WO1996040381A1 - Golf ball with wound hoop-stress layer - Google Patents
Golf ball with wound hoop-stress layer Download PDFInfo
- Publication number
- WO1996040381A1 WO1996040381A1 PCT/US1996/007793 US9607793W WO9640381A1 WO 1996040381 A1 WO1996040381 A1 WO 1996040381A1 US 9607793 W US9607793 W US 9607793W WO 9640381 A1 WO9640381 A1 WO 9640381A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- wound
- golf ball
- layer
- fiber
- elastic modulus
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/0023—Covers
- A63B37/0029—Physical properties
- A63B37/0033—Thickness
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/0038—Intermediate layers, e.g. inner cover, outer core, mantle
- A63B37/0039—Intermediate layers, e.g. inner cover, outer core, mantle characterised by the material
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/0038—Intermediate layers, e.g. inner cover, outer core, mantle
- A63B37/004—Physical properties
- A63B37/0045—Thickness
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/005—Cores
- A63B37/0051—Materials other than polybutadienes; Constructional details
- A63B37/0053—Thread wound
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/005—Cores
- A63B37/0051—Materials other than polybutadienes; Constructional details
- A63B37/0054—Substantially rigid, e.g. metal
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/005—Cores
- A63B37/006—Physical properties
- A63B37/0064—Diameter
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B37/00—Solid balls; Rigid hollow balls; Marbles
- A63B37/0003—Golf balls
- A63B37/007—Characteristics of the ball as a whole
- A63B37/0077—Physical properties
- A63B37/0086—Flexural modulus; Bending stiffness
Definitions
- This invention is directed to a golf ball having a thin wound hoop-stress layer.
- a golf ball having an inner resilient core, a layer wound of high-modulus fibers and an outer cover layer.
- the elastic thread of wound balls must be wound under high tension in order to produce a ball that will achieve the necessary velocity. Often, this causes the thread to break during winding or later manufacturing processes. Reduced thread tension during winding would minimize this problem, but would also cause a loss of velocity and compression which would then necessitate the use of a relatively hard end stiff cover that would provide the necessary hoop stress. This cover would give the ball an unacceptably harsh feel, negating a primary attribute of the wound ball.
- Solid construction balls have a slightly different problem. Since the cover layer must provide significant hoop stress, it is usually hard and stiff as a result. This problem is magnified when the core is made of a relatively soft compound in an attempt to give the ball a softer feel when struck.
- the present invention takes a different approach, that of providing an additional wound rather than solid layer to provide the necessary hoop stress.
- This layer is wound of a high tensile elastic modulus material such as aromatic polyamide fibers (for example aramid fibers sold by E.I. duPont De Nemours Co., Wilmington, DE, under the trademark of "Kevlar") , glass fiber, or metal wire.
- This wound high tensile elastic modulus layer under the cover gives a soft and flexible construction element that serves to provide the hoop stress while contributing minimally to the hardness of feel.
- the cover material may be chosen for spin, feel and durability alone, without adding structural requirements as well.
- the invention has a further benefit for golfers with a low swing speed.
- a low swing speed does not sufficiently compress the gclf ball at impact, and thus does not generate high enough internal stresses in the ball to achieve the explosive rebound off the club face which is enjoyed by those with higher swing speeds.
- the contact time between the ball and club face is longer and the golfer does not get the same crisp feel.
- a high modulus hoop stress layer will produce higher internal stresses at low swing speeds, giving these players enhanced rebound and feel.
- a further advantage to the invention is that the moment of inertia of the ball, and thus its spin characteristics, can be controlled by choosing the mass density and thickness of the hoop stress layer. For example, a very high moment of inertia could be created by using metallic wire in the wound hoop stress layer. The result would be a ball with a relatively low initial spin rate and low spin decay rate during flight.
- the invention includes a golf ball having a substantially spherical inner core, a first wound layer of high tensile elastic modulus fibers wound about the inner core, and a second molded layer of a polymeric material surrounding the wound layer.
- the invention also includes a method of making a golf ball, including providing an inner core, winding a high elastic modulus fiber on the inner core to create a first wound layer, and molding an outer layer of polymeric material about the first wound layer.
- the inner core in the above method and apparatus may be made of solid resilient materials or a center wound with a low modulus fiber under an initial tension.
