WO2009048573A3 - Densification of metal oxides - Google Patents
Densification of metal oxides Download PDFInfo
- Publication number
- WO2009048573A3 WO2009048573A3 PCT/US2008/011586 US2008011586W WO2009048573A3 WO 2009048573 A3 WO2009048573 A3 WO 2009048573A3 US 2008011586 W US2008011586 W US 2008011586W WO 2009048573 A3 WO2009048573 A3 WO 2009048573A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- methods
- present
- densification
- metal oxides
- nanocrystalline
- Prior art date
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
- C04B35/486—Fine ceramics
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G25/00—Compounds of zirconium
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G25/00—Compounds of zirconium
- C01G25/02—Oxides
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
- C04B35/645—Pressure sintering
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
- C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/608—Green bodies or pre-forms with well-defined density
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- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/76—Crystal structural characteristics, e.g. symmetry
- C04B2235/762—Cubic symmetry, e.g. beta-SiC
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/76—Crystal structural characteristics, e.g. symmetry
- C04B2235/765—Tetragonal symmetry
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/78—Grain sizes and shapes, product microstructures, e.g. acicular grains, equiaxed grains, platelet-structures
- C04B2235/781—Nanograined materials, i.e. having grain sizes below 100 nm
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/78—Grain sizes and shapes, product microstructures, e.g. acicular grains, equiaxed grains, platelet-structures
- C04B2235/785—Submicron sized grains, i.e. from 0,1 to 1 micron
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
Abstract
The present invention relates to methods for manufacturing of fully densified nanocrystalline metal oxide ceramic materials at low sintering temperature. Methods of the invention involve dry compaction of a product resulting from hydrothermal treatment of metal ion suspensions and subsequent sintering. The present invention may produce ceramic bodies that exhibit nanocrystalline structural features with measured densities that are found to be extremely similar to the theoretical density.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/682,048 US20100272997A1 (en) | 2007-10-10 | 2008-10-08 | Densification of metal oxides |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US99849907P | 2007-10-10 | 2007-10-10 | |
US60/998,499 | 2007-10-10 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2009048573A2 WO2009048573A2 (en) | 2009-04-16 |
WO2009048573A3 true WO2009048573A3 (en) | 2009-07-23 |
Family
ID=40549780
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2008/011586 WO2009048573A2 (en) | 2007-10-10 | 2008-10-08 | Densification of metal oxides |
Country Status (2)
Country | Link |
---|---|
US (1) | US20100272997A1 (en) |
WO (1) | WO2009048573A2 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2463257B1 (en) * | 2009-08-07 | 2018-06-06 | Tosoh Corporation | Transparent zirconia sintered body and method for producing same |
CN105338948B (en) | 2013-06-27 | 2019-02-01 | 义获嘉伟瓦登特股份有限公司 | Nanocrystal zirconium oxide and its processing method |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4518397A (en) * | 1979-06-29 | 1985-05-21 | Minnesota Mining And Manufacturing Company | Articles containing non-fused aluminum oxide-based abrasive mineral |
US4774041A (en) * | 1983-10-17 | 1988-09-27 | Toyo Soda Manufacturing Co. Ltd. | High-strength zirconia type sintered body and process for preparation thereof |
CA2014482A1 (en) * | 1989-04-17 | 1990-10-17 | Paul Moltgen | Production of alpha-al 0 sintered bodies |
JP2001303237A (en) * | 2000-04-25 | 2001-10-31 | Mitsubishi Heavy Ind Ltd | METHOD FOR MANUFACTURING In-Sn OXIDE POWDER AND ITO TARGET MATERIAL |
US6540130B1 (en) * | 1996-03-27 | 2003-04-01 | Roedhammer Peter | Process for producing a composite material |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0218853B1 (en) * | 1985-09-06 | 1994-11-09 | Toray Industries, Inc. | Method for manufacturing a sintered zirconia material |
JPH07267730A (en) * | 1994-03-30 | 1995-10-17 | Sumitomo Electric Ind Ltd | Zirconia vane for rotary compressor |
US6087285A (en) * | 1997-10-13 | 2000-07-11 | Tosoh Corporation | Zirconia sintered body, process for production thereof, and application thereof |
US6168745B1 (en) * | 1998-11-28 | 2001-01-02 | Materials And Systems Research, Inc. | Method for forming t'-phase zirconia for high temperature applications |
SG107103A1 (en) * | 2002-05-24 | 2004-11-29 | Ntu Ventures Private Ltd | Process for producing nanocrystalline composites |
DE102004004259B3 (en) * | 2004-01-23 | 2005-11-24 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Transparent polycrystalline sintered ceramics of cubic crystal structure |
JP2008511524A (en) * | 2004-09-01 | 2008-04-17 | アドバンスド ナノテクノロジー リミテッド | Zirconia ceramic |
US7241437B2 (en) * | 2004-12-30 | 2007-07-10 | 3M Innovative Properties Company | Zirconia particles |
WO2006091613A2 (en) * | 2005-02-24 | 2006-08-31 | Rutgers, The State University Of New Jersey | Nanocomposite ceramics and process for making the same |
US7601403B2 (en) * | 2005-04-15 | 2009-10-13 | The Regents Of The University Of California | Preparation of dense nanostructured functional oxide materials with fine crystallite size by field activation sintering |
JP2007009646A (en) * | 2005-07-04 | 2007-01-18 | Panahome Corp | Safety door |
CN101573308B (en) * | 2006-12-29 | 2016-11-09 | 3M创新有限公司 | zirconia body and method |
GB0821674D0 (en) * | 2008-11-27 | 2008-12-31 | Univ Loughborough | Ceramic |
-
2008
- 2008-10-08 US US12/682,048 patent/US20100272997A1/en not_active Abandoned
- 2008-10-08 WO PCT/US2008/011586 patent/WO2009048573A2/en active Application Filing
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4518397A (en) * | 1979-06-29 | 1985-05-21 | Minnesota Mining And Manufacturing Company | Articles containing non-fused aluminum oxide-based abrasive mineral |
US4774041A (en) * | 1983-10-17 | 1988-09-27 | Toyo Soda Manufacturing Co. Ltd. | High-strength zirconia type sintered body and process for preparation thereof |
CA2014482A1 (en) * | 1989-04-17 | 1990-10-17 | Paul Moltgen | Production of alpha-al 0 sintered bodies |
US6540130B1 (en) * | 1996-03-27 | 2003-04-01 | Roedhammer Peter | Process for producing a composite material |
JP2001303237A (en) * | 2000-04-25 | 2001-10-31 | Mitsubishi Heavy Ind Ltd | METHOD FOR MANUFACTURING In-Sn OXIDE POWDER AND ITO TARGET MATERIAL |
Also Published As
Publication number | Publication date |
---|---|
US20100272997A1 (en) | 2010-10-28 |
WO2009048573A2 (en) | 2009-04-16 |
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