WO2006082007A8 - Process and apparatus for the polymerization of ethylene - Google Patents

Process and apparatus for the polymerization of ethylene

Info

Publication number
WO2006082007A8
WO2006082007A8 PCT/EP2006/000783 EP2006000783W WO2006082007A8 WO 2006082007 A8 WO2006082007 A8 WO 2006082007A8 EP 2006000783 W EP2006000783 W EP 2006000783W WO 2006082007 A8 WO2006082007 A8 WO 2006082007A8
Authority
WO
WIPO (PCT)
Prior art keywords
ethylene
polymer particles
gas
discharged
fraction
Prior art date
Application number
PCT/EP2006/000783
Other languages
French (fr)
Other versions
WO2006082007A1 (en
Inventor
Giuseppe Penzo
Cyrus Ahmadzade-Youssefi
Rainer Karer
Ulrich Nieken
Original Assignee
Basell Polyolefine Gmbh
Giuseppe Penzo
Cyrus Ahmadzade-Youssefi
Rainer Karer
Ulrich Nieken
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to PL06706488T priority Critical patent/PL1853635T3/en
Priority to US11/883,713 priority patent/US7582723B2/en
Priority to MX2007009396A priority patent/MX2007009396A/en
Priority to EP06706488A priority patent/EP1853635B1/en
Application filed by Basell Polyolefine Gmbh, Giuseppe Penzo, Cyrus Ahmadzade-Youssefi, Rainer Karer, Ulrich Nieken filed Critical Basell Polyolefine Gmbh
Priority to JP2007553521A priority patent/JP2008528776A/en
Priority to AU2006210053A priority patent/AU2006210053A1/en
Priority to DE602006002026T priority patent/DE602006002026D1/en
Priority to BRPI0607244A priority patent/BRPI0607244B1/en
Priority to KR1020077017950A priority patent/KR101222265B1/en
Priority to CA002592333A priority patent/CA2592333A1/en
Publication of WO2006082007A1 publication Critical patent/WO2006082007A1/en
Priority to IL183737A priority patent/IL183737A0/en
Priority to EGNA2007000690 priority patent/EG24418A/en
Priority to NO20074411A priority patent/NO20074411L/en
Publication of WO2006082007A8 publication Critical patent/WO2006082007A8/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F10/02—Ethene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/0035—Periodical feeding or evacuation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/006—Separating solid material from the gas/liquid stream by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/34—Polymerisation in gaseous state
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C08F6/005—Removal of residual monomers by physical means from solid polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2208/00274—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00761—Discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F110/02—Ethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S526/92—Apparatus for use in addition polymerization processes

Abstract

Process for the polymerization of ethylene or of ethylene with further 1 -olefins, in which the ethylene is polymerized in the presence of a catalyst in a gas-phase reactor and reaction gas comprising propane and unpolymerized ethylene is circulated to remove the heat of polymerization, wherein the polymer particles are discharged continuously or discontinuously from the reactor, the polymer particles are separated from the major part of the concomitantly discharged gas and the polymer particles are degassed, the gas is freed of entrained fine particles and is separated from a low-boiling fraction comprising ethylene or from a high boiling fraction containing further 1-olefins or alkanes having from 4 to 12 carbon atoms in a first separation stage, a propane fraction is separated off in a second separation stage and this propane fraction is used for degassing the polymer particles discharged from the reactor, with the proportion of ethylene in the propane fraction being less than 1 mol% and the proportion of 1-olefins and alkanes having from 4 to 12 carbon atoms in the propane fraction being less than 4 mol%, in each case based on the total propane fraction. Furthermore, an apparatus for carrying out the process. In this way, a high heat discharge from the reactor, satisfactory degassing of the discharged polymer particles and recovery of the reaction gas discharged together with the polymer particles and also the gas used for degassing the polymer particles are made possible.
PCT/EP2006/000783 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene WO2006082007A1 (en)

Priority Applications (13)