- Fig. 1 illustrates a cut-away view of a solid inner core golf ball in accordance with the current invention
- Fig. 2 illustrates a cross-section of a wound inner core golf ball in accordance with the present invention
- Fig. 3 illustrates a hollow golf ball center for a golf ball in accordance with the present invention.
- a substantially spherical inner core 100 has a wound layer 105 of high tensile elastic modulus material wound about it.
- This wound layer has a cover layer 110 of polymeric material molded about and surrounding it.
- the inner core is solid and formed of a resilient material, preferably a polybutadiene or natural rubber containing compound.
- the wound layer is formed of high tensile fiber wound about the inner core and preferably in contact with the inner core.
- a variety of high tensile modulus fibers may provide the requisite hoop stress in a minimally thick layer, preferably glass, Dacron, polyamide, aromatic polyamide (such as duPont's Kevlar aramid fiber), carbon, or metal fibers.
- Metals such as steel (particularly stainless steel) - monel metal, or titanium are preferred. If a wound layer is created from metal fiber, the ball will have an increased moment of inertia, and thus will rotate at a slower speed when struck with a golf club, and will retain its rotational velocity longer during flight.
- the strength of these high tensile elastic modulus fibers is preferably high to accommodate the extremely high stresses placed upon the golf ball windings when it is struck with a golf club. It can be varied, however, to provide a golf ball with a good feel and durability. A tensile strength of at least 250 kpsi is preferred, however a tensile strength of at least 500 kpsi is more preferred.
- the tensile elastic modulus of the high tensile elastic modulus fiber along with its gauge or thickness may also be varied to provide a stiffer, a softer or a more durable ball as desired. A modulus of at least 10000 kpsi is preferred. A modulus of at least 20000 kpsi is most preferred.
- a single fiber is wound about the inner core to create the wound layer.
- the fiber is preferably a continuous fiber to provide for ease of winding.
- the fiber material is preferably in yarn, thread or filament form.
- the wound layer 105 preferably has an outside diameter of between 1.40 and 1.81 inches, and an inside diameter of between 1.30 and 1.80 inches.
- the wound layer is preferably wound to a thickness of between 0.01 and 0.10 inches.
- the cover layer 110 preferably has an outside diameter of between 1.68 and 1.85 inches. More preferably, it has an 5 outside diameter of between 1.68 and 1.72 inches. Its thickness is preferably between 0.04 and 0.14 inches.
- the preferred cover materials are an iono er (such as the variety of ionomers sold by the DuPont Chemical Company under the trade name of "Surlyn") , or balata, a naturally occurring 0 substance or its synthetic equivalent. This layer is preferably in direct contact with the wound layer.
- the combined thickness of the wound layer and the cover layer is preferably between 0.05 and 0.24 inches.
- FIG. 2 Another embodiment is shown in Fig. 2 for a golf 5 ball with a wound inner core.
- the inner core of the golf ball is made of a resilient center 115 with a layer 120 of low tensile elastic modulus material wound about it.
- Layer 120 has a wound layer 125 of high tensile elastic modulus fiber surrounding it.
- a cover layer 130 is
- the resilient center 115 is preferably a solid and preferably made of polybutadiene, however.
- Fig. 3 shows an alternative embodiment of center 115: a hollow center 135 made of natural rubber that is filled with a suitable liquid
- layer 120 surrounding the center may be solid or wound of an elastic material. If wound, it preferably has a tensile elastic modulus less than
- layer 120 is wound, an initial strain of at least 100% is preferred.
- Layer 120 and high elastic modulus layer 125 are preferably in contact, as are layers 125 and 130.
- Wound layer 125 has the characteristics described
- the high tensile elastic modulus fiber that comprises layer 125 should be wound about the core with an initial tension applied to the fiber during the winding process which provides an initial strain on the fiber being wound.
- An initial strain of less than 4% is most preferred.
- An initial strain of less than 10% is more preferred.
- An initial strain of less than 25% is preferred.
- the fiber itself is continuous for ease of winding about the core.
- a cover layer is molded about the wound layer, preferably by injection or compression molding processes well known to those of ordinary skill in the art of manufacturing golf balls.
Abstract
The invention includes a golf ball having a substantially spherical inner core (100), a first wound layer (105) of high tensile elastic modulus fibers wound about the inner core (100), and a second molded layer (110) of a polymeric material surrounding the wound layer (105), as well as a method of making a golf ball, including providing an inner core (100) winding a high elastic modulus fiber on the inner core (100) to create a first wound layer (105), and molding an outer layer (110) of polymeric material about the first wound layer (105). The inner core (100) in the above method and apparatus may be made of solid resilient materials or a center (115) wound with a low modulus fiber (120) and provided with an initial tension.
