en)

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JPH07501673A (en) 1995-02-16
US5401920A (en) 1995-03-28
CA2122727A1 (en) 1993-06-24
AU665976B2 (en) 1996-01-25
BR9206870A (en) 1995-11-28
AU3227293A (en) 1993-07-19
EP0619934A1 (en) 1994-10-19

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