Application Number Priority Date Filing Date Title
AU2006210053A AU2006210053A1 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene
MX2007009396A MX2007009396A (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene.
EP06706488A EP1853635B1 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene
BRPI0607244A BRPI0607244B1 (en) 2005-02-04 2006-01-30 process for the polymerization of ethylene or ethylene with other 1-olefins, apparatus for performing the process, and use of propane
JP2007553521A JP2008528776A (en) 2005-02-04 2006-01-30 Ethylene polymerization method and apparatus
US11/883,713 US7582723B2 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene
DE602006002026T DE602006002026D1 (en) 2005-02-04 2006-01-30 METHOD AND DEVICE FOR POLYMERIZING ETHYLENE
PL06706488T PL1853635T3 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene
KR1020077017950A KR101222265B1 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene
CA002592333A CA2592333A1 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene
IL183737A IL183737A0 (en) 2005-02-04 2007-06-07 Process and apparatus for the polymerization of ethylene
EGNA2007000690 EG24418A (en) 2005-02-04 2007-07-03 Process and apparatus for the polymerization of ethylene
NO20074411A NO20074411L (en) 2005-02-04 2007-08-29 Process and apparatus for polymerizing ethylene

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102005005506A DE102005005506A1 (en) 2005-02-04 2005-02-04 Polymerization of ethylene optionally with 1-olefins involves polymerizing ethylene in presence of catalyst to form polymer particles and circulating unpolymerized ethylene to remove heat of polymerization
DE102005005506.0 2005-02-04
US65618505P 2005-02-25 2005-02-25
US60/656,185 2005-02-25

Publications (2)

Publication Number Publication Date
WO2006082007A1 WO2006082007A1 (en) 2006-08-10
WO2006082007A8 true WO2006082007A8 (en) 2007-08-30

Family

ID=36709737

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/000783 WO2006082007A1 (en) 2005-02-04 2006-01-30 Process and apparatus for the polymerization of ethylene

Country Status (22)

Country Link
US (1) US7582723B2 (en)
EP (1) EP1853635B1 (en)
JP (1) JP2008528776A (en)
KR (1) KR101222265B1 (en)
CN (1) CN100537609C (en)
AR (1) AR054728A1 (en)
AT (1) ATE402961T1 (en)
AU (1) AU2006210053A1 (en)
BR (1) BRPI0607244B1 (en)
CA (1) CA2592333A1 (en)
DE (2) DE102005005506A1 (en)
EG (1) EG24418A (en)
ES (1) ES2308718T3 (en)
IL (1) IL183737A0 (en)
MX (1) MX2007009396A (en)
MY (1) MY138311A (en)
NO (1) NO20074411L (en)
PL (1) PL1853635T3 (en)
RU (1) RU2394842C2 (en)
TW (1) TW200630389A (en)
WO (1) WO2006082007A1 (en)
ZA (1) ZA200706446B (en)