Description
GOLF BALL WITH WOUND HOOP-STRESS LAYER
Field of the invention
This invention is directed to a golf ball having a thin wound hoop-stress layer. In particular it is directed to a golf ball having an inner resilient core, a layer wound of high-modulus fibers and an outer cover layer.
Prior Art In the past, the cover of a golf ball has been relied upon to provide a confining hoop stress function which is believed to increase the initial velocity of a golf ball when struck by a golf club. For balls having a wound core, typically a solid or liquid filled center wound with a rubber thread, this hoop stress function of the cover has been only of moderate importance, since the wound core can be made lively enough on its own without requiring a cover providing significant hoop stress about the core. On the other hand, golf balls with solid cores tend to have a marginal velocity on their own, and are benefitted by a layer providing additional hoop stress. To date, this stress has been provided by a cover made of a relatively stiff material. The drawbacks of these ball constructions are numerous. The elastic thread of wound balls must be wound under high tension in order to produce a ball that will achieve the necessary velocity. Often, this causes the thread to break during winding or later manufacturing processes. Reduced thread tension during winding would minimize this problem, but would also cause a loss of velocity and compression which would then necessitate the use of a relatively hard end stiff cover that would provide the necessary hoop stress. This cover would give the ball an unacceptably harsh feel, negating a primary attribute of the wound ball. Solid construction balls have a slightly different problem. Since the cover layer must provide significant hoop stress, it is usually hard and stiff as a result. This problem is magnified when the core is made of a
relatively soft compound in an attempt to give the ball a softer feel when struck.
One technique suggested in the prior art to avoid the problem of an overly hard stiff cover was disclosed in U.S. Patent No. 4,431,193 issued to Nesbitt on February 14, 1984. Rather than have a single layer cover over the core, the cover would be molded in two layers: a hard stiff inner layer of a high flexural modulus material that provides significant hoop stress, surrounded by a soft, flexible outer cover of a lower flexural modulus material. This design is at best a compromise. In order to provide the hoop stress necessary, a high flexural modulus inner layer is used that, because of its thickness (.02-.07 inches) and its high flexural modulus (51 kpsi) , still provides a too-stiff feel to the golfer.
The present invention takes a different approach, that of providing an additional wound rather than solid layer to provide the necessary hoop stress. This layer is wound of a high tensile elastic modulus material such as aromatic polyamide fibers (for example aramid fibers sold by E.I. duPont De Nemours Co., Wilmington, DE, under the trademark of "Kevlar") , glass fiber, or metal wire. This wound high tensile elastic modulus layer under the cover gives a soft and flexible construction element that serves to provide the hoop stress while contributing minimally to the hardness of feel. By providing this wound layer, the cover material may be chosen for spin, feel and durability alone, without adding structural requirements as well.
The invention has a further benefit for golfers with a low swing speed. A low swing speed does not sufficiently compress the gclf ball at impact, and thus does not generate high enough internal stresses in the ball to achieve the explosive rebound off the club face which is enjoyed by those with higher swing speeds. The contact time between the ball and club face is longer and the golfer does not get the same crisp feel. A high modulus hoop stress layer will produce higher internal stresses at low swing
speeds, giving these players enhanced rebound and feel. A further advantage to the invention is that the moment of inertia of the ball, and thus its spin characteristics, can be controlled by choosing the mass density and thickness of the hoop stress layer. For example, a very high moment of inertia could be created by using metallic wire in the wound hoop stress layer. The result would be a ball with a relatively low initial spin rate and low spin decay rate during flight. These and other advantages of the invention will be discussed below.
Summary of the Invention
The invention includes a golf ball having a substantially spherical inner core, a first wound layer of high tensile elastic modulus fibers wound about the inner core, and a second molded layer of a polymeric material surrounding the wound layer. The invention also includes a method of making a golf ball, including providing an inner core, winding a high elastic modulus fiber on the inner core to create a first wound layer, and molding an outer layer of polymeric material about the first wound layer. The inner core in the above method and apparatus may be made of solid resilient materials or a center wound with a low modulus fiber under an initial tension.
Brief Description of the Drawings
Fig. 1 illustrates a cut-away view of a solid inner core golf ball in accordance with the current invention;
Fig. 2 illustrates a cross-section of a wound inner core golf ball in accordance with the present invention; and
Fig. 3 illustrates a hollow golf ball center for a golf ball in accordance with the present invention.
Detailed Description In Fig. 1, a substantially spherical inner core 100 has a wound layer 105 of high tensile elastic modulus material
wound about it. This wound layer has a cover layer 110 of polymeric material molded about and surrounding it.
The inner core is solid and formed of a resilient material, preferably a polybutadiene or natural rubber containing compound.
The wound layer is formed of high tensile fiber wound about the inner core and preferably in contact with the inner core. A variety of high tensile modulus fibers may provide the requisite hoop stress in a minimally thick layer, preferably glass, Dacron, polyamide, aromatic polyamide (such as duPont's Kevlar aramid fiber), carbon, or metal fibers. Metals such as steel (particularly stainless steel) - monel metal, or titanium are preferred. If a wound layer is created from metal fiber, the ball will have an increased moment of inertia, and thus will rotate at a slower speed when struck with a golf club, and will retain its rotational velocity longer during flight.
The strength of these high tensile elastic modulus fibers is preferably high to accommodate the extremely high stresses placed upon the golf ball windings when it is struck with a golf club. It can be varied, however, to provide a golf ball with a good feel and durability. A tensile strength of at least 250 kpsi is preferred, however a tensile strength of at least 500 kpsi is more preferred. The tensile elastic modulus of the high tensile elastic modulus fiber along with its gauge or thickness may also be varied to provide a stiffer, a softer or a more durable ball as desired. A modulus of at least 10000 kpsi is preferred. A modulus of at least 20000 kpsi is most preferred. In the preferred embodiment, a single fiber is wound about the inner core to create the wound layer. The fiber is preferably a continuous fiber to provide for ease of winding. The fiber material is preferably in yarn, thread or filament form. The wound layer 105 preferably has an outside diameter of between 1.40 and 1.81 inches, and an inside diameter of
between 1.30 and 1.80 inches. The wound layer is preferably wound to a thickness of between 0.01 and 0.10 inches.
The cover layer 110 preferably has an outside diameter of between 1.68 and 1.85 inches. More preferably, it has an 5 outside diameter of between 1.68 and 1.72 inches. Its thickness is preferably between 0.04 and 0.14 inches. The preferred cover materials are an iono er (such as the variety of ionomers sold by the DuPont Chemical Company under the trade name of "Surlyn") , or balata, a naturally occurring 0 substance or its synthetic equivalent. This layer is preferably in direct contact with the wound layer. The combined thickness of the wound layer and the cover layer is preferably between 0.05 and 0.24 inches.
Another embodiment is shown in Fig. 2 for a golf 5 ball with a wound inner core. In this embodiment, the inner core of the golf ball is made of a resilient center 115 with a layer 120 of low tensile elastic modulus material wound about it. Layer 120 has a wound layer 125 of high tensile elastic modulus fiber surrounding it. A cover layer 130 is
20 molded about and surrounds wound layer 125.
The resilient center 115 is preferably a solid and preferably made of polybutadiene, however. Fig. 3 shows an alternative embodiment of center 115: a hollow center 135 made of natural rubber that is filled with a suitable liquid
25 or paste-like material 140.
Referring back to Fig. 2, layer 120 surrounding the center may be solid or wound of an elastic material. If wound, it preferably has a tensile elastic modulus less than
30 5000 psi. If layer 120 is wound, an initial strain of at least 100% is preferred. Layer 120 and high elastic modulus layer 125 are preferably in contact, as are layers 125 and 130.
Wound layer 125 has the characteristics described
35 above regarding the wound layer of. Fig. 1. The high tensile elastic modulus fiber that comprises layer 125 should be wound about the core with an initial tension applied to the
fiber during the winding process which provides an initial strain on the fiber being wound. An initial strain of less than 4% is most preferred. An initial strain of less than 10% is more preferred. An initial strain of less than 25% is preferred. The fiber itself is continuous for ease of winding about the core.
Once the wound layer is created, a cover layer is molded about the wound layer, preferably by injection or compression molding processes well known to those of ordinary skill in the art of manufacturing golf balls.
Claims
1. A golf ball comprising: a substantially spherical inner core; a first wound layer of high tensile elastic modulus fiber wound about said core; and a second molded layer of a polymeric material surrounding said wound layer.