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EP2046843B1 (en) 2006-08-03 2010-01-20 Basell Polyolefine GmbH Process for the polyolefin finishing
EP2123682A1 (en) * 2008-05-20 2009-11-25 INEOS Manufacturing Belgium NV Olefin polymerisation process
WO2011045701A1 (en) * 2009-10-16 2011-04-21 Sasol Technology (Proprietary) Limited Separation of components from a multi-component hydrocarbon stream which includes ethylene
MY161690A (en) * 2010-07-09 2017-05-15 Univation Tech Llc Ethylene expansion for low temperature refrigeration in polyethylene vent recovery
EP2723781B1 (en) 2011-06-21 2017-08-30 Basell Polyolefine GmbH Method and apparatus for discharging a polymer from a gas-phase reactor
KR101378892B1 (en) * 2011-07-14 2014-04-04 주식회사 엘지화학 Method of preparing polyolefin resin
EP2768870B1 (en) * 2011-10-17 2018-01-10 Ineos Europe AG Polymer degassing process control
CN104684941B (en) * 2012-10-02 2017-10-03 英尼奥斯欧洲股份公司 Method for improving polyplant operation
EP2743278A1 (en) 2012-12-11 2014-06-18 Basell Polyolefine GmbH Process for degassing and buffering polyolefin particles obtained by olefin polymerization
EP2743279A1 (en) 2012-12-11 2014-06-18 Basell Polyolefine GmbH Process for treating polyolefin particles obtained by gas-phase polymerization
WO2015128329A1 (en) * 2014-02-26 2015-09-03 Ineos Europe Ag Polymerisation process and polymerisation unit comprising a degassing section
EP3237106B1 (en) * 2014-12-22 2018-09-12 SABIC Global Technologies B.V. Recovery of hydrocarbons from a hydrocarbon recycle
EP3313898B1 (en) 2015-07-31 2020-03-04 ExxonMobil Chemical Patents Inc. Recovery of unreacted monomers from olefin polymerization processes
EP3377537B2 (en) 2015-11-18 2022-02-16 Basell Polyolefine GmbH Polymerization process with a partial shutdown phase
WO2017102303A1 (en) * 2015-12-15 2017-06-22 Sabic Global Technologies B.V. Olefin polymerization process
GB201620525D0 (en) 2016-12-02 2017-01-18 Ineos Europe Ag Process
ES2786567T3 (en) * 2017-06-23 2020-10-13 Borealis Ag Procedure and apparatus for the withdrawal of polymeric material from an olefin polymerization reactor with gases and solid
EP3438133A1 (en) 2017-08-04 2019-02-06 Basell Polyolefine GmbH Polymerization process including discharging polyolefin particles from a gas-phase polymerization reactor
CN108854859B (en) * 2018-07-27 2023-08-18 中化蓝天霍尼韦尔新材料有限公司 Suspension gas-liquid phase reaction device and operation method
CN113166284B (en) * 2018-12-18 2023-02-24 巴塞尔聚烯烃股份有限公司 Gas phase process for preparing ethylene polymers
CN112745435B (en) * 2019-10-31 2022-07-12 中国石油化工股份有限公司 Process for converting polymer slurry into polymer solution and process for producing butyl rubber
US11820841B2 (en) * 2020-01-28 2023-11-21 Exxonmobil Chemical Patents Inc. Reducing accumulation of C6+ hydrocarbon components in polyolefin gas-phase reactors
EP4046981A4 (en) * 2020-09-07 2023-06-28 LG Chem, Ltd. Method for preparing oligomer
KR20220104418A (en) * 2021-01-18 2022-07-26 주식회사 엘지화학 Method for preparing oligomer
CN115246903B (en) * 2021-04-28 2023-09-12 中国石油化工股份有限公司 Continuous solution polymerization process
JP2024007084A (en) * 2022-07-05 2024-01-18 住友化学株式会社 Polyolefin production apparatus and polyolefin production method

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Also Published As

Publication number Publication date
BRPI0607244A2 (en) 2010-03-23
ATE402961T1 (en) 2008-08-15
EP1853635A1 (en) 2007-11-14
IL183737A0 (en) 2007-09-20
MY138311A (en) 2009-05-29
PL1853635T3 (en) 2009-01-30
CA2592333A1 (en) 2006-08-10
TW200630389A (en) 2006-09-01
CN100537609C (en) 2009-09-09
US20080177012A1 (en) 2008-07-24
CN101107273A (en) 2008-01-16
DE602006002026D1 (en) 2008-09-11
JP2008528776A (en) 2008-07-31
MX2007009396A (en) 2007-09-25
RU2007129830A (en) 2009-02-10
BRPI0607244B1 (en) 2016-05-31
US7582723B2 (en) 2009-09-01
AU2006210053A1 (en) 2006-08-10
AR054728A1 (en) 2007-07-11
DE102005005506A1 (en) 2006-08-10
WO2006082007A1 (en) 2006-08-10
KR20070116221A (en) 2007-12-07
RU2394842C2 (en) 2010-07-20
ES2308718T3 (en) 2008-12-01
EP1853635B1 (en) 2008-07-30
KR101222265B1 (en) 2013-01-15
EG24418A (en) 2009-05-25
NO20074411L (en) 2007-10-31
ZA200706446B (en) 2008-06-25

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