2. The golf ball of claim 1, wherein said first wound layer has an inside diameter of between 1.30 and 1.80 inches„
3. The golf ball of claim 2, wherein said first wound layer has a thickness of between 0.01 and 0.10 inches.
4. The golf ball of claim 3, wherein said second molded layer is the cover and has a thickness of between 0.04 and 0.14 inches.
5. The golf ball of claim 4, wherein said fiber is made of a material selected from the group consisting of glass, Dacron, aromatic polyamide, carbon or metal.
6. The golf ball of claim 1, wherein said fiber has a tensile strength of at least 250 kpsi.
7. The golf ball of claim 6, wherein said fiber has a tensile elastic modulus of at least 10000 kpsi.
8. The golf ball of claim 7, wherein said fiber has a tensile elastic modulus of at least 20000 kpsi.
9. The golf ball of claim 8, wherein said fiber is a continuous fiber.
10. The golf ball of claim 1, wherein said core, is comprised of a resilient center and a second wound layer of a low tensile elastic modulus material wound about said resilient center.
11. The golf ball of claim 10, wherein said low tensile elastic modulus material has a modulus of less than 2000 psi.
12. A method of making a golf ball, comprising the steps of: providing an inner core; winding a high elastic modulus fiber on said core to create a first wound layer; molding an outer layer of polymeric material about said first wound layer.
13. The method of claim 12, further comprising a step of tensioning said high elastic modulus fiber as said fiber is wound on said core to provide said fiber with an initial strain of less than about 25%.
14. A method of making a golf ball, comprising the steps of; providing a golf ball center; tensioning a low tensile elastic modulus fiber to have an initial strain of at least 100%; winding said low tensile elastic modulus fiber on said center to create a golf ball inner core having a low modulus wound layer; tensioning a high tensile elastic modulus fiber to have an initial strain of less than about 25%; winding said high tensile elastic modulus fiber about said low modulus wound layer to create a high modulus wound layer; molding a cover layer of polymeric material about said high modulus wound layer.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP50075897A JP3554334B2 (en) | 1995-06-07 | 1996-05-28 | Golf ball with hoop stress wound layer |
AU59353/96A AU5935396A (en) | 1995-06-07 | 1996-05-28 | Golf ball with wound hoop-stress layer |
GB9725590A GB2316877B (en) | 1995-06-07 | 1996-05-28 | Golf ball with wound hoop-stress layer |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US484,243 | 1995-06-07 | ||
US08/484,243 US5713801A (en) | 1995-06-07 | 1995-06-07 | Golf ball with wound hoop-stress layer |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1996040381A1 true WO1996040381A1 (en) | 1996-12-19 |
Family
ID=23923338
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US1996/007793 WO1996040381A1 (en) | 1995-06-07 | 1996-05-28 | Golf ball with wound hoop-stress layer |
Country Status (5)
Country | Link |
---|---|
US (1) | US5713801A (en) |
JP (1) | JP3554334B2 (en) |
AU (1) | AU5935396A (en) |
GB (1) | GB2316877B (en) |
WO (1) | WO1996040381A1 (en) |
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Publication number | Priority date | Publication date | Assignee | Title |
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US711177A (en) * | 1902-06-12 | 1902-10-14 | Kempshall Mfg Co | Playing-ball. |
-
1995
- 1995-06-07 US US08/484,243 patent/US5713801A/en not_active Expired - Fee Related
-
1996
- 1996-05-28 JP JP50075897A patent/JP3554334B2/en not_active Expired - Fee Related
- 1996-05-28 GB GB9725590A patent/GB2316877B/en not_active Expired - Fee Related
- 1996-05-28 WO PCT/US1996/007793 patent/WO1996040381A1/en active Application Filing
- 1996-05-28 AU AU59353/96A patent/AU5935396A/en not_active Abandoned
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US711177A (en) * | 1902-06-12 | 1902-10-14 | Kempshall Mfg Co | Playing-ball. |
Also Published As
Publication number | Publication date |
---|---|
JPH10508782A (en) | 1998-09-02 |
AU5935396A (en) | 1996-12-30 |
GB2316877B (en) | 1999-04-14 |
GB2316877A (en) | 1998-03-11 |
US5713801A (en) | 1998-02-03 |
JP3554334B2 (en) | 2004-08-18 |
GB9725590D0 (en) | 1998-02-04 |